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Titrations in Nonaqueous Solvents discuss the theory, practice, and data on acidic and basic strength of nonaqueous solvents. This book is organized into three parts encompassing six chapters. The first part considers the general principles of acids and bases and methods of end-point determination. This part also covers the fundamentals, advantages, and limitations of titration instruments, such as potentiometers, burets, titration vessels, and electrodes. The classification of titration solvents according to their functions as color indicators and titrant solutions is provided in this part. The remaining parts describe the analytical procedures for acidity and basicity of nonaqueous solvents. These parts also provide a tabulated data on the acidic and basic strengths, stability, and dissociation constants of various titration solvents. Analytical chemists, and analytical chemistry teachers and students will find this book invaluable.
Arising no doubt from its pre-eminence as a natural liquid, water has always been considered by chemists as the original solvent in which very varied chemical reactions can take place, both for preparational and for analytical purposes. This explains the very long-standing interest shown in the study of aqueous solutions. In this con nection, it must be stressed that the theory of Arrhenius and Ostwald (1887-1894) on electrolytic dissociation, was originally devised solely for solutions in water and that the first true concept of acidity resulting from this is linked to the use of this solvent. The more recent development of numerous physico-chemical measurement methods has made possible an increase of knowledge in this area up to an extremely advanced degree of systematization. Thus today we have available both a very large amount of experimental data, together with very refined methods of deduction and of quantitative treatment of chemical reactions in solution which enable us to make the fullest use of this data. Nevertheless, . it appears quite evident at present that there are numerous chemical processes which cannot take place in water, and that its use as a solvent imposes 2 INTRODUCTION limitations. In order to overcome these limitations, it was natural that interest should be attracted to solvents other than water and that the new possibilities thus opened up should be explored.
pH Measurements is a seven-chapter simplified text on obtaining a high degree of accuracy in practical pH measurement. The introductory chapter of this book relates the principles of pH measurements to the actual measurement. This chapter specifically tackles the factors involved in the measurement and what magnitude of effect does each factor have on the measurement. These topics are followed by discussions on the components of pH equipment and technique, including the electrodes and buffers. A chapter considers the general approach of pH measurements and illustrates with examples of some common difficult samples. The concluding chapter shows the isolation and correction a pH equipment malfunction. pH equipment operators and users will find this book rewarding.
Non-Aqueous Solvents in Inorganic Chemistry gives a concise treatment of the important inorganic non-aqueous solvents, emphasizing why they do in fact exhibit solvent power, how they are prepared and handled experimentally, how they can be used as media for the synthesis or analysis of inorganic and organometallic compounds, and how far the various acid-base concepts can be useful in accounting for many (but not all) of the reactions observed. This book is intended primarily for the undergraduate reader—both for the intending Chemistry Honours or R.I.C. graduate and the non-specialist student of chemistry. The subject matter is presented in a simple and readable form, without the inclusion of elaborate tables of properties and with the minimum of detail necessary for comprehension. Therefore, those working for the A- and S-level chemistry examinations for the G.C.E. could read much of the book with profit; and the research student who aspires to work in the field of non-aqueous solvents will, it is hoped, find this book a useful introduction to a fascinating branch of inorganic chemistry.
An excellent resource for all graduate students and researchers using electrochemical techniques. After introducing the reader to the fundamentals, the book focuses on the latest developments in the techniques and applications in this field. This second edition contains new material on environmentally-friendly solvents, such as room-temperature ionic liquids.
Nonaqueous Electrolytes Handbook, Volume II, is an authoritative and updated information source for nonaqueous solvent systems. The information in this handbook covers literature to 1973 and includes data for some 310 solvent systems. This volume has been organized to include 11 well-defined areas: Solubilities of Electrolytes; EMF and Potentiometric Titrations; Vapor Pressures; Cryoscopy; Heats of Solution Calorimetry; Polarography; Ligand Exchange Rates and Electrode Reactions; Electrical Double Layer; Spectroscopy and Structure of Electrolytes; Organic Electrolyte Battery Systems; and Additional References and Data Sources. The section on polarography is divided further according to inorganic electrolytes, organic electrolytes, and organometallic compounds, in order to present the wealth of data in a concise and orderly manner. As in Volume I, the last section covers additional data sources, reviews, and data and references that were received too late to include in the earlier sections. The method of presentation of material is briefly described in the introduction to each section to facilitate the use of the tabulated information and bibliographies are given at the end of each section. A Compound Index is included.