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Requires no prior knowledge of the subject, but is comprehensive and detailed making it useful for both the novice and experienced user of the powder diffraction method. Useful for any scientific or engineering background, where precise structural information is required. Comprehensively describes the state-of-the-art in structure determination from powder diffraction data both theoretically and practically using multiple examples of varying complexity. Pays particular attention to the utilization of Internet resources, especially the well-tested and freely available computer codes designed for processing of powder diffraction data.
Volume 8 of Developments in Applied Spectroscopy presents a collection of selected papers presented at special symposia and other sessions during the 20th Mid-America Symposium on Spectroscopy, held in Chicago, May 12-15, 1969. In general, these papers are those of the symposium type and not papers per taining to a specific research topic that one would expect to find in the journals. The 20th Mid-America Symposium was sponsored by the Chicago Section in cooperation with the Niagara Frontier, Rocky Mountain, St. Louis, and Southeastern Sections of the Society of Applied Spectroscopy, and the Chicago Gas Chromatography Group. Although the Mid-America is still occasionally thought of as a regional meeting, its attendees and authors come from all parts of the United States and Canada. Both theoretical and applied principles were presented in sessions on emission, atomic absorption, x-ray, nuclear particle, Raman and infrared, nuclear magnetic resonance, and electron spin resonance spectroscopy; computer applications; air and water pollution, instrumental applications to biomedicine toxicology; spectra and characterization; matrix isolation and gas chromatography-mass spectrometry. In addition, there were symposia on trace element analyses, silicate analyses, Mossbauer spectroscopy, electron spectroscopy for chemical analyses (ESCA), spectroscopy of materials under high pressure, and reference spectra and retrieval systems. The various chairmen of the Symposium Committee, H. Bedell, Dr. Charles Bell, Dr. Eleanor Berman, Dr. Roy Bible, Sam Booras, James E. Burroughs, Adrian Chisholm, Dr. Paul Day, Tod Engelskirchen, G. A. Ettelt, Dr. L. S.
Thermodynamic and Transport Properties of Organic Salts is concerned with the thermodynamic and transport properties of organic salts, namely, pure salts, mixtures, and solutions. The transport properties of pure molten salts and binary mixtures of molten salts with organic ions are given, along with the transport properties of organic salts in aqueous solutions. This book is divided into three sections and opens with a discussion on the statistical treatment and of computer simulation methods for molten salts as well as their results for pressure-volume-temperature (PVT) data. The PVT data for organic molten salts determined experimentally are considered, and the thermal properties as well as the melting mechanism of pure salts are described. A method by which PVT data at high pressure can be estimated from those at low pressure with sufficiently high accuracy is also outlined. The next section deals with salt mixtures, their phase diagrams, and their transport properties. The final section looks at the transport properties of organic salts in aqueous solutions; thermodynamic quantities of micelle formation; and formation of lyotropic liquid crystals by organic salts. Two appendixes showing the structure of the pure solids and the use of the melts in electrochemical studies are included. This monograph will be a useful resource for organic chemists.
A little over ?ve years have passed since the ?rst edition of this book appeared in print. Seems like an instant but also eternity, especially considering numerous developments in the hardware and software that have made it from the laboratory test beds into the real world of powder diffraction. This prompted a revision, which had to be beyond cosmetic limits. The book was, and remains focused on standard laboratory powder diffractometry. It is still meant to be used as a text for teaching students about the capabilities and limitations of the powder diffraction method. We also hope that it goes beyond a simple text, and therefore, is useful as a reference to practitioners of the technique. The original book had seven long chapters that may have made its use as a text - convenient. So the second edition is broken down into 25 shorter chapters. The ?rst ?fteen are concerned with the fundamentals of powder diffraction, which makes it much more logical, considering a typical 16-week long semester. The last ten ch- ters are concerned with practical examples of structure solution and re?nement, which were preserved from the ?rst edition and expanded by another example – R solving the crystal structure of Tylenol .