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A novel countercurrent liquid-liquid extractor is presented and illustrated with applications. The apparatus consists essentially of an assembly of mixer-settlers, feeders, reservoirs, and flow lines that are made of glass or other chemical resistant materials. The applicability of the extractor is illustrated by extractions involving zirconium and hafnium, and niobium and tantalum.
Liquid Phase Extraction thoroughly presents both existing and new techniques in liquid phase extraction. It not only provides all information laboratory scientists need for choosing and utilizing suitable sample preparation procedures for any kind of sample, but also showcases the contemporary uses of sample preparation techniques in the most important industrial and academic project environments, including countercurrent chromatography, pressurized-liquid extraction, single-drop Microextraction, and more. Written by recognized experts in their respective fields, it serves as a one-stop reference for those who need to know which technique to choose for liquid phase extraction. Used in conjunction with a similar release, Solid Phase Extraction, it allows users to master this crucial aspect of sample preparation. Defines the current state-of-the-art in extraction techniques and the methods and procedures for implementing them in laboratory practice Includes extensive referencing that facilitates the identification of key information Aimed at both entry-level scientists and those who want to explore new techniques and methods
Recent Advances in Liquid-liquid Extraction focuses on the applications of liquid extraction. The selection first discusses solvent extraction. Concerns include organic and inorganic separations, mass transfer process, solvent extraction economics, and coalescence in liquid-liquid systems. The book focuses on the chemistry of solvent extraction. Extraction by acidic organophosphorus compounds; extraction by phosphorus-bonded oxygen-donor solvents; extraction by high-molecular weight amines; and synergistic extraction are elaborated. The book also focuses on industrial organic processes; industrial contacting equipment; response characteristics and control of extraction processes; and calculation of contactors with longitudinal mixing. The selection presents the study of longitudinal mixing in liquid-liquid contactors. Rotating disc contactors, packed columns, vibrating plate extractors, and Oldshue-Rushton columns are described. The text also discusses heat transfer by direct liquid-liquid contact and the coalescence of liquid droplets and liquid dispersion. The selection is a vital source of data for readers interested in liquid extraction.
This work presents an up-to-date account of some of the fundamental aspects of liquid-liquid extraction technology together with an account of extraction processes in a number of important industries. The work is divided into two parts. Volume 1 is concerned with the thermodynamics of phase equilibria; mass transfer in liquid-liquid systems, including the complicating role of interfacial turbulence; behavior of liquid-liquid dispersions; and the selection and design of countercurrent contactors for particular applications. Volume 2 gives an account of the process chemistry and associated extraction operations in a number of industries of current interest. New extraction techniques have been developed in recent years for specific applications and these are illustrated with reference to the hydrometallurgical, nuclear, pharmaceutical and food industries.
Get Cutting-Edge Coverage of All Chemical Engineering Topics— from Fundamentals to the Latest Computer Applications First published in 1934, Perry's Chemical Engineers' Handbook has equipped generations of engineers and chemists with an expert source of chemical engineering information and data. Now updated to reflect the latest technology and processes of the new millennium, the Eighth Edition of this classic guide provides unsurpassed coverage of every aspect of chemical engineering-from fundamental principles to chemical processes and equipment to new computer applications. Filled with over 700 detailed illustrations, the Eighth Edition of Perry's Chemcial Engineering Handbook features: Comprehensive tables and charts for unit conversion A greatly expanded section on physical and chemical data New to this edition: the latest advances in distillation, liquid-liquid extraction, reactor modeling, biological processes, biochemical and membrane separation processes, and chemical plant safety practices with accident case histories Inside This Updated Chemical Engineering Guide - Conversion Factors and Mathematical Symbols • Physical and Chemical Data • Mathematics • Thermodynamics • Heat and Mass Transfer • Fluid and Particle Dynamics Reaction Kinetics • Process Control • Process Economics • Transport and Storage of Fluids • Heat Transfer Equipment • Psychrometry, Evaporative Cooling, and Solids Drying • Distillation • Gas Absorption and Gas-Liquid System Design • Liquid-Liquid Extraction Operations and Equipment • Adsorption and Ion Exchange • Gas-Solid Operations and Equipment • Liquid-Solid Operations and Equipment • Solid-Solid Operations and Equipment • Size Reduction and Size Enlargement • Handling of Bulk Solids and Packaging of Solids and Liquids • Alternative Separation Processes • And Many Other Topics!
Liquid-Liquid and Solid-Liquid Extractors, part of the Industrial Equipment for Chemical Engineering set, presents a concise and easy-to-use book on the calculation of differential liquid–liquid extraction, an investigation of equilibrium and material transfer between a fluid and a divided solid, and the fundamentals of liquid–solid extraction, among other strategies. The author also provides methods needed for the understanding the machinery used in applied thermodynamics in the hopes of encouraging students and engineers to construct the programs they need. Chapters are complemented with appendices which provide additional information and associated references. Presents reliable and simple methods of extraction and partitioning Provides a clear analysis on the topic of liquid-liquid and solid-liquid extraction Includes practical applications that readers can implement and study