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An up-to-date overview of reflectometers used for optical spectroscopy of various kinds of liquids, ranging from well-known transparent liquids to "pathological" industrial liquids. The book reviews and explains basic materials for anyone wanting to get to know the theory, spectral analysis and modern devices needed for the measurement of refractive index and absorption of liquids. Moreover, the book gives an introduction to reflectivity from optically nonlinear liquids such as liquids containing nanoparticles.
UV-VIS spectroscopy is one of the oldest methods in molecular spectroscopy. The definitive formulation of the Bouguer-Lambert Beer law in 1852 created the basis for the quantitative evaluation of absorption measurements at an early date. This led firstly to colorimetry, then to photometry and finally to spectrophotometry. This evolution ran parallel with the development of detectors for measuring light intensities, i.e. from the human eye via the photo element and photocell, to the photomultiplier and from the photo graphic plate to the present silicon-diode detector both of which allow simultaneous measurement of the complete spectrum. With the development of quantum chemistry, increasing atten tion was paid to the correlation between light absorption and the structure of matter with the result that in recent decades a number of excellent discussions of the theory of electronic spectroscopy (UV-VIS and luminescence sp,~ctroscopy) have been published. Consequently, this extremely ivteresting aspect of molecular spec troscopy has dominated the teaching of the subject both in my own lectures and those of others. However, it is often overlooked that, in addition to the theory, applications of spectroscopic methods are of particular interest to scientists. For this reason, a lecture series about electronic spectroscopy given in the Institute for Physical Chemistry at the Heinrich-Heine-University in Dusseldorf was supplemented by one about "UV-VIS spectroscopy and its applications". This formed the basis of the present book.
Experimental Methods and Instrumentation for Chemical Engineers, Second Edition, touches many aspects of engineering practice, research, and statistics. The principles of unit operations, transport phenomena, and plant design constitute the focus of chemical engineering in the latter years of the curricula. Experimental methods and instrumentation is the precursor to these subjects. This resource integrates these concepts with statistics and uncertainty analysis to define what is necessary to measure and to control, how precisely and how often.The completely updated second edition is divided into several themes related to data: metrology, notions of statistics, and design of experiments. The book then covers basic principles of sensing devices, with a brand new chapter covering force and mass, followed by pressure, temperature, flow rate, and physico-chemical properties. It continues with chapters that describe how to measure gas and liquid concentrations, how to characterize solids, and finally a new chapter on spectroscopic techniques such as UV/Vis, IR, XRD, XPS, NMR, and XAS. Throughout the book, the author integrates the concepts of uncertainty, along with a historical context and practical examples.A problem solutions manual is available from the author upon request. - Includes the basics for 1st and 2nd year chemical engineers, providing a foundation for unit operations and transport phenomena - Features many practical examples - Offers exercises for students at the end of each chapter - Includes up-to-date detailed drawings and photos of equipment
This book is the first comprehensive work to be published on far-ultraviolet (FUV) and deep-ultraviolet (DUV) spectroscopy, subjects of keen interest because new areas of spectroscopy have been born in the FUV and DUV regions. For example, FUV spectroscopy in condensed matter has become possible due to the development of attenuated total reflection/FUV spectroscopy. As other examples, DUV surface-enhanced Raman scattering and DUV tip-enhanced Raman scattering have received great attention. Imaging by DUV spectroscopy has also become an area of interest. More recently, FUV and DUV spectroscopy have shown potential for applications in several fields including industry. All these topics are described in this book. Doctoral students and researchers in universities and national research institutes as well as researchers in various industries will find this volume highly useful.
