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The authors provide new insights into the theoretical and applied aspects of metal electrodeposition. The theory largely focuses on the electrochemistry of metals. Details on the practice discuss the selection and use of metal coatings, the technology of deposition of metals and alloys, including individual peculiarities, properties and structure of coatings, control and investigations. This book aims to acquaint advanced students and researchers with recent advances in electrodeposition while also being an excellent reference for the practical electrodeposition of metals and alloys.
Electrochemistry is the branch of chemistry that deals with the chemical action of electricity and the production of electricity by chemical reactions. In a world short of energy sources yet long on energy use, electrochemistry is a critical component of the mix necessary to keep the world economies growing. Electrochemistry is involved with such important applications as batteries, fuel cells, corrosion studies, hydrogen energy conversion, and bioelectricity. Research on electrolytes, cells, and electrodes is within the scope of this old but extremely dynamic field. This book details advances in metal electrodeposition.
Excellent teaching and resource material . . . it is concise, coherently structured, and easy to read . . . highly recommended for students, engineers, and researchers in all related fields." -Corrosion on the First Edition of Fundamentals of Electrochemical Deposition From computer hardware to automobiles, medical diagnostics to aerospace, electrochemical deposition plays a crucial role in an array of key industries. Fundamentals of Electrochemical Deposition, Second Edition is a comprehensive introduction to one of today's most exciting and rapidly evolving fields of practical knowledge. The most authoritative introduction to the field so far, the book presents detailed coverage of the full range of electrochemical deposition processes and technologies, including: * Metal-solution interphase * Charge transfer across an interphase * Formation of an equilibrium electrode potential * Nucleation and growth of thin films * Kinetics and mechanisms of electrodeposition * Electroless deposition * In situ characterization of deposition processes * Structure and properties of deposits * Multilayered and composite thin films * Interdiffusion in thin film * Applications in the semiconductor industry and the field of medicine This new edition updates the prior edition to address the new developments in the science and its applications, with new chapters on innovative applications of electrochemical deposition in semiconductor technology, magnetism and microelectronics, and medical instrumentation. Added coverage includes such topics as binding energy, nanoclusters, atomic force, and scanning tunneling microscopy.Example problems at the end of chapters and other features clarify and improve understanding of the material. Written by an author team with extensive experience in both industry and academe, this reference and text provides a well-rounded introduction to the field for students, as well as a means for professional chemists, engineers, and technicians to expand and sharpen their skills in using the technology.
Gold and noble metals have been attractive to humans from ancient times because of their beautiful features. In modern society, noble metals, especially gold, play important roles as components in electronic devices because of their high electrical conductivity, chemical stability, and density. In the field of MEMS devices, the demand for continuous miniaturization and sensitivity enhancement is always high. Especially for MEMS accelerometers, sensitivity is affected by Brownian noise, and components with sufficient mass are needed to suppress this noise. Therefore, it is difficult to reduce the dimensions of components to allow further miniaturization of the device. This book presents recent progress in noble metal electrodeposition and applications of gold-based materials in the realization of highly sensitive CMOS-MEMS accelerometers.
This symposium provided a forum for current work on the electrodeposition and characterization of functional coatings and nanostructures. Central issues include the control of size and architecture and the ample choices and demands of substrate and deposited materials. The focus materials of this symposium were semiconductors, oxides and composites with e.g. ceramic nanoparticles or nanotubes.
This new volume of Modern Aspects of Electrochemistry reviews different methods for the production of metal powders including mechanical, chemical and electrochemical powders. Electrochemically produced metal powders are of high purity and they are extremely active during sintering. These powders find a wide-range of applications in automotive, aerospace, energy device and electronics industries.
Nanocomposite coatings have various properties that can be utilized for corrosion protection and tribological improvements. Synthesis of the nanocomposite coatings using an electrodeposition method allows unique control of the experimental parameters. By fine tuning the experimental parameters, various compositions and properties can be obtained for the nanocomposite coatings. This book covers some of the electrochemical methods used for nanocomposite coating deposition as well as discusses in detail examples of several nanocomposite coating. The corrosion and tribological performance of the nanocomposite coatings are also covered and some nanocomposite coatings are discussed for specific technological areas, such as fuel cells and microelectronics.
Solution Methods for Metal Oxide Nanostructures reviews solution processes that are used for synthesizing 1D, 2D and 3D metal oxide nanostructures in either thin film or in powder form for various applications. Wet-chemical synthesis methods deal with chemical reactions in the solution phase using precursors at proper experimental conditions. Wet-chemical synthesis routes offer a high degree of controllability and reproducibility for 2D nanomaterial fabrication. Solvothermal synthesis, template synthesis, self-assembly, oriented attachment, hot-injection, and interface-mediated synthesis are the main wet-chemical synthesis routes for 2D nanomaterials. Solution Methods for Metal Oxide Nanostructures also addresses the thin film deposition metal oxides nanostructures, which plays a very important role in many areas of chemistry, physics and materials science.Each chapter includes information on a key solution method and their application in the design of metal oxide nanostructured materials with optimized properties for important applications. The pros and cons of the solution method and their significance and future scope is also discussed in each chapter. Readers are provided with the fundamental understanding of the key concepts of solution synthesis methods for fabricating materials and the information needed to help them select the appropriate method for the desired application. - Reviews the most relevant wet chemical solution methods for metal oxide nanostructures, including sol-gel, solvothermal, hydrothermal, co-precipitation methods, and more - Addresses thin film deposition techniques for metal oxide nanostructures, such as spray-pyrolysis, electrodeposition, spin coating and self-assembly - Discusses the pros and cons of each solution method and its significance and future opportunities
This book is a hard bound edition of a special issue (vol. 48/20-22) of the journal Electrochimica Acta. It summarizes the highlights of the 53rd Annual meeting of the International Society of Electrochemistry and Annual meeting of the GDCh-Fachgruppe Angewandte Elektrochemie. The theme of the conference was Electrochemistry in Molecular and Microscopic dimensions and was based on the role of electrochemistry in the miniaturization of chemical and physical methods. Topics covered are : - development of electrochemistry with microscopic and molecular resolution; - initiation of advances in Electrochemical Microsystem Technologies EMT, and micro/nano-electronics; - development of Electrochemical Materials Science for nanomaterials; - enhancement of miniaturization and sensitivity of electroanalysis, and; - the bridge from electrochemistry to biology and medicine of microscopic and molecular understanding. - Summarizes the highlights of two major electrochemistry meetings. - It includes research papers on the electrochemical processes in micro- and nanotechnology. - Highlights developments and advances in electrochemistry.
This comprehensive handbook covers all fundamentals of electrochemistry for contemporary applications. It provides a rich presentation of related topics of electrochemistry with a clear focus on energy technologies. It covers all aspects of electrochemistry starting with theoretical concepts and basic laws of thermodynamics, non-equilibrium thermodynamics and multiscale modeling. It further gathers the basic experimental methods such as potentiometry, reference electrodes, ion-sensitive electrodes, voltammetry and amperometry. The contents cover subjects related to mass transport, the electric double layer, ohmic losses and experimentation affecting electrochemical reactions. These aspects of electrochemistry are especially examined in view of specific energy technologies including batteries, polymer electrolyte and biological fuel cells, electrochemical capacitors, electrochemical hydrogen production and photoelectrochemistry. Organized in six parts, the overall complexity of electrochemistry is presented and makes this handbook an authoritative reference and definitive source for advanced students, professionals and scientists particularly interested in industrial and energy applications.