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This book provides a detailed description of technical elements of a microbore column liquid chromatograph suitable for use in trace analysis. It presents examples of analyses, especially from the spheres of biochemistry, pharmacology, and environmental analytical chemistry.
Organic Trace Analysis by Liquid Chromatography focuses on high-performance liquid chromatography in the field of formulations analysis, which includes quality control of pharmaceutical preparations, pesticide formulations, cosmetics, and food colors. This book explores the application of liquid chromatography to trace analysis. Organized into 10 chapters, this book starts with an overview of the special requirements of liquid chromatography for trace analysis. This text then compares the approach to gas chromatography and formulations analysis, noting the significant difference. Other chapters consider the liquid chromatography equipment and examine the best types and conditions of instrumentation suitable for trace analysis. This book discusses as well the chromatography theory and includes descriptive accounts of the principles of the different forms of chromatography. The final chapter describes the typical approaches that are used for trace analysis. This book is a valuable resource for analysts engaged in the determination of trace organics in many various substrates.
"Organic Trace Analysis" presents the basics of trace analysis, from sample preparation to the measurement: Students are introduced to statistical evaluation, quality control technologies, sampling and preparation of organic traces, as well as to enrichment and separation of samples. Spectroscopic techniques as chromatography, capillary electrophoresis, mass spectrometry, and receptor-based bioanalysis are presented in detail.
Trace Analysis, Volume 2 is devoted to critical discussions of selected topics in organic and inorganic analytical chemistry including instrumentation, techniques, and applications to the detection, identification, and quantitation of trace quantities of substances in a large variety of sample materials. The volume presents expositions of selected topics on trace analysis such as vitamin analysis in foods and tissues; liquid chromatography - mass spectrometry with emphasis on approaches to interfacing; approaches to the isolation and concentration of trace organics from aqueous samples; and the advantages of unmodified silica gel for the chromatographic separation of polar substances. The book will be highly useful to both organic and inorganic chemists.
Trace Analysis, Volume 3 focuses on critical discussions of selected topics in organic and inorganic analytical chemistry including instrumentation, techniques, and applications to the detection, identification, and quantitation of trace quantities of substances in a large variety of sample materials. The book is divided into two parts: Section 1, biological fluids and tissues, and Section 2, environmental analysis. Chapters are devoted in the discussion of subjects on the analysis of carbonyl compounds; the use of enzymatic methods for clinical analysis; the use of fluorescence spectroscopy for single compounds or multicomponent analysis of pollutants in air, water, and soils, with emphasis on fuel oils; and the analysis of polycyclic aromatic compounds in combustion emissions. Organic and inorganic chemists and medical technicians will find the book a good reference text.
Microcolumn High-Performance Liquid Chromatography
HPLC is the principal separation technique for identification of the pesticides in environmental samples and for quantitative analysis of analytes. At each stage of the HPLC procedure, the chromatographer should possess both the practical and theoretical skills required to perform HPLC experiments correctly and to obtain reliable, repeatable, and r