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That the field of Mossbauer spectroscopy continues for the remarks section of the index, and the inclusion to be an important growth area in science and tech of some new appendices and tables (such as the en nology, despite recent economic pressures, is ade ergy conversion tables, nuclear radius and moment quately evidenced by the present volume. Covering re data, and the report of the ASTM Task Group on search published only in the year 1969, its size is com Mossbauer Nomenclature and Conventions). The parable to its predecessor, Mossbauer Effect Data advertisement section, too, provides a collection of Index 1958-1965. With such continuing growth in information useful to many readers. many fields, the need for specialized information re In summary, the new editors are to be congratulated trieval tools for the research worker is now becoming for their excellent and tremendous effort in putting together such a fine compilation in a remarkably short an increasingly important internationally recognized time. The user community, I am sure, will strongly concern. MEDI 1969 satisfies much of this need for the community it addresses in a timely manner. urge them to continue this series, as I know their pred This work not only follows in the footsteps of its ecessor has been urged to help fill the gap for the years 1966-1968. predecessor, but also includes a number of important and very useful innovations. Among these are the classification of substances investigated according to ARTHUR H. MUIR, JR.
When presented with a new compound or material, the inorganic chemist will usually have several questions in mind about its composition and structure. Although a simple elemental analysis may answer many questions about its composition, the chemist will still have questions about its structure, and, ifthe material contains a metal atom, he will often want to know its oxidation state, coordination number and geometry. Further, at an increasingly frequent rate, the chemist may need details of the spin state, magnetic and perhaps dynamic properties of the material. If the investigator is fortunate, the material or compound may contain an ele ment such as iron, tin, antimony, iodine, gold, or one of several of the rare earth metals which are amenable to study by the Mossbauer effect. Often the Mossbauer effect can, sometimes with quite simple experiments, provide the answers to all of these questions. The goal of this book is to illustrate the effectiveness of the Mossbauer effect in providing the answers to the many questions that arise in char acterizing new materials and, indeed, in studying known materials in more detail. Several chapters introduce the effect to the novice and provide details about the various hyperfine interactions that are the "bread and butter" of the Mossbauer spectroscopist. Three chapters deal specifically with the experimental aspects of the technique and the increasing impor tance of sophisticated computer analysis of the resulting data.
This is the ninth volume of a continuing series intended to provide a forum for publication of develop ments in Mossbauer effect methodology and in spectroscopy and its applications. Mossbauer Effect Methodology, Volume 9, records the proceedings of the Ninth Symposium on Mossbauer Effect Methodology. The symposium was sponsored by the New England Nuclear Corporation and interest was concentrated on spectroscopy and applications, with more than usual emphasis on new methodology. The symposium was held in the Palmer House in Chicago on February 3, 1974. Dr. Stanley Hanna presided over the afternoon and evening sessions. Attendance was lower than usual; about one hundred participants were present. This may reflect the continu ing pressure of travel budget limitations. Contributing Sponsors were Austin Science Associates, El Scint, Inc., Nuclear Science Instruments and Ranger Electronics. These organizations demonstrated their products for Mossbauer applications. The continuing improvements in the spectrometers and their adjuncts was evident. The Selection Committee again had a most difficult task, and was obliged to accept only about half of the submitted papers. A most interesting group of papers on applications and spectroscopy featured reports on electronic relaxation phenomena, magnetic phase and spin transformations, photochromism in strontium titanate, lattice studies, and phase determination by Kossel analysis. The excellent methodology session included presentations on data analysis techniques for spectral folding, hyperfine interaction analysis and recoil-free fraction measurement, a backscatter spectrometer and a report on a Selective Excitation Double Mossbauer method to study time-dependent phenomena.
This referenced compilation of magnetic transition temperatures represents (with the Addendum) papers actually received by the RMIC through May 1972 and consists of two lists (alphabetical by compounds), one for Curie and one for Neel temperatures. Where different values appeared in the literature for a single compound, all are listed with sepa rate references given for each. There is no attempt at critical evaluation, which, except for a few welt-studied and well characterized materials, would hardly be worth the effort. All that one can say for most of the compounds is that for a given material with a certain (or all too often uncertain) history of preparati'on and treatment, stoichiometry, homoge neity, and chemical or structural purity a magnetic transition was indicated at the temperature(s) listed. Only when the reasons for different values are explicitly stated in the literature do they appear as brief comments in the body of the lists. In order to include the most recent data, and to eliminate the delay involved in recomposition of the lists, an addendum is provided. While this requires the perusal of two lists rather than one, it does ensure that the compilation represents the entire RMIC collection at the moment of going to press. The 2478 references are restricted to those papers specifying a Curie or Neel temperature and do not reflect the complete magnetics literature even for the materials listed.
