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Dynamic Mechanical Analysis (DMA) is a powerful technique for understanding the viscoelastic properties of materials. It has become a powerful tool for chemists, polymer and material scientists, and engineers. Despite this, it often remains underutilized in the modern laboratory. Because of its high sensitivity to the presence of the glass transition, many users limit it to detecting glass transitions that can’t be seen by differential scanning calorimetry (DSC). This book presents a practical and straightforward approach to understanding how DMA works and what it measures. Starting with the concepts of stress and strain, the text takes the reader through stress–strain, creep, and thermomechanical analysis. DMA is discussed as both the instrument and fixtures as well as the techniques for measuring both thermoplastic and thermosetting behavior. This edition offers expanded chapters on these areas as well as frequency scanning and other application areas. To help the reader grasp the material, study questions have also been added. Endnotes have been expanded and updated. Features Reflects the latest DMA research and technical advances Includes case studies to demonstrate the use of DMA over a range of industrial problems Includes numerous references to help those with limited materials engineering background Demonstrates the power of DMA as a laboratory tool for analysis and testing
As plastics are being used more extensively in high-performance markets, it is imperative that designers and engineers understand all aspects of polymer behavior over an extended service life. Dynamic Mechanical Analysis for Plastics Engineering describes practical uses for DMA information. All of the information for 120 families of thermoplastics is based on independent test data conducted exclusively for this product and is not available through any other source. This PDL addition shows how to use the DMA data to predict, at various temperatures, each materials estimated service life and potential for failure. This book explains the correlation between time and temperature-dependence and illustrates how time-dependent responses such as creep and stress relaxation affect the practical utility of different materials. Basic polymer structures are discussed and test results show how these structural details can be detected and understood.
Thermal Analysis of Textiles and Fibers offers systematic and comprehensive coverage of the subject, from the principles of fiber structure and established TA methods, to advanced TA techniques and their application to high-performance fibers and textiles. Thermal analysis is a convenient method for assessing fiber and fabric performance as monitored under end-use relevant conditions. Expertise in this field requires knowledge of both TA methods and of fiber behavior, information that is brought together in this new volume. In recent years, thermal analysis has been applied to a variety of novel and high-performance fibers, such as Kevlar, Vectran, PBI, polyolefins, polypropylene, PAN and PVA, amongst others. TA techniques are also used in fiber identification, characterization and stability testing and may be combined with spectroscopic techniques to yield still more information about fiber properties. - Includes chapters on novel and high-performance fibers that are used in assembling technical textiles - Covers advanced TA methods, such as combined and modulated techniques - Brings together focused information on TA for fibers and textiles that is not otherwise available in a single volume
Challenges in Mechanics of Time-Dependent Materials, Volume 2 of the Proceedings of the 2020 SEM Annual Conference& Exposition on Experimental and Applied Mechanics, the second volume of seven from the Conference, brings together contributions to this important area of research and engineering. The collection presents early findings and case studies on fundamental and applied aspects of Experimental Mechanics, including papers in the following general technical research areas: Characterization Across Length Scales Extreme Environments & Environmental Effects Soft Materials Damage, fatigue and Fracture Inhomogeneities & Interfaces Viscoelasticity Research in Progress
Mechanical and Dynamic Properties of Biocomposites A comprehensive review of the properties of biocomposites and their applications Mechanical and Dynamic Properties of Biocomposites offers a comprehensive overview of the mechanical and dynamic properties of biocomposites and natural fiber-reinforced polymer composites. This essential resource helps with materials selection in the development of products in the fields of automotive and aerospace engineering as well as the construction of structures in civil engineering. With contributions from a panel of experts in the field, the book reviews the mechanical and damping properties of lingo-cellulosic fibers and their composites. The authors highlight the factors that contribute to the improved properties and their advancements in modern industrialization. Besides, the book is designed to (a) introduce the mechanical and damping properties of lingo-cellulosic fibers and their composites, (b) factors that contribute to improvement in properties such as hybridization, chemical treatment of natural fibers, additive or fillers, etc. and (c) the real-time applications with case studies and future prospects. Key features: Presents viable alternatives to conventional composites Examines the environmentally friendly and favorable mechanical properties of biocomposites Reviews the potential applications of biocomposites in the fields of automotive, mechanical and civil engineering Brings together in one comprehensive resource information found scattered across the professional literature Written for materials scientists, polymer chemists, chemists in industry, civil engineers, construction engineers, and engineering scientists in industry, Mechanical and Dynamic Properties of BIocomposites offers a compreshensive review of the properties and applications of biocomposites.
