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A concise introduction to modern crystal structure determination, emphasizing both the crystallographic background and the successive practical steps. In the theoretical sections, more importance is attached to a good understanding, than to a rigorous mathematical treatment. The most important measuring techniques, including the use of modern area detectors, and the methods of data reduction, structure solution and refinement are discussed from a practical point of view. Special emphasis is put on the ability to recognize and avoid possible errors and traps, and to judge the quality of results.
The Crystalline States of Organic Compounds is a broad survey of the techniques by which molecular crystals are investigated, modeled, and applied, starting with the fundamentals of intra- and intermolecular bonding supplemented by a concise tutorial on present-day diffraction methods, then proceeding to an examination of crystallographic databases with their statistics and of such fundamental and fast-growing topics as intermolecular potentials, polymorphism, co-crystallization, and crystal structure prediction by computer. A substantial part of the book is devoted to the techniques of choice in modern simulation, Monte Carlo and molecular dynamics, with their most recent developments and application to formed crystals and to the concomitant phases involved in nucleation and growth. Drawing on the decades-long experience of its author in teaching and research in the field of organic solid state, The Crystalline States of Organic Compounds is an indispensable source of key insights and future directions for students and researchers at any level, in academia and in industry. - Condenses theoretical information and practical methods in a single resource - Provides a guide on the use of crystallographic databases, structure statistics, and molecular simulations - Includes a large number of worked examples and tutorials, with extensive graphics and multimedia
Crystallography may be described as the science of the structure of materi als, using this word in its widest sense, and its ramifications are apparent over a broad front of current scientific endeavor. It is not surprising, therefore, to find that most universities offer some aspects of crystallography in their undergraduate courses in the physical sciences. It is the principal aim of this book to present an introduction to structure determination by X-ray crystal lography that is appropriate mainly to both final-year undergraduate studies in crystallography, chemistry, and chemical physics, and introductory post graduate work in this area of crystallography. We believe that the book will be of interest in other disciplines, such as physics, metallurgy, biochemistry, and geology, where crystallography has an important part to play. In the space of one book, it is not possible either to cover all aspects of crystallography or to treat all the subject matter completely rigorously. In particular, certain mathematical results are assumed in order that their applications may be discussed. At the end of each chapter, a short bibliog raphy is given, which may be used to extend the scope of the treatment given here. In addition, reference is made in the text to specific sources of information. We have chosen not to discuss experimental methods extensively, as we consider that this aspect of crystallography is best learned through practical experience, but an attempt has been made to simulate the interpretive side of experimental crystallography in both examples and exercises.
A textbook for the student beginning a serious study of X-ray crystallography.
The purpose of this book is to explain why molecular structure can be determined by single-crystal diffraction of X rays. It is not an account of the practical procedural details, but rather an account of the underlying physical principles, and the kinds of experiments and methods of handling the experimental data that are used.
A Course On Crystallography Is A Necessary Beginning For All Solid State Physics Courses, Since The Student Must Have A Clear Concