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This resource contains over sixty laboratory experiments and is specifically referenced to Chemistry for Changing Times.
Newest techniques for complex investigations based on actual plant and industry data. These Guidelines establish a basis for successful feedback through investigation of process incidents to determine the many causes and to implement changes which will prevent recurrence. It provides a clear definition of the role of incident investigation in overall process safety management, as well as guidelines, concepts, and options. Detailed investigation techniques and how to establish such a system are set out for plant staff, technical professionals, or middle level managers. Primary focus is on incidents with catastrophic potential but the concepts should also be used for investigating environmental incidents, minor injuries, less significant property damage events, or near misses. Also provides an overview of incident investigation principles as implemented by other industries worldwide. The annotated bibliography included makes this practical handbook an invaluable reference source. parag Partial contents : Basic Incident Investigation Techniques Practical Investigation Considerations Multiple Cause Determination Recommendations and Follow-through Formal Reports and Communications Issues Development and Implementation.
This book provides an historical overview of the recent developments in the history of diverse fields within chemistry. It follows on from Recent Developments in the History of Chemistry, a volume published in 1985. Covering chiefly the last 20 years, the primary aim of Chemical History: Reviews of the Recent Literature is to familiarise newcomers to the history of chemistry with some of the more important developments in the field. Starting with a general introduction and look at the early history of chemistry, subsequent chapters go on to investigate the traditional areas of chemistry (physical, organic, inorganic) alongside analytical chemistry, physical organic chemistry, medical chemistry and biochemistry, and instruments and apparatus. Topics such as industrial chemistry and chemistry in national contexts, whilst not featuring as separate chapters, are woven throughout the content. Each chapter is written by experts and is extensively referenced to the international chemical literature. Chemical History: Reviews of the Recent Literature is also ideal for chemists who wish to become familiar with historical aspects of their work. In addition, it will appeal to a wider audience interested in the history of chemistry, as it draws together historical materials that are widely scattered throughout the chemical literature.
A range of alternative mechanisms can usually be postulated for most organic chemical reactions, and identification of the most likely requires detailed investigation. Investigation of Organic Reactions and their Mechanisms will serve as a guide for the trained chemist who needs to characterise an organic chemical reaction and investigate its mechanism, but who is not an expert in physical organic chemistry. Such an investigation will lead to an understanding of which bonds are broken, which are made, and the order in which these processes happen. This information and knowledge of the associated kinetic and thermodynamic parameters are central to the development of safe, efficient, and profitable industrial chemical processes, and to extending the synthetic utility of new chemical reactions in chemical and pharmaceutical manufacturing, and academic environments. Written as a coherent account of the principal methods currently used in mechanistic investigations, at a level accessible to academic researchers and graduate chemists in industry, the book is highly practical in approach. The contributing authors, an international group of expert practitioners of the techniques covered, illustrate their contributions by examples from their own research and from the relevant wider chemical literature. The book covers basic aspects such as product analysis, kinetics, catalysis, and investigation of reactive intermediates. It also includes material on significant recent developments, e.g. computational chemistry, calorimetry, and electrochemistry, in addition to topics of high current industrial relevance, e.g. reactions in multiphase systems, and synthetically useful reactions involving free radicals and catalysis by organometallic compounds.
Chemistry: An Everyday Approach to Chemical Investigation is intended to accompany any mainstream general chemistry course, and consists of 27 experiments that can be completed using only chemicals found in consumer products. The manual is an ideal resource for courses emphasizing green chemistry in which the use of hazardous materials is reduced or eliminated altogether. Many of the experiments requiring simple equipment and glassware can be performed at remote sites providing laboratory experience for use with on-line or long distance learning courses. The advantages of using accessible materials in chemistry laboratory are considerable. Students can reinforce lecture discussions while working with familiar materials. For instructors, assembling the chemicals required for a lab course can be accomplished with limited budgets and without access to a chemical company. Problems with safety and waste disposal are significantly reduced.
This book provides a comprehensive treatment of investing chemical processing incidents. It presents on-the-job information, techniques, and examples that support successful investigations. Issues related to identification and classification of incidents (including near misses), notifications and initial response, assignment of an investigation team, preservation and control of an incident scene, collecting and documenting evidence, interviewing witnesses, determining what happened, identifying root causes, developing recommendations, effectively implementing recommendation, communicating investigation findings, and improving the investigation process are addressed in the third edition. While the focus of the book is investigating process safety incidents the methodologies, tools, and techniques described can also be applied when investigating other types of events such as reliability, quality, occupational health, and safety incidents.