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Volume 20 of Reviews in Mineralogy attempted to: (1) provide examples illustrating the state-of-the-art in powder diffraction, with emphasis on applications to geological materials; (2) describe how to obtain high-quality powder diffraction data; and (3) show how to extract maximum information from available data. In particular, the nonambient experiments are examples of some of the new and exciting areas of study using powder diffraction, and the interested reader is directed to the rapidly growing number of published papers on these subjects. Powder diffraction has evolved to a point where considerable information can be obtained from ug-sized samples, where detection limits are in the hundreds of ppm range, and where useful data can be obtained in milliseconds to microseconds. We hope that the information in this volume will increase the reader's access to the considerable amount of information contained in typical diffraction data.
"Highlights in Mineralogical Crystallography" presents a collection of review articles with the common topic: structural properties of minerals and synthetic analogues. It is a valuable resource for mineralogists, materials scientists, crystallographers, and earth scientists. This book includes: An introduction to the RRUFF database for structural, spectroscopic, and chemical mineral identification. A systematic evaluation of structural complexity of minerals. ab initio computer modelling of mineral surfaces. Natural quasicrystals of meteoritic origin. The potential role of terrestrial ringwoodite on the water content of the Earth's mantle. Structural characterization of nanocrystalline bio-related minerals by electron-diffraction tomography. The uniqueness of mayenite-type compounds as minerals and high-tech ceramics.
reviewers, and reported by users of the earlier This third edition (or issue) of the Quantitative Data File for ore minerals (QDF) of the Commission on editions. The result is that 510 species and 125 are Mineralogy of the International Mineralogical compositional or structural variants, or varieties, of Association (COM-IMA) is published, with the species, are represented in QDF3. A large number of support of the Natural History Museum, London, by the entries include data collected from the type Chapman & Hall. It has been greatly revised and specimen of a mineral: these include data extracted enlarged and now includes graphs of the reflectance from the published literature. In this respect, QDF3 spectra for all of its entries. These have been differs from earlier editions. included in response to requests from users of the We have also revised and simplified the notes earlier editions. Also included, for those users concerning X-ray data: no longer are the strongest unfamiliar with the application of such spectra to lines in the powder diffraction pattern quoted, nor mineral identification, are introductory notes, are cell dimensions generally given. Instead, it was illustrated with examples of R spectra. decided to refer to data from the original description, The 635 data sets, which are arranged or to data in the PDF of the JCPDS.
Mandarino and Anderson are the first to bring together all of the known data on this classic mineral locality, Mont Saint-Hilaire, Quebec. This site is one of the most important sources of rare and beautiful minerals in the world. The location is outstanding, both for the rarity of its minerals anf the number of its mineral species. Over 200 mineral species have been identified a Mont Saint-Hilaire, including some found nowhere else or located only in remote areas of the earth. The numerous mineral species found at Mont Saint-Hilaire are described in detail and handsomely illustrated in almost 200 color and black-and-white photomicrographs, sketches, and crystal drawings. The text consists mostly of mineral description and addresses the interests of amateur and professional mineralogists alike. Five appendices present specialized technical data on unit cell parameters, X-ray powder diffraction, occurrence, mineral classification, and chemical analysis for the professional. The book will be a valuable aid to the reader in the identificaton and collection of minerals.
A little over ?ve years have passed since the ?rst edition of this book appeared in print. Seems like an instant but also eternity, especially considering numerous developments in the hardware and software that have made it from the laboratory test beds into the real world of powder diffraction. This prompted a revision, which had to be beyond cosmetic limits. The book was, and remains focused on standard laboratory powder diffractometry. It is still meant to be used as a text for teaching students about the capabilities and limitations of the powder diffraction method. We also hope that it goes beyond a simple text, and therefore, is useful as a reference to practitioners of the technique. The original book had seven long chapters that may have made its use as a text - convenient. So the second edition is broken down into 25 shorter chapters. The ?rst ?fteen are concerned with the fundamentals of powder diffraction, which makes it much more logical, considering a typical 16-week long semester. The last ten ch- ters are concerned with practical examples of structure solution and re?nement, which were preserved from the ?rst edition and expanded by another example – R solving the crystal structure of Tylenol .
In this, the only book available to combine both theoretical and practical aspects of x-ray diffraction, the authors emphasize a "hands on" approach through experiments and examples based on actual laboratory data. Part I presents the basics of x-ray diffraction and explains its use in obtaining structural and chemical information. In Part II, eight experimental modules enable the students to gain an appreciation for what information can be obtained by x-ray diffraction and how to interpret it. Examples from all classes of materials -- metals, ceramics, semiconductors, and polymers -- are included. Diffraction patterns and Bragg angles are provided for students without diffractometers. 192 illustrations.