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Carbohydrate Analysis by Modern Liquid Phase Separation Techniques, Second Edition, presents readers with the various principles of modern liquid phase separation techniques and their contributions to the analysis of complex carbohydrates and glycoconjugates. In a selection of all-new chapters, this fully updated volume covers each technique in detail. The book aims to help analysts solve any of the many practical problems they may face in tackling the analysis of carbohydrates. In addition, it addresses current difficulties that must be resolved in carbohydrate research, thus inspiring further important technological developments to meet these challenges. This is an essential resource for anyone seeking a broad view of the science of carbohydrates and separation techniques. - Covers the basic principles of modern liquid phase separation techniques, along with their applications - Compiles up-to-date information on the field of carbohydrate analysis, along with updates on separation science - Focuses on problems currently faced in carbohydrate analysis and the solutions necessary for further progress
Handbook of Modern Pharmaceutical Analysis, Second Edition, synthesizes the complex research and recent changes in the field, while covering the techniques and technology required for today's laboratories. The work integrates strategy, case studies, methodologies, and implications of new regulatory structures, providing complete coverage of quality assurance from the point of discovery to the point of use. - Treats pharmaceutical analysis (PA) as an integral partner to the drug development process rather than as a service to it - Covers method development, validation, selection, testing, modeling, and simulation studies combined with advanced exploration of assays, impurity testing, biomolecules, and chiral separations - Features detailed coverage of QA, ethics, and regulatory guidance (quality by design, good manufacturing practice), as well as high-tech methodologies and technologies from "lab-on-a-chip" to LC-MS, LC-NMR, and LC-NMR-MS
Analytical Methods for Pesticides and Plant Growth Regulators, Volume XIV: Modern Analytical Techniques covers an updated treatment of the most frequently used techniques for pesticide analysis, i.e., thin-layer chromatography, gas chromatography (packed and capillary columns), high-performance liquid chromatography, and mass spectrometry. People involved in the analysis of pesticides will find the book useful.
Completely revised and updated, Chemical Analysis: Second Edition is an essential introduction to a wide range of analytical techniques and instruments. Assuming little in the way of prior knowledge, this text carefully guides the reader through the more widely used and important techniques, whilst avoiding excessive technical detail. Provides a thorough introduction to a wide range of the most important and widely used instrumental techniques Maintains a careful balance between depth and breadth of coverage Includes examples, problems and their solutions Includes coverage of latest developments including supercritical fluid chromatography and capillary electrophoresis
Modern Environmental Analysis Techniques for Pollutants presents established environmental analysis methods, rapidly emerging technologies, and potential future research directions. As methods of environmental analysis move toward lower impact, lower cost, miniaturization, automation, and simplicity, new methods emerge and ultimately improve the accuracy of their analytical results. This book gives in-depth, step-by-step descriptions of a variety of techniques, including methods used in sampling, field sample handling, sample preparation, quantification, and statistical evaluation. Modern Environmental Analysis Techniques for Pollutants aims to deliver a comprehensive and easy-to-read text for students and researchers in the environmental analysis arena and to provide essential information to consultants and regulators about analytical and quality control procedures helpful in their evaluation and decision-making procedures. - Bridges the gap in current literature on analytical chemistry techniques and their application to environmental analysis - Covers the use of nanomaterials in environmental analysis, as well as the monitoring and analysis of nanomaterials in the environment - Looks to the past, present and future of environmental analysis, with chapters on historical background, established and emerging techniques and instrumentation, and predictions
Separation science plays a critical role in maintaining our standard of living and quality of life. Many industrial processes and general necessities such as chemicals, medicines, clean water, safe food, and energy sources rely on chemical separations. However, the process of chemical separations is often overlooked during product development and this has led to inefficiency, unnecessary waste, and lack of consensus among chemists and engineers. A reevaluation of system design, establishment of standards, and an increased focus on the advancement of separation science are imperative in supporting increased efficiency, continued U.S. manufacturing competitiveness, and public welfare. A Research Agenda for Transforming Separation Science explores developments in the industry since the 1987 National Academies report, Separation and Purification: Critical Needs and Opportunities. Many needs stated in the original report remain today, in addition to a variety of new challenges due to improved detection limits, advances in medicine, and a recent emphasis on sustainability and environmental stewardship. This report examines emerging chemical separation technologies, relevant developments in intersecting disciplines, and gaps in existing research, and provides recommendations for the application of improved separation science technologies and processes. This research serves as a foundation for transforming separation science, which could reduce global energy use, improve human and environmental health, and advance more efficient practices in various industries.
In the dynamic field of pharmaceutical sciences, analytical techniques play an indispensable role. The precision and reliability of these methods are crucial for ensuring the quality, safety, and efficacy of pharmaceutical products throughout their development, manufacturing, and regulatory approval stages. Recent decades have seen significant advancements in analytical instrumentation, methodologies, and data analysis, leading to a transformative shift in pharmaceutical analytics. This book is intended as a comprehensive guide to modern pharmaceutical analytical techniques, aiming to bridge the gap between theoretical knowledge and practical application in the evolving pharmaceutical industry. It serves as a valuable resource for students, researchers, and professionals involved in pharmaceutical analysis, providing a systematic overview of the latest analytical tools and strategies used in drug discovery, development, and quality control. Each chapter is carefully designed to offer detailed insights into the theoretical foundations, practical considerations, and recent advancements relevant to each analytical technique. The content is enriched with illustrative examples, case studies, and critical discussions. Special attention is given to emerging trends, such as nanotechnology-enabled analytical platforms, microfluidic-based assays, and in silico predictive modeling, highlighting the transformative potential of these cutting-edge technologies in pharmaceutical analytics. We hope this book will foster interdisciplinary collaboration, drive innovation, and promote best practices in pharmaceutical analytical sciences. We express our sincere gratitude to the contributors for their scholarly efforts and to the readers for their interest and engagement in this work.
Plants are important source of lead molecules for drug discovery. These lead molecules serve as starting materials for laboratory synthesis of drug as well a model for production of biologically active compounds. Phytochemical processing of raw plant materials is essentially required to optimize the concentration of known constituents and also to maintain their activities. Extraction techniques and analytical techniques have played critical roles in phytochemical processing of raw materials. Extraction technologies from conventional extraction to green extraction as well as analytical techniques from single technique to hyphenated/coupled techniques most frequently used in phytochemistry laboratories are covered in the book.
The aim of this book is to present a range of analytical methods that can be used in formulation design and development and focus on how these systems can be applied to understand formulation components and the dosage form these build. To effectively design and exploit drug delivery systems, the underlying characteristic of a dosage form must be understood--from the characteristics of the individual formulation components, to how they act and interact within the formulation, and finally, to how this formulation responds in different biological environments. To achieve this, there is a wide range of analytical techniques that can be adopted to understand and elucidate the mechanics of drug delivery and drug formulation. Such methods include e.g. spectroscopic analysis, diffractometric analysis, thermal investigations, surface analytical techniques, particle size analysis, rheological techniques, methods to characterize drug stability and release, and biological analysis in appropriate cell and animal models. Whilst each of these methods can encompass a full research area in their own right, formulation scientists must be able to effectively apply these methods to the delivery system they are considering. The information in this book is designed to support researchers in their ability to fully characterize and analyze a range of delivery systems, using an appropriate selection of analytical techniques. Due to its consideration of regulatory approval, this book will also be suitable for industrial researchers both at early stage up to pre-clinical research.