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Completely rewritten, revised, and updated, this Sixth Edition reflects the latest technologies and applications in spectroscopy, mass spectrometry, and chromatography. It illustrates practices and methods specific to each major chemical analytical technique while showcasing innovations and trends currently impacting the field. Many of the chapters have been individually reviewed by teaching professors and include descriptions of the fundamental principles underlying each technique, demonstrations of the instrumentation, and new problem sets and suggested experiments appropriate to the topic. About the authors... JAMES W. ROBINSON is Professor Emeritus of Chemistry, Louisiana State University, Baton Rouge. A Fellow of the Royal Chemical Society, he is the author of over 200 professional papers and book chapters and several books including Atomic Absorption Spectroscopy and Atomic Spectroscopy. He was Executive Editor of Spectroscopy Letters and the Journal of Environmental Science and Health (both titles, Marcel Dekker, Inc.) and the Handbook of Spectroscopy and the Practical Handbook of Spectroscopy (both titles, CRC Press). He received the B.Sc. (1949), Ph.D. (1952), and D.Sc. (1978) degrees from the University of Birmingham, England. EILEEN M. SKELLY FRAME recently was Clinical Assistant Professor and Visiting Research Professor, Rensselaer Polytechnic Institute, Troy, New York. Dr. Skelly Frame has extensive practical experience in the use of instrumental analysis to characterize a wide variety of substances, from biological samples and cosmetics to high temperature superconductors, polymers, metals, and alloys. Her industrial career includes supervisory roles at GE Corporate Research and Development, Stauffer Chemical Corporate R&D, and the Research Triangle Institute. She is a member of the American Chemical Society, the Society for Applied Spectroscopy, and the American Society for Testing and Materials. Dr. Skelly Frame received the B.S. degree in chemistry from Drexel University, Philadelphia, Pennsylvania, and the Ph.D. in analytical chemistry from Louisiana State University, Baton Rouge. GEORGE M. FRAME II is Scientific Director, Chemical Biomonitoring Section of the Wadsworth Laboratory, New York State Department of Health, Albany. He has a wide range of experience in the field and has worked at the GE Corporate R&D Center, Pfizer Central Research, the U.S. Coast Guard R&D Center, the Maine Medical Center, and the USAF Biomedical Sciences Corps. He is an American Chemical Society member. Dr. Frame received the B.A. degree in chemistry from Harvard College, Cambridge, Massachusetts, and the Ph.D. degree in analytical chemistry from Rutgers University, New Brunswick, New Jersey.
PRINCIPLES OF INSTRUMENTAL ANALYSIS is the standard for courses on the principles and applications of modern analytical instruments. In the 7th edition, authors Skoog, Holler, and Crouch infuse their popular text with updated techniques and several new Instrumental Analysis in Action case studies. Updated material enhances the book's proven approach, which places an emphasis on the fundamental principles of operation for each type of instrument, its optimal area of application, its sensitivity, its precision, and its limitations. The text also introduces students to elementary analog and digital electronics, computers, and the treatment of analytical data. Important Notice: Media content referenced within the product description or the product text may not be available in the ebook version.
Analytical chemistry today is almost entirely instrumental analytical chemistry and it is performed by many scientists and engineers who are not chemists. Analytical instrumentation is crucial to research in molecular biology, medicine, geology, food science, materials science, and many other fields. With the growing sophistication of laboratory equipment, there is a danger that analytical instruments can be regarded as "black boxes" by those using them. The well-known phrase "garbage in, garbage out" holds true for analytical instrumentation as well as computers. This book serves to provide users of analytical instrumentation with an understanding of their instruments. This book is written to teach undergraduate students and those working in chemical fields outside analytical chemistry how contemporary analytical instrumentation works, as well as its uses and limitations. Mathematics is kept to a minimum. No background in calculus, physics, or physical chemistry is required. The major fields of modern instrumentation are covered, including applications of each type of instrumental technique. Each chapter includes: A discussion of the fundamental principles underlying each technique Detailed descriptions of the instrumentation. An extensive and up to date bibliography End of chapter problems Suggested experiments appropriate to the technique where relevant This text uniquely combines instrumental analysis with organic spectral interpretation (IR, NMR, and MS). It provides detailed coverage of sampling, sample handling, sample storage, and sample preparation. In addition, the authors have included many instrument manufacturers’ websites, which contain extensive resources.