This volume presents a complete and thorough examination of advances in the instrumentation, evaluation, and implementation of UV technology for reliable and efficient data acquisition and analysis. It provides real-world applications in expanding fields such as chemical physics, plasma science, photolithography, laser spectroscopy, astronomy and a
Unlock the Power of Spectroscopy for Analysis Spectroscopy provides critical insights into chemical structures and properties. This book offers an in-depth guide to Four essential spectroscopy techniques for every chemist's toolkit: UV-Vis, IR, Mass, and NMR. Learn the theoretical foundations that make spectroscopy possible. Master the instrumentation involved in modern spectroscopic analysis. Discover practical applications from molecular identification to structural elucidation. Whether you are new to spectroscopy or looking to deepen your expertise, this book has you covered. Key Features: · Comprehensive overview of UV-Vis, IR, Mass, and NMR spectroscopic techniques · Plain explanations of fundamental principles behind spectroscopy · Detailed guidance on instrumentation, equipment, and procedures · Practical examples demonstrating spectroscopic analysis in chemical research. · Extensive illustrations and spectra to enhance understanding. · Chapter summaries and practice questions for testing knowledge Written by leading experts in analytical chemistry, this book combines deep scientific rigor with accessibility and relevance. It empowers chemistry students and working professionals to advance their skills and careers through a fuller command of essential spectroscopy techniques.
TheKramers-Kronigrelationsconstitutethemathematicalformulationofthe fundamental connection between the in-phase to the out-of-phase response of a system to a sinusoidal time-varying external perturbation. Such connection exists in both classical and quantum physical systems and derives directly from the principle of causality. Apart from being of great importance in high energy physics, statistical physics, and acoustics, at present the Kramers-Kronig relations are basic and widely-accepted tools for the investigation of the linear optical properties of materials, since they allow performing the so-called inversion of optical data, i.e. acquiring knowledge on dispersive phenomena by measurements of absorptive phenomena over the whole energy spectrum or vice versa. Since the late ’80s, a growing body of theoretical results as well as of experimental evidences has shown that the Kramers-Kronig relations can be adopted for e?ciently acquiring knowledge on nonlinear optical phenomena. These results suggest that the Kramers-Kronig relations may become in a near future standard techniques in the context of nonlinear spectroscopy. Thisbookisthe?rstcomprehensivetreatisedevotedtoprovidingauni- ing picture of the physical backgrounds, of the rigorous mathematical theory, and of the applications of the Kramers-Kronig relations in both ?elds of l- ear and nonlinear optical spectroscopy. Some basic programs written for the 1 MATLAB environment are also included. This book is organized as an argumentative discourse, progressing from the linear to the nonlinear phenomena, from the general to the speci?c s- tems, and from the theoretical to the experimental results.
An accessible, introductory text explaining how to select, set up and use optical spectroscopy and optical microscopy techniques.
This book is essential for anyone seeking to understand and apply the latest analytical techniques in forensic investigation, saving time, materials, energy, and manpower by providing guidance on the most appropriate techniques for different types of investigations. Advances in Analytical Techniques for Forensic Investigation is aimed to describe the applicability of different types of analytical techniques used for the forensic investigation, including FT-IR, chromatography, mass spectroscopy, NMR spectroscopy, atomic absorption spectroscopy, UV- vis spectroscopy, etc. This book will focus on current and emerging developments in the latest analytical techniques and methods used in the forensic investigation and sample analysis of various physical, chemical, and biological samples in order to facilitate the smooth conduction of justice.
Techniques of Vacuum Ultraviolet Spectroscopy was first published in 1967. In the three decades since, the techniques associated with vacuum ultraviolet spectroscopy have been greatly expanded. Originally published as two volumes in the serial "Experimental Methods in the Physical Sciences," Vacuum Ultraviolet Spectroscopy combines in one paperback volume information on the many advances in vacuum ultraviolet (VUV) research. In addition, the book provides students and researchers with concise reviews of the important aspects of designing experiments in the VUV region.This is the only comprehensive treatise describing the use of synchrotron and other light sources for research, along with the new technologies in optical elements, multilayers, mirror coatings, soft x-ray zone plates, VUV detectors, interferometric spectrometers, and subjects such as spectromicroscopy, lithography, and photon-induced fluorescence. Vacuum Ultraviolet Spectroscopy is an ideal handbook both for the beginner and for the experienced researcher in any field requiring the use of VUV radiation. Key Features* Detailed review of synchrotron radiation sources including undulators and wigglers* Comprehensive outline of monochromator design* Concise review of optics theory for multilayers, spectrometers, and zone plates* Information about other important VUV sources such as laser produced plasmas and Electron Beam Ion Trap (EBIT) sources* Applications such as spectromicroscopy, lithography, and fluorescence