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International Series of Monographs in Analytical Chemistry, Volume 44: The Determination of Impurities in Nuclear Grade Sodium Metal (and Related Sodium Compounds) provides analytical chemical procedures for the determination of impurities in nuclear grade sodium metal. This book is composed of 25 chapters, and begins with a presentation of the methods for dissolving, bulk separation, sampling, and handling of sodium metal. The rest of the book describes the procedures for impurity determination in nuclear grade sodium metals, including aluminum, bismuth, boron, cadmium, calcium, magnesium, carbon, cesium, and chloride. Other impurities considered include chromium, cobalt, copper, hydrogen, iodine, iron, lead, lithium, manganese, nickel, oxide, oxygen, and phosphorus. The last chapters examine the procedures for determination of potassium, silicon, sulfur, and uranium impurities. This book is of value to analytical and inorganic chemists.
Principles of Field Ionization and Field Desorption Mass Spectrometry delves deeper into field ionization and field desorption. The book covers the five main subareas of field ionization and field desorption mass spectrometry that has grown in importance. Coverage includes the theory of field ionization and field desorption; field ionization and field desorption techniques and sources; high field surface chemistry; kinetics and mechanisms of decompostion of field ions in the gas phase; and qualitative and mixture analysis with field ionization and field desorption mass spectrometry. The text is recommended for students, experts, and researchers in chemistry, especially those who wish to learn more or have an in-depth study about field ionization and field desorption, its principles, and its applications in chemistry.
Analytical Chemistry of Organic Halogen Compounds presents the procedures applied in the analysis of organic halogen compounds. This book is composed of eight chapters that discuss the methods involved in the production and application of organic halogen compounds and in overcoming contamination problems caused by these compounds. After briefly dealing with the preparation, characteristics, and reactions of organic halogen compounds, this book goes on discussing the fundamental concepts of methods for the detection of halogens in organic compounds, namely, chlorine, bromine, iodine, and fluorine. The following chapter describes the characteristic features, advantages, and disadvantages of ultramicro and submicro chemical methods. A chapter also examines the qualitative and quantitative studies of organic halogen compounds based on the thermal and chemical stability of these compounds. The concluding chapters discuss the interference or interfering effects of halogens and their elimination in the determination of other elements. A list of physical constants of organic halogen compounds of general pharmaceutical and industrial significance is provided. This book is an ideal source for analytical chemists and other workers who are interested in the theoretical bases of the methods.
The international seminar "Material Behavior and Physical Chemistry in Liquid Metal Systems" was organized by the Institute of Materials and Solid State Research of the Karlsruhe Nuclear Research Center (Karlsruhe, Federal Republic of Germany). The seminar was held at the Nuclear Engineering School of the center on March 24-26, 1981. The aim of the seminar was to give metallurgists, chemists,. and physicists working in different areas of the science and technology of liquid metals an opportunity to discuss the basic work and the need for further work in this field. Since the seminar was held near one of the laboratories which for the last few years has been engaged in liquid alkali metal studies, partic ipants also had an opportunity to observe modern equipment for liquid alkali metal research. Interest in the application of liquid metals as working fluids in energy production, conversion, and storage is increasing. The technology has already demonstrated its high standards, which make possible the operation of large sodium-cooled fast reactors. Past conferences have shown, however, that there is still a lack of basic knowledge and understanding. Therefore, the aim of the present seminar was to discuss basic work in detail, and most of the papers contributed to this objective.
Science and Technology of Liquid Metal Coolants in Nuclear Engineering is a comprehensive consolidation of the latest research and knowledge on liquid metal coolants. Over the last decades, various new technologies have been developed for the liquid metal coolants of fast breeder and fusion reactors and accelerator driven systems. Details of pumps and instrumentation used in these coolants and their operating principles are included to provide the reader with a well-rounded understanding of the topic and to guide on the operation of different liquid metal coolant systems. Methods for the safe handling and control of impurity levels in these coolants are clearly discussed, along with alkali metal fires and their management, including methods for safe disposal of sodium waste. - Discusses the thermophysical and chemical properties of liquid metals described with their microscopic origin - Includes methods for the safe handling of liquid metal coolants and their purification and management - Discusses pumps and instrumentation principles and design