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Spectrophotometry enables one to determine, with good precision and sensitivity, almost all the elements present in small and trace quantities of any material. The method is particularly useful in the determination of non-metals and allows the determination elements in a large range of concentrations (from single % to low ppm levels) in various materials.In Separation, Preconcentration and Spectrophotometry in Inorganic Analysis, much attention has been paid to separation and preconcentration methods, since they play an essential role in increasing the selectivity and sensitivity of spectrophotometric methods. Separation and preconcentration methods have also been utilised in other determination techniques.Spectrophotometric methods which are widely used for the determination of the elements in a large variety of inorganic materials are presented in the book whilst separation and preconcentration procedures combined with spectrophotometry are also described. This book contains recent advances in spectrophotometry, detailed discussion of the instrumentation, and the techniques and reagents used for spectrophotometric determination of elements in a wide range of materials as well as a detailed discussion of separation and preconcentration procedures that precede the spectrophotometric detection.
Analytical Chemistry of Zirconium and Hafnium compiles literature on the characterization and analysis of zirconium and hafnium. Various methods in studying the properties of the featured elements are presented in this book. This book also discusses the aqueous solutions of zirconium and hafnium. It then explains the methods such as dissolution of ores and alloys, detection and identification, and gravimetric determinations. This text further examines the titrimetric, electrometric, and absorptiometric methods, as well as methods of separations using ion-exchange and using solvent extraction, along with separation of hafnium from zirconium. The latter part of this text presents methods such as spectrographic analyses, X-ray analyses, and neutron activation analysis and separation of tracers. This book will come in handy for chemists and chemistry students, as well as for others interested in studying zirconium and hafnium.
Modern Methods for the Separation of Rarer Metal Ions describes several separation methods of more than 50 elements. This book is divided into 19 chapters that include separation methods involving the actinide elements, rare earths, and many rarer elements of the main and transition groups of the periodic table. The introductory chapter discusses the principles of the separation techniques presented in this book. The remaining chapters explore the application of specific separation methods, such as ion exchange, chromatography, liquid-liquid extraction, distillation, and coprecipitation. The approach of each chapter is a presentation of separation principle of an element first followed by numerous examples of applications to the solution of practical problems encountered in separation chemistry. Chapters 2 and 3 examine the separations involving the actinides and rare earth elements using ion exchange and liquid-liquid extraction These are followed by chapters dealing with separations of other rarer elements, which have been arranged according to their position in the periodic table. These elements are: Li, Rb, Cs, Fr, Be, Ra, Ga, In, Tl, Ge, Ag, Au, Ti, Zr, Hf, V, Nb, Ta, Mo, W, Tc, Re and the platinum metals. This book will be of great use to analytical chemists.