Clay–Polymer Nanocomposites is a complete summary of the existing knowledge on this topic, from the basic concepts of synthesis and design to their applications in timely topics such as high-performance composites, environment, and energy issues. This book covers many aspects of synthesis such as in- situ polymerization within the interlamellar spacing of the clays or by reaction of pristine or pre-modified clays with reactive polymers and prepolymers. Indeed, nanocomposites can be prepared at industrial scale by melt mixing. Regardless the synthesis method, much is said in this book about the importance of theclay pre-modification step, which is demonstrated to be effective, on many occasions, in obtaining exfoliated nanocomposites. Clay–Polymer Nanocomposites reports the background to numerous characterization methods including solid state NMR, neutron scattering, diffraction and vibrational techniques as well as surface analytical methods, namely XPS, inverse gas chromatography and nitrogen adsorption to probe surface composition, wetting and textural/structural properties. Although not described in dedicated chapters, numerous X-ray diffraction patterns of clay–polymer nanocomposites and reference materials are displayed to account for the effects of intercalation and exfoliations of layered aluminosilicates. Finally, multiscale molecular simulation protocols are presenting for predicting morphologies and properties of nanostructured polymer systems with industrial relevance. As far as applications are concerned, Clay–Polymer Nanocomposites examines structural composites such as clay–epoxy and clay–biopolymers, the use of clay–polymer nanocomposites as reactive nanocomposite fillers, catalytic clay-(conductive) polymers and similar nanocomposites for the uptake of hazardous compounds or for controlled drug release, antibacterial applications, energy storage, and more. - The most comprehensive coverage of the state of the art in clay–polymer nanocomposites, from synthesis and design to opportunities and applications - Covers the various methods of characterization of clay–polymer nanocomposites - including spectroscopy, thermal analyses, and X-ray diffraction - Includes a discussion of a range of application areas, including biomedicine, energy storage, biofouling resistance, and more
Dynamic mechanical analysis (DMA) has left the domain of the rheologist and has become a prevalent tool in the analytical laboratory. However, information on the use of this important tool is still scattered among a range of books and articles. Novices in the field have to dig through thermal analysis, rheology, and materials texts just to find the
This volume offers a comprehensive guide on the theory and practice of amorphous solid dispersions (ASD) for handling challenges associated with poorly soluble drugs. In twenty-three inclusive chapters, the book examines thermodynamics and kinetics of the amorphous state and amorphous solid dispersions, ASD technologies, excipients for stabilizing amorphous solid dispersions such as polymers, and ASD manufacturing technologies, including spray drying, hot melt extrusion, fluid bed layering and solvent-controlled micro-precipitation technology (MBP). Each technology is illustrated by specific case studies. In addition, dedicated sections cover analytical tools and technologies for characterization of amorphous solid dispersions, the prediction of long-term stability, and the development of suitable dissolution methods and regulatory aspects. The book also highlights future technologies on the horizon, such as supercritical fluid processing, mesoporous silica, KinetiSol®, and the use of non-salt-forming organic acids and amino acids for the stabilization of amorphous systems. Amorphous Solid Dispersions: Theory and Practice is a valuable reference to pharmaceutical scientists interested in developing bioavailable and therapeutically effective formulations of poorly soluble molecules in order to advance these technologies and develop better medicines for the future.
This book disseminates recent research, theories, and practices relevant to the areas of surface engineering and the processing of materials for functional applications in the aerospace, automobile, and biomedical industries. The book focuses on the hidden technologies and advanced manufacturing methods that may not be standardized by research institutions but are greatly beneficial to material and manufacturing industrial engineers in many ways. It details projects, research activities, and innovations in a global platform to strengthen the knowledge of the concerned community. The book covers surface engineering including coating, deposition, cladding, nanotechnology, surface finishing, precision machining, processing, and emerging advanced manufacturing technologies to enhance the performance of materials in terms of corrosion, wear, and fatigue. The book captures the emerging areas of materials science and advanced manufacturing engineering and presents recent trends in research for researchers, field engineers, and academic professionals.
Dynamic Response of Linear Mechanical Systems: Modeling, Analysis and Simulation can be utilized for a variety of courses, including junior and senior-level vibration and linear mechanical analysis courses. The author connects, by means of a rigorous, yet intuitive approach, the theory of vibration with the more general theory of systems. The book features: A seven-step modeling technique that helps structure the rather unstructured process of mechanical-system modeling A system-theoretic approach to deriving the time response of the linear mathematical models of mechanical systems The modal analysis and the time response of two-degree-of-freedom systems—the first step on the long way to the more elaborate study of multi-degree-of-freedom systems—using the Mohr circle Simple, yet powerful simulation algorithms that exploit the linearity of the system for both single- and multi-degree-of-freedom systems Examples and exercises that rely on modern computational toolboxes for both numerical and symbolic computations as well as a Solutions Manual for instructors, with complete solutions of a sample of end-of-chapter exercises Chapters 3 and 7, on simulation, include in each “Exercises” section a set of miniprojects that require code-writing to implement the algorithms developed in these chapters