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The market leader for the full-year organic laboratory, this manual derives many experiments and procedures from the classic Feiser lab text, giving it an unsurpassed reputation for solid, authoritative content. The Sixth Edition includes new experiments that stress greener chemistry, as well as updated NMR spectra and a Premium Website that includes glassware-specific videos with pre-lab, gradable exercises. Offering a flexible mix of macroscale and microscale options for most experiments, this proven manual emphasizes safety and allows instructors to save on the purchase and disposal of expensive, sometimes hazardous, organic chemicals. Macroscale versions can be used for less costly experiments, allowing students to get experience working with conventionally-sized glassware.
This updated revision offers total coverage of organic laboratory experiments and techniques focusing on modern laboratory instrumentation, a strong emphasis on lab safety, additional concentration on sequential reaction sequences, excellent pre- and post-lab exercises, and multistep experiments which maximize the number of manipulations students perform per lab period. The microscale approach is low in cost, offers ease of doing experiments and uses minimal amounts of chemicals. A number of experiments include instructions for scaling up.
This book contains volume 1 of 2 and describes safety guidelines for academic chemistry laboratories to prevent accidents for college and university students. Contents include: (1) "Your Responsibility for Accident Prevention"; (2) "Guide to Chemical Hazards"; (3) "Recommended Laboratory Techniques"; and (4) "Safety Equipment and Emergency Procedures." Appendices include the Web as a source of safety information and incompatible chemicals.
The well-known and tested organic chemistry laboratory techniques of the two best-selling organic chemistry lab manuals: INTRODUCTION TO ORGANIC LABORATORY TECHNIQUES: A SMALL SCALE APPROACH and INTRODUCTION TO ORGANIC LABORATORY TECHNIQUES: A MICROSCALE APPROACH, 3/e are now assembled in one textbook. Professors can use any experiments alongside MICROSCALE AND MACROSCALE TECHNIQUES IN THE ORGANIC LABORATORY. Experiments can be selected and assembled from the two Pavia organic chemistry lab manuals, from professors' homegrown labs, or even competing texts. The 375 page, hardcover book serves as a reference for all students of organic chemistry. With clearly written prose and accurately drawn diagrams, students can feel confident setting up and running organic labs.
This cutting-edge lab manual takes a multiscale approach, presenting both micro, semi-micro, and macroscale techniques. The manual is easy to navigate with all relevant techniques found as they are needed. Cutting-edge subjects such as HPLC, bioorganic chemistry, multistep synthesis, and more are presented in a clear and engaging fashion.
The market leader for the full-year organic laboratory, this manual derives many experiments and procedures from the classic Feiser lab text, giving it an unsurpassed reputation for solid, authoritative content. The Williamson/Minard/Masters manual's flexible mix of macroscale and microscale options for most experiments allows instructors to save on the purchase and disposal of expensive, sometimes hazardous organic chemicals. Macroscale versions can be used for less costly experiments, giving students experience working with conventionally sized glassware. The Fifth Edition of the manual includes new experiments that stress greener chemistry, revised content in computational chemistry, and more information on laboratory safety procedures. New! Experiments that stress greener chemistry appear throughout the manual and are identified with a green chemistry icon. For example, the use of household bleach is explored as an alternative to the toxic chromium ion as an oxidizing agent for cyclohexanol. New! The laboratory safety chapter now includes material on working with closed systems and laboratory courtesy. New! The chapter on mass spectrometry describes time-of-flight and mass quadrupole analyzers, and includes sections on GC-MS and computer-aided spectral identification as well as ESI and MALDI ionization. New! Bioassay experiments include a bioassay of eugenol isolated from cloves. New! Material is now offered on diffuse reflectance IR analysis, capillary GC, and temperature programming. Revised! The place of organic chemistry labwork has been put in a broader context via reorganization of and revisions to the first fifteen chapters dealing with basic lab methods, computational chemistry, and instrumental methods. Revised! Computational chemistry, which allows students to determine the precise structure of molecules, has been extensively revised to provide extended coverage of ab initio and semi-empirical models and calculations. Revised! The discussions of NMR theory and the interpretation of 1HNMR spectra have been updated. The In this experiment... section appears before selected microscale experiments and presents the overarching objective of the experiment, keeping students from getting bogged down in the details of experimental procedures. For Further Investigation procedures appear in selected experiments. These are optional, additional procedures that can be assigned to further explore the chemical principle being presented. A Cleaning Up section appears at the end of every experiment and instructs students on how to dispose of all the by-products used in the experiment. Other pedagogical features include pre-lab exercises, marginal notes, clear line drawings, and end-of-chapter questions.
This book offers a comprehensive introductory treatment of the organic laboratory techniques for handling glassware and equipment, safety in the laboratory, micro- and miniscale experimental procedures, theory of reactions and techniques, relevant background information, applications and spectroscopy.
Featuring new experiments unique to this lab textbook, as well as new and revised essays and updated techniques, this Sixth Edition provides the up-to-date coverage students need to succeed in their coursework and future careers. From biofuels, green chemistry, and nanotechnology, the book’s experiments, designed to utilize microscale glassware and equipment, demonstrate the relationship between organic chemistry and everyday life, with project-and biological or health science focused experiments. As they move through the book, students will experience traditional organic reactions and syntheses, the isolation of natural products, and molecular modeling. Important Notice: Media content referenced within the product description or the product text may not be available in the ebook version.