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Newer Methods of Preparative Organic Chemistry, Volume III focuses on the improved methods in preparative organic chemistry. This book presents a variety of topics, including the synthesis of acetylenes, methods for the preparation of pyrylium salts, and the use of phosphoric acid chlorides in the preparation of esters of phosphoric acids. Organized into 11 chapters, this volume starts with an overview of the reaction between methylene and sulfur involving dehydrogenation or oxidation. This text then examines the chemistry of pyridine, which exhibits different reaction characteristics than benzene. Other chapters consider the cyclic derivatives of carboxylic acids, such as lactams, lactones, or thiolactones, which can be converted by partial reduction into heterocycles of the same ring size. The final chapter outlines the fundamental reactions of diazoketones and discusses the preparative significance of the diazoketones. This book is a valuable resource for synthetic organic chemists involved in research institutions and industrial laboratories.
Newer Methods of Preparative Organic Chemistry, Volume II focuses on several improved methods in preparative organic chemistry. This book presents a variety of detailed laboratory procedures in organic chemistry. Organized into 14 chapters, this volume starts with an overview of the compound acetoacetaldehyde, which is prepared from sodium formylacetone with acetic anhydride in ether. This text then explains the requirements I a rational peptide synthesis, including controlled reaction conditions, retention of optical activity, high yields, and analogous applicability to free amino acids and to terminal amino acids of oligopeptides. Other chapters consider the general equation of the inner anhydride of acetic acid. This book discusses as well the relation between polarity and reactivity in phosphines. The final chapter deals with the methylation of aromatic compounds, which is a typical radical reaction. This book is intended for synthetic organic chemists. Graduate students and research workers in the fields of organic chemistry and biochemistry will find this book useful.
Index to Reviews, Symposia Volumes and Monographs in Organic Chemistry for the Period 1940-1960 presents a resume of published monographs, reviews, and symposia lectures in organic chemistry. The editors adopted the plan of listings by symposia volume or journal, backed up by the total subject and author indexes. In this way the user can readily locate a particular article through the author index or the subject index; or should he recall that an article appeared in a particular source, the chronological listing in that source can be scanned quickly. The Index gives a convenient overview of the accomplishments of organic chemists during this very prolific period of the growth of the field. Frequently, several articles on the same or similar subject appear, hence the historical perspective can be sensed by rapid evaluation of the reviews selected. This Index will be useful to research workers, teachers and students. It will also assist editors and authors to select specific areas which require critical review.
Methods for the Oxidation of Organic Compounds: Alcohols, Alcohol Derivatives, Alkyl Halides, Nitroalkanes, Alkyl Azides, Carbonyl Compounds, Hydroxyarenes and Aminoarenes describes the different methods used for the controlled oxidation of alcohols, alcohol derivatives, alkyl halides, nitroalkanes, alkyl azides, carbonyl compounds, hydroxyarenes, and aminoarenes. Most of the oxidative techniques considered are illustrated with detailed experimental procedures taken from the literature. This book is comprised of eight chapters and begins with a discussion on the oxidation of alcohols, with particular emphasis on the formation of carbonyl compounds and carboxylic acids. The following chapters focus on the oxidation of esters and alkyl halides; ethers, acetals, and metal derivatives of alcohols; amines, nitro compounds, and azides; carbonyl compounds; 1,2-diols and related compounds; and hydroxyarenes, aminoarenes, dihydroxyarenes, diaminoarenes, and aminohydroxyarenes. Methods such as catalytic oxidation, catalytic dehydrogenation, and electrochemical and biochemical oxidation are mentioned. This monograph should be of interest to organic chemists and research students.
Includes Part 1, Number 2: Books and Pamphlets, Including Serials and Contributions to Periodicals July - December)