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Based on the author's many years of experience in practicing safety assessment in industry and teaching students or professionals in this area, the topic of this book is seldom found on university curricula and many professionals do not have the knowledge required to interpret thermal data in terms of risks. For this reason, Francis Stoessel adopts a unique systematic how-to-do approach: Each chapter begins with a case history illustrating the topic and presenting the lessons learned from the incident. In so doing, he analyzes a goldmine of numerous examples stemming from industrial practice, additionally providing a series of problems or case studies at the end of each chapter. Divided into three distinct sections, part one looks at the general aspects of thermal process safety, while Part 2 deals with mastering exothermal reactions. The final section discusses the avoidance of secondary reactions, including heat accumulation and thermal confinement.
Vollständig überarbeitete,aktualisierte 2. Auflage mit fünf neuen Kapiteln und den aktuellen IUPAC-Normen. Beschäftigt sich mit thermischen Risiken in der chemischen Prozessindustrie. Jedes Kapitel beginnt mit einer Fallstudie und den aus Zwischenfällen gewonnen Erkenntnissen.
Assess the potential hazards of your process before designing the plant. 100 case studies have been added to the original text of the first edition. This second edition provides a basis for the identification and evaluation of chemical reaction hazards not only for practising chemists, engineers and plant personnel but also for students.
Hardbound. Exothermic reactions used for the production of chemicals present a hazard if they proceed without control. Runaway reactions can result in a blow-off of the reactor top and an emission of reactants and products, possibly followed by a gas explosion. Undesired exothermic reactions initiated during production, purification or storage by excessive temperatures or other causes have similar destructive effects, even if the origin is different. Although the hazards connected with exothermic reactions have been known since the inception of the chemical industry, a systematic knowledge of the possible effects has only been developed in the last 25 years. A number of incidents in the chemical industry, which have been investigated by groups of experts from various companies, have promoted the understanding of these hazards. The author has investigated incidents in plants and tested experimental methods for more than 20 years. In particular he was inter
Drawn from international sources, this book provides principles and strategies for the evaluation of chemical reactions, and for using this information in process design and management. A useful resource for engineers who design, start-up, operate, and manage chemical and petrochemical plants, the book places special emphasis on the use of state-of-the-art technology in theory, testing methods, and applications in design and operations.
This revised edition of a best-selling book continues to provide a basis for the identification and evaluation of chemical reaction hazards for chemists, engineers, plant personnel, and students. Before undertaking the design of a chemical manufacturing process it is vital that the chemical reactions involved be fully understood, potential hazards assessed, and safety measures planned. Chemical Reaction Hazards aims to help the people responsible for this design and operation to meet the general duties of safety. Two major additions to this revised book are the appendices. One of these describes 100 incidents, illustrating their cause and indicating consequences if appropriate procedures within this guide are not followed. The second provides a practical example of a typical chemical reaction hazard assessment, from consideration of the process description, through experimental testing to the specification of safety measures.
In its recent investigation of chemical reactivity accidents, the US Chemical Safety Board noted a gap in technical guidance and regulatory coverage. This volume closes the gap in technical guidance, helping small and large companies alike identify, address, and manage chemical reactivity hazards. It guides the reader through an analysis of the potential for chemical reactivity accidents to help prevent fires, explosions, toxic chemical releases or chemical spills. This volume is applicable to processes at any scale and is particularly useful for chemists, safety managers, and engineers involved in scale-up. An enclosed CD-ROM provides portable checklists, analysis tools, and a list of additional references. Note: CD-ROM/DVD and other supplementary materials are not included as part of eBook file.
The wide range of applications of thermal methods of analysis in measuring physical properties, studying chemical reactions and determining the thermal behaviour of samples is of interest to academics and to industry. These applications prompted the writing of this book, in the hope that the descriptions, explanations and examples given would be of help to the analyst and would stimulate the investigation of other thermal techniques. Thermal studies are a fascinating means of examining the samples and the problems brought to us by colleagues, students and clients. If time allows, watching crystals change on a hot-stage microscope, or measuring the properties and changes on a DSC or TG or any thermal instrument can be a rewarding activity, besides providing valuable analytical information. This book started from a series of lectures delivered at Kingston University and at meetings of the Thermal Methods Group of the United Kingdom. The collaboration and information supplied to all the contribu tors by colleagues and instrument manufacturers is most gratefully ack nowledged, as are the valuable contributions made at meetings of the International Confederation for Thermal Analysis and Calorimetry (ICT AC) and at the European Symposia on Thermal Analysis and Calorimetry (ESTAC).
Guidelines for Chemical Reactivity Evaluation and Application to Process Design; CONTENTS; List of Tables; List of figures; Preface; Acknowledgments; Glossary; List of Symbols; 1. INTRODUCTION; 2. IDENTIFICATION OF HAZARDOUS CHEMICAL REACTIVITY; 3. CHEMICAL REACTIVITY CONSIDERATIONS IN PROCESS/REACTOR DESIGN AND OPERATION; REFERENCES; INDEX.