Spectroscopic Properties of Inorganic and Organometallic Compounds provides a unique source of information on an important area of chemistry. Divided into sections mainly according to the particular spectroscopic technique used, coverage in each volume includes: NMR (with reference to stereochemistry, dynamic systems, paramagnetic complexes, solid state NMR and Groups 13-18); nuclear quadrupole resonance spectroscopy; vibrational spectroscopy of main group and transition element compounds and coordinated ligands; and electron diffraction. Reflecting the growing volume of published work in this field, researchers will find this Specialist Periodical Report an invaluable source of information on current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading experts in their specialist fields, this series is designed to help the chemistry community keep current with the latest developments in their field. Each volume in the series is published either annually or biennially and is a superb reference point for researchers. www.rsc.org/spr
This year's issue is again exciting not only because People with common goals establish communities. Usually, in the natural sciences, communities originate it lists the 1 OOth excited resonance state, but also be around fields because institutions, conferences, and cause it contains extensive new information and addi 197 the literature are normally field oriented. In excep tional interesting articles on Au by Louis Roberts, 151 tional cases, communities have a method as the com Eu by Chris Barton and Norman Greenwood, and 129 mon bond, for instance, Mossbauer spectroscopy. The I by Hendrick deWaard. One innovation might be minimum requirement to be a "Mossbauer woman or suggested: for our irreproducible results we have the man" seems to be the possession of a Mossbauer sys International Journal of Irreproducible Results; how tem and the MEDI. Every member of the M6ssbauer ever, there is no literature for our reproducible nega community must have realized our extremely fortunate tive results. Sometimes nature's hidden tricks are un situation: before we put a drive system into motion known to us and experiments with some isotopes are we know within minutes if similar work has been pub tried unsuccessfully again and again. A chapter for lished somewhere in the world.
Solid State Physics
Spectroscopy in Heterogeneous Catalysis deals with the applications of spectroscopy in heterogeneous catalysis. The concepts and capabilities of a particular technique, experimental procedures, and examples of all proven or potentially important applications are discussed. The use of spectroscopic measurements in guiding empirical approaches to applied problems and to fundamental studies of the chemical identity of catalytic surfaces is also described. This book is comprised of eight chapters and begins with a discussion on the scope of spectroscopy in catalysis and applications of spectroscopy to zeolite catalysts. The following chapters focus on infrared spectroscopy, with emphasis on the theory and interpretation of infrared spectra; Raman spectroscopy and the theory of the Raman effect; diffuse reflectance and photoacoustic spectroscopies; and Mössbauer spectroscopy. Electron spin resonance spectroscopy and nuclear magnetic resonance spectroscopy are also considered. The final chapter is devoted to X-ray photoelectron spectroscopy (XPS) and its application to core electrons, along with the experimental equipment and procedures used. The applications of XPS to studies of surface behavior and catalyst composition and chemistry are outlined. This monograph will be a useful resource for physicists, researchers, and potential researchers in heterogeneous catalysis.
Here in one source is a wide variety of practical, everydayinformation often required by chemists but seldom found together,if at all, in the standard handbooks, data collections, manuals,and other usual sources. Discussing physical, chemical, andmechanical properties of substances and systems, the authors answersuch questions as: * How do I test for and destroy peroxides in different solventsand what is the best way to purify such solvents? * What are the structure, physical properties, and recentreferences to the use of common-name solvents and solvent aids suchas the "Skellysolves," "Cellosolves," "Crownanes," and"Glymes"? * What is the utility of a particular molecular sieve, orpermeation gel, or epoxy cement, or liquid crystal, and where do Ibuy them and find references to their application? The book is divided into nine chapters and covers properties ofatoms and molecules, spectroscopy, photochemistry, chromatography,kinetics and thermodynamics, various experimental techniques, andmathematical and numerical information, including the definitions,values, and usage rules of the newly adopted International Systemof Units (SI Units). A section on statistical treatment of datawhich provides an actual least-squares computer program is alsoincluded. In the spectroscopy chapter, very extensive andup-to-date collections of spectral correlation data are presentedfor ir, uv-vis, optical rotation, nmr, and mass spectra, along withdata on esr and nqr spectroscopy. Also included is a variety ofhard-to-classify but frequently sought information, such as namesand addresses of microanalysis companies and chemistry publishers,descriptions and commercial sources of atomic and molecular models,and safety data for hazardous chemicals. More than 500 keyreferences are also included, most of which are recent. There areimportant hints and definitions associated with the art as well asthe state of the art for the appropriate subjects. Also foundthroughout the book are about 250 suppliers and directions forobtaining special booklets or other material. Containing a wealth of useful information, The Chemist'sCompanion will be an indispensable guide for students andprofessional chemists in nearly all the chemical disciplines. Inaddition, it will provide for the teacher and student an unusualadjunct for use in a broad cross-section of chemistry courses.