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This book provides up-to-date discussion of modern polarographic methods, with examples and experimental details. It is designed for the practicing analyst and a factor in bringing the reincarnated area of analytical chemistry into a new and healthy maturity.
Lists citations with abstracts for aerospace related reports obtained from world wide sources and announces documents that have recently been entered into the NASA Scientific and Technical Information Database.
It is now time for a comprehensive treatise to look at the whole field of electrochemistry. The present treatise was conceived in 1974, and the earliest invitations to authors for contributions were made in 1975. The completion of the early volumes has been delayed by various factors. There has been no attempt to make each article emphasize the most recent situation at the expense of an overall statement of the modern view. This treatise is not a collection of articles from Recent Advances in Electrochemistry or Modern Aspects of Electrochemistry. It is an attempt at making a mature statement about the present position in the vast area of what is best looked at as a new interdisciplinary field. Texas A & M University J. O'M. Bockris University of Ottawa B. E. Conway Case Western Reserve University Ernest Yeager Texas A & M University Ralph E. White Preface to Volume 8 Experimental methods in electrochemistry are becoming more diverse. This volume describes many of the new techniques that are being used as well as some of the well-established techniques. It begins with two chapters (1 and 2) on electronic instrumentation and methods for utilization of microcomputers for experimental data acquisition and reduction. Next, two chapters (3 and 4) on classical methods of electrochemical analysis are presented: ion selective electrodes and polarography.
Introduction1. CONDUCTOMETRYElectrolytic ConductanceOhm’s LawSpecific ConductanceEquivalent ConductanceMolar ConductanceDetermination of Electrolytic ConductanceTypes of Conductivity CellsConductivity MeasurementsImmersed-Electrode MeasurementsElectrodeless MeasurementsApplications of Conductivity MeasurementsDetermination of Ionic Product of Water (KW)Determination of Solubility of Sparingly Soluble SaltsConductometric TitrationsDetermination of Purity of WaterConcentration DeterminationIon ChromatographyProblemsReferences2. POTENTIOMETRYPrincipleInstrumentationReference ElectrodesIndicator ElectrodesAnalytical InformationAdvantagesApplicationsPotentiometric TitrationsOther ApplicationsProblemsReferences3. VOLTAMMETRYPolarographyDc Polarography (Conventional Polarography)PrincipleFaradaic and Non-Faradaic ProcessesFaradaic CurrentNon-Faradaic CurrentPolarographic WaveCharging CurrentMass TransportLimiting CurrentsPolarographic MaximaInstrumentationPotentiostatElectrochemical CellTwo-electrode PolarographThree-electrode PolarographInert AtmosphereQuantitative TechniquesWave Height–Concentration PlotsInternal Standard (Pilot Ion) MethodMethod of Standard AdditionPulse PolarographyBasic PrincipleNormal Pulse PolarographyDifferential Pulse PolarographyPulse Voltammetry at Stationary ElectrodeApplicationsFundamental Harmonic AC PolarographyFaradaic Electrode ProcessesChronopotentiometryLinear Sweep Voltammetry and Related TechniquesTheory for Faradaic ProcessesCoupled Chemical ReactionsStripping VoltammetryAnodic Stripping VoltammetryElectrodesTheory and TechniquesCathodic Stripping VoltammetryAdsorptive Stripping VoltammetryProblemsReferences4. AMPEROMETRYPrincipleInstrumentationAmperometric Detection and BiosensorsAmperometric TitrationsTitrations with DMETitrations with Rotating Pt ElectrodeBiamperometric TitrationsAdvantages of Amperometric TitrationsApplicationsProblemsReferences5. COULOMETRYControlled Potential MethodsCoulometric MeasurementsControlled Current MethodsCoulometric MeasurementsApplications
Because of its simplicity of use and quantitative results, Scanning Electrochemical Microscopy (SECM) has become an indispensable tool for the study of surface reactivity. The fast expansion of the SECM field over several years has been fueled by the introduction of new probes, commercially available instrumentation, and new practical applications. Scanning Electrochemical Microscopy, Third Edition offers essential background and in-depth overviews of specific applications in self-contained chapters. The vitality and growing popularity of SECM over the past 30+ years have largely been determined by its versatility and capability to remain useful in the changing scientific and technological environments. New applications reported during the last decade reflect significant current activity in biomedical and energy-related research. This thoroughly updated edition provides up-to-date comprehensive reviews of different aspects of SECM. New chapters by renowned professionals in the field cover recent advances in different areas of SECM including nanoSECM, surface reactions and films, batteries, and fuel cells. Expanded coverage of electrocatalysis and surface interrogation as well as photoelectrochemistry and photoelectrocatalysis are also provided. Useful for a broad range of interdisciplinary research—from biological systems to nanopatterning—this book is invaluable to all interested in learning and applying SECM.
It is now time for a comprehensive treatise to look at the whole field of electrochemistry. The present treatise was conceived in 1974, and the earliest invitations to authors for contributions were made in 1975. The completion of the early volumes has been delayed by various factors. There has been no attempt to make each article emphasize the most recent situation at the expense of an overall statement of the modern view. This treatise is not a collection of articles from Recent Advances in Electrochemistry or Modern Aspects of Electrochemistry. It is an attempt at making a mature statement about the present position in the vast area of what is best looked at as a new interdisciplinary field. Texas A & M University J. O'M. Bockris University of Ottawa B. E. Conway Case Western Reserve University Ernest Yeager Texas A & M University Ralph E. White Preface to Volume 8 Experimental methods in electrochemistry are becoming more diverse. This volume describes many of the new techniques that are being used as well as some of the well-established techniques. It begins with two chapters (1 and 2) on electronic instrumentation and methods for utilization of microcomputers for experimental data acquisition and reduction. Next, two chapters (3 and 4) on classical methods of electrochemical analysis are presented: ion selective electrodes and polarography.
This comprehensive presentation of the integral equation method as applied to electro-analytical experiments is suitable for electrochemists, mathematicians and industrial chemists. The discussion focuses on how integral equations can be derived for various kinds of electroanalytical models. The book begins with models independent of spatial coordinates, goes on to address models in one dimensional space geometry and ends with models dependent on two spatial coordinates. Bieniasz considers both semi-infinite and finite spatial domains as well as ways to deal with diffusion, convection, homogeneous reactions, adsorbed reactants and ohmic drops. Bieniasz also discusses mathematical characteristics of the integral equations in the wider context of integral equations known in mathematics. Part of the book is devoted to the solution methodology for the integral equations. As analytical solutions are rarely possible, attention is paid mostly to numerical methods and relevant software. This book includes examples taken from the literature and a thorough literature overview with emphasis on crucial aspects of the integral equation methodology.