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Inelastic neutron scattering (INS) is a spectroscopic technique in which neutrons are used to probe the dynamics of atoms and molecules in solids and liquids. This book is the first, since the late 1960s, to cover the principles and applications of INS as a vibrational-spectroscopic technique. It provides a hands-on account of the use of INS, concentrating on how neutron vibrational spectroscopy can be employed to obtain chemical information on a range of materials that are of interest to chemists, biologists, materials scientists, surface scientists and catalyst researchers. This is an accessible and comprehensive single-volume primary text and reference source.
- Up-to-date account of the principles and practice of inelastic and spectroscopic methods available at neutron and synchrotron sources - Multi-technique approach set around a central theme, rather than a monograph on one technique - Emphasis on the complementarity of neutron spectroscopy and X-ray spectroscopy which are usually treated in separate books
This volume analyzes both the theoretical and experimental aspects of neutron spectroscopy of solids, whereby complex crystals may be analyzed in relation to the theories of symmetry and neutron scattering near a structural or magnetic transition.
The large incoherent scattering cross-section of hydrogen combined with an exact knowledge of the form of the scattering function can be utilized in neutron spectroscopic experiments to study local structural environments as well as interaction strengths. An inportant application of this technique is to focus on a particular hydrogen atom, or hydrogenous molecular group in the material, mainly by employing isotopic substitution. Hydrogen is thereby used as a local probe of structure as well as dynamics. Examples include: site geometry and occupancy in metal hydrides, potential well geometry of hydrogen-metal complexes and hydrogen-bonded systems, and dynamical coupling in linear chain hydrogen-bonded materials. 19 refs., 3 figs.
Vibrational Spectroscopy Provides In A Very Readable Fashion A Comprehensive Account Of The Fundamental Principles Of Infrared And Raman Spectroscopy For Structural Applications To Inorganic, Organic And Coordination Compounds. Theoretical Analyses Of The Spectra By Normal Coordinate Treatment, Factor Group Analysis And Molecular Mechanics Are Delineated.The Book Features: * Coverage From First Principles To Recent Advances * Relatively Self-Contained Chapters * Experimental Aspects * Step By Step Treatment Of Molecular Symmetry And Group Theory * Recent Developments Such As Non-Linear Raman Effects * Comprehensive Treatment Of Rotation Spectroscopy * Band Intensities * Spectra Of Crystals * End-Of-Chapter Exercises.Suitable For Students And Researchers Interested In The Field Of Vibrational Spectroscopy. No Prior Knowledge Of Concepts Specific To Vibrational Spectroscopy Is Necessary. Mathematical Background Such As Matrices And Vectors Are Provided.
- Up-to-date account of the principles and practice of inelastic and spectroscopic methods available at neutron and synchrotron sources - Multi-technique approach set around a central theme, rather than a monograph on one technique - Emphasis on the complementarity of neutron spectroscopy and X-ray spectroscopy which are usually treated in separate books
Experimental Neutron Resonance Spectroscopy deals with the experimental technique of neutron resonance spectroscopy. Pulsed accelerator time-of-flight spectrometers and gamma rays from neutron capture in resonances are discussed. Total neutron cross section measurements are presented, along with neutron scattering and capture cross-section measurements and measurements on fissile nuclides. This book is comprised of five chapters and begins with an introduction to pulsed accelerator time-of-flight spectrometers with moderated continued neutron spectra, together with the pulsed Van De Graaff. Experimental techniques used for neutron cross section measurements, including detectors and data acquisition equipment, are then outlined. Scattering measurements and capture measurements as well as gamma-ray spectra from the capture of neutrons in resonances are considered. The final chapter focuses on the detailed and varied experiments that have been performed on the complicated fission process, together with the parameters of the resonances of the fissile nuclides. This monograph will be a useful resource for spectroscopists and physicists.