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This book examines the meso- and nanoscopic aspects of fluid adsorption in porous solids using a non-invasive method of small angle neutron scattering (SANS) and small angle x-ray scattering (SAXS). Starting with a brief summary of the basic assumptions and results of the theory of small-angle scattering from porous media, the author focuses on the practical aspects and methodology of the ambient and high pressure SANS and SAXS experiments and corresponding data analysis. It is illustrated with results of studies of the vapor and supercritical fluid adsorption in porous materials published during the last decade, obtained both for man-made materials (e.g. porous fractal silica, Vycor glass, activated carbon) and geological samples (e.g. sandstones, shales and coal). In order to serve the needs of broad readership, the results are presented in the relevant context (e.g. petroleum exploration, anthropogenic carbon capture and sequestration, ion adsorption in supercapacitors, hydrogen storage, etc.).
Small-angle scattering of X-rays (SAXS) and neutrons (SANS) is an established method for the structural characterization of biological objects in a broad size range from individual macromolecules (proteins, nucleic acids, lipids) to large macromolecular complexes. SAXS/SANS is complementary to the high resolution methods of X-ray crystallography and nuclear magnetic resonance, allowing for hybrid modeling and also accounting for available biophysical and biochemical data. Quantitative characterization of flexible macromolecular systems and mixtures has recently become possible. SAXS/SANS measurements can be easily performed in different conditions by adding ligands or binding partners, and by changing physical and/or chemical characteristics of the solvent to provide information on the structural responses. The technique provides kinetic information about processes like folding and assembly and also allows one to analyze macromolecular interactions. The major factors promoting the increasingly active use of SAXS/SANS are modern high brilliance X-ray and neutron sources, novel data analysis methods, and automation of the experiment, data processing and interpretation. In this book, following the presentation of the basics of scattering from isotropic macromolecular solutions, modern instrumentation, experimental practice and advanced analysis techniques are explained. Advantages of X-rays (rapid data collection, small sample volumes) and of neutrons (contrast variation by hydrogen/deuterium exchange) are specifically highlighted. Examples of applications of the technique to different macromolecular systems are considered with specific emphasis on the synergistic use of SAXS/SANS with other structural, biophysical and computational techniques.
This book covers the most common neutron detectors used in neutron scattering facilities and all of those in use at Oak Ridge National Lab. It starts describing the facilities, instruments and the critical detector parameters needed by various instruments. Then the key components of the 3He-based linear position-sensitive detectors as well as on their electronics, which require particular attention to signal processing and noise reduction, are introduced. One chapter is dedicated to the 3He alternatives where scintillators play a critical role. It also covers emerging neutron detection technologies including semiconductors, vacuum-based devices and their associated readouts, which will be required in the future for high rate and high-resolution neutron detectors. The authors explain the logic behind the choice of materials as well as the various constraints that neutron detectors must respect to be useful. Some of these constraints, such as efficiency and gamma-ray sensitivity are common to all neutron counters while others, like timing resolution, dynamic range, and peak counting rate, depend on the applications. The book guides experts, the nuclear science community, and young scholars through the physical processes and the required electronics in a way that is accessible for those not professionally involved in designing detector’s components and electronic circuits.
Based partly on the original importers' catalogues and partly on the wide range of pieces handled by the author Bryan Catley, a leading specialist in the subject, this book covers a comprehensive range of art deco figures. Between the wars, an entirely modern style of decorative sculpture emerged which was a complete break with the heavy romantic late 19th century schools, and was totally in sympathy with the vibrant young society of the 1920s. The use of bronze and ivory for the great number of these sensual figures in no way obscures the the fact that many are of exceptionally high quality; add to this their sense of movement and rhythm and one realises that the large sums thay now command is a reflection of a discriminative international collectors' market. This new revised edition provides a comprehensive listing of the great variety and range of figures, of which there are still more to be found.
Neutron scattering proves itself a highly international area of research as scientists and engineers from twenty-one countries come together in this volume - to discuss the growth and maturation of the use of neutrons as a probe in materials research and to survey current applications. A wide range of materials are examined, including polymers, cements, high-Tc superconducting oxides and carbides, inorganic glasses, magnetic films, ceramics and metallic alloys. Topics include: instrumentation at major neutron facilities in North America; developments in instrumentation and techniques; neutron reflectivity studies of surfaces and interfaces; small angle neutron scattering (SANS) studies of polymers and complex fluids; SANS studies of ceramics and metals; residual stress analysis; cementitious materials; high-Tc superconducting materials; interfaces, multilayers and nanocrystals of magnetic materials; oxide materials; inorganic glasses; alloys; and adsorbed systems, inelastic scattering and dynamics.
Neutron spin echo (NSE) spectroscopy is the highest energy resolution neutron scattering technique available for examining a large area (in time and space) in condensed matter physics. This broad dynamic and spatial range is extensively exploited in the study of a wide range of scientific problems ranging from the dynamics of glasses, polymer melts, complex fluids and microemulsions to the elementary excitations in superfluid 4He and to ferromagnets and spin glasses. This book reviews the current status and future prospects in NSE spectroscopy describing the method, latest instrumentation and also the use of NSE in fundamental, hard- and soft-matter science. It provides first-hand information for researchers working in the fields touched by NSE. In addition, young researchers, PhD students and graduates interested in the method will obtain a comprehensive overview and guidelines to implementing the NSE technique.
This book provides a comprehensive and up-to-date introduction to the fundamental theory and applications of slow-neutron scattering.