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This book provides notes for basic laboratory experiments in qualitative analysis of cations. The book introduces readers to basic methods and laboratory safety. Subsequent chapters cover six groups of cations. Each chapter explains important details that are required to understand how a particular analytical method works for detecting cations in samples, starting from sedimentation and ending with the identification. Key Features: - Simple, reader friendly format - introductory notes and summary - Covers several groups of metals - Appendix for handy reference with tables and references This is a useful textbook for early chemistry students and teachers as it equips the readers with sufficient information required to analyze chemical samples and deduce the presence of specific cations as part of laboratory coursework.
Chemistry: Inorganic Qualitative Analysis in the Laboratory is a textbook dealing with qualitative analysis in the laboratory, as well as with the process of anion and cation analysis. The book presents an overview of the subject of inorganic qualitative analysis, including as the equipment, reagents, and procedures that are going to be used in the laboratory. Preliminary experiments include the classification of precipitates, handling precipitates, separation techniques, flame tests, Brown ring test, solvent extraction. The text also describes in detail how to prepare the experiment for anion and cation analysis such as testing for water solubility in a solid sample or the sodium carbonate treatment of a water-soluble sample. The book also explains the qualitative analysis for anions in preliminary and specific tests. In the qualitative analysis for cations, the student follows different procedures for Cation Groups I, II, III, IV or V. For example, the ions of Cation Group V cannot be precipitated by any Cation Groups I-IV reagents, nor by any single group reagent. The textbook is suitable for both chemistry teachers and freshmen students.
In revising the text opportunity has been taken to introduce SI units throughout. An Appendix has been included which contains tables of SI units and a table of conversion factors for use when consulting data in non-SI units. Chapter 19 now includes experiments demon strating the use of ion-exchange and solid-liquid chromatography_ Exercises involving colorimetry have been included in Chapter 17. These techniques are introduced as part of a complementary exercise where their relevance is seen as part of a complete piece of work. Minor improvements have been made to some of the experimental procedures and we are grateful to those who have made helpful suggestions in this respect. G. PASS H. SUTCLIFFE iii Preface to the First Edition The student of inorganic chemistry is fortunate in having a wide choice of textbooks covering the descriptive and theoretical aspects of the sUbject. There is no comparable choice of textbooks covering practical inorganic chemistry. Moreover, there is a tendency for many students to draw an unfortunate distinction between chemistry taught in the lecture room, and laboratory work. Consideration of these points prompted the preparation of this book, in which we have attempted to emphasize the relationship between theory and practice.
Many years have passed since the last edition of the present book was published. The discovery during this period of many new reagents has resulted in a vast accumulation of data on their application and made this completely revised edition necessary.Numerous new tests and various new chapters have been added. Chapters 3,4 and 5 of the fifth edition have been combined into one chapter, which is divided into sections devoted to the elements. These sections are arranged in alphabetical order to make for easier location of information on a given element. To further improve the usefulness of the volume, a reference list has been provided for each sub-section followed by a biography of the appropriate quantitative methods.