This book describes both the theory of atomic spectroscopy and all the major atomic spectrometric techniques (AAS, Flame-AES, Plasma AES, AFS, and ICP-MS), including basic concepts, instrumentation and applications. Spectrochemical Analysis by Atomic Absorption and Emission is very wide in scope and will be extremely useful to both undergraduates and lecturers undertaking modern analytical chemistry courses. It contains many figures and tables which illuminate the text, covers various sample preparation methods and gives suggestions for further reading.
"Intrumental Analysis provides comprehensive, modern, and engaging coverage of chemical instrumentation, written with the undergraduate student in mind. At its core, it includes the underlying theory, instrumental design, applications, and operation of spectroscopic, electroanalytical, chromatiographic, and mass spectral instrumentation. It provides students with the requistic skills to identify the comparative advantages and disadvantages in choosing one analytical technique over another by combining direct comparisons of the techniques with a discussion of how these choices affect the interpretation of the data in its final form."--
The critically acclaimed guide to the principles, techniques, and instruments of electroanalytical chemistry-now expanded and revised Joseph Wang, internationally renowned authority on electroanalytical techniques, thoroughly revises his acclaimed book to reflect the rapid growth the field has experienced in recent years. He substantially expands the theoretical discussion while providing comprehensive coverage of the latest advances through late 1999, introducing such exciting new topics as self-assembled monolayers, DNA biosensors, lab-on-a-chip, detection for capillary electrophoresis, single molecule detection, and sol-gel surface modification. Along with numerous references from the current literature and new worked-out examples, Analytical Electrochemistry, Second Edition offers clear, reader-friendly explanations of the fundamental principles of electrochemical processes as well as important insight into the potential of electroanalysis for problem solving in a wide range of fields, from clinical diagnostics to environmental science. Key topics include: The basics of electrode reactions and the structure of the interfacial region Tools for elucidating electrode reactions and high-resolution surface characterization An overview of finite-current controlled potential techniques Electrochemical instrumentation and electrode materials Principles of potentiometric measurements and ion-selective electrodes Chemical sensors, including biosensors, gas sensors, solid-state devices, and sensor arrays
"Introduction to Instrumental Analysis", second edition, contains 28 chapters and approximately 1100 pages which deal with an introduction to most aspects of electricity and electronics including computers and computer interfacing to analytical instruments, and all of the major categories of the instrumental methods of chemical analysis. The text has been updated from the first edition to include recent advances in instrumentation. The writing has been revised in order to make it more understandable to students and other readers. The instrumental methods of analysis that are described in the text include all of the major absorptive and luminescent spectral methods, the atomic and ionic spectral methods including atomic absorption, atomic and ionic emission, and laser-enhanced ionization, chemiluminescence and electrochemiluminescence, photoacoustic spectroscopy, radiative scattering, refractometry, nuclear magnetic resonance, electron spin resonance, multiple x-ray methods, radiochemical methods, mass spectrometry, all of the major electroanalytical methods, all of the major chromatographic methods, thermal analysis, and automated laboratory analysis including the use of laboratory robots and control loops. The appendixes include the answers to all of the problems, a listing of ASCII characters, abbreviations that are used in the text, and mathematical constants that are used in the text
Crucial to research in molecular biology, medicine, geology, food science, materials science, and many other fields, analytical instrumentation is used by many scientists and engineers who are not chemists. Undergraduate Instrumental Analysis, Seventh Edition provides users of analytical instrumentation with an understanding of these instruments, c
Instrumental Methods of Analysis is a textbook designed to introduce various analytical and chemical methods, their underlying principles and applications to the undergraduate engineering students of biotechnology and chemical engineering. This book would also be of interest to students who pursue their B. Sc / M. Sc degree programs in biotechnology and chemistry.