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Teaches students the basic techniques and equipment of the organic chemistry lab — the updated new edition of the popular hands-on guide. The Organic Chem Lab Survival Manual helps students understand the basic techniques, essential safety protocols, and the standard instrumentation necessary for success in the laboratory. Author James W. Zubrick has been assisting students navigate organic chemistry labs for more than three decades, explaining how to set up the laboratory, make accurate measurements, and perform safe and meaningful experiments. This practical guide covers every essential area of lab knowledge, from keeping detailed notes and interpreting handbooks to using equipment for chromatography and infrared spectroscopy. Now in its eleventh edition, this guide has been thoroughly updated to cover current laboratory practices, instruments, and techniques. Focusing primarily on macroscale equipment and experiments, chapters cover microscale jointware, drying agents, recrystallization, distillation, nuclear magnetic resonance, and much more. This popular textbook: Familiarizes students with common lab instruments Provides guidance on basic lab skills and procedures Includes easy-to-follow diagrams and illustrations of lab experiments Features practical exercises and activities at the end of each chapter Provides real-world examples of lab notes and instrument manuals The Organic Chem Lab Survival Manual: A Student’s Guide to Techniques, 11th Edition is an essential resource for students new to the laboratory environment, as well as those more experienced seeking to refresh their knowledge.
A Clear And Reliable Guide To Students Of Practical Organic Chemistry At The Undergraduate And Postgraduate Levels. This Edition S Special Emphasis Is On Semi Micro Methods And Modern Techniques And Reactions.
Now in its fifth edition, the book has been updated to include more detailed descriptions of new or more commonly used techniques since the last edition as well as remove those that are no longer used, procedures which have been developed recently, ionization constants (pKa values) and also more detail about the trivial names of compounds.In addition to having two general chapters on purification procedures, this book provides details of the physical properties and purification procedures, taken from literature, of a very extensive number of organic, inorganic and biochemical compounds which are commercially available. This is the only complete source that covers the purification of laboratory chemicals that are commercially available in this manner and format.* Complete update of this valuable, well-known reference* Provides purification procedures of commercially available chemicals and biochemicals* Includes an extremely useful compilation of ionisation constants
Diagnose and Troubleshoot Problems in Chemical Process Equipment with This Updated Classic! Chemical engineers and plant operators can rely on the Third Edition of A Working Guide to Process Equipment for the latest diagnostic tips, practical examples, and detailed illustrations for pinpointing trouble and correcting problems in chemical process equipment. This updated classic contains new chapters on Control Valves, Cooling Towers, Waste Heat Boilers, Catalytic Effects, Fundamental Concepts of Process Equipment, and Process Safety. Filled with worked-out calculations, the book examines everything from trays, reboilers, instruments, air coolers, and steam turbines...to fired heaters, refrigeration systems, centrifugal pumps, separators, and compressors. The authors simplify complex issues and explain the technical issues needed to solve all kinds of equipment problems. Comprehensive and clear, the Third Edition of A Working Guide to Process Equipment features: Guidance on diagnosing and troubleshooting process equipment problems Explanations of how theory applies to real-world equipment operations Many useful tips, examples, illustrations, and worked-out calculations New to this edition: Control Valves, Cooling Towers, Waste Heat Boilers, Catalytic Effects, and Process Safety Inside this Renowned Guide to Solving Process Equipment Problems • Trays • Tower Pressure • Distillation Towers • Reboilers • Instruments • Packed Towers • Steam and Condensate Systems • Bubble Point and Dew Point • Steam Strippers • Draw-Off Nozzle Hydraulics • Pumparounds and Tower Heat Flows • Condensers and Tower Pressure Control • Air Coolers • Deaerators and Steam Systems • Vacuum Systems • Steam Turbines • Surface Condensers • Shell-and-Tube Heat Exchangers • Fire Heaters • Refrigeration Systems • Centrifugal Pumps • Separators • Compressors • Safety • Corrosion • Fluid Flow • Computer Modeling and Control • Field Troubleshooting Process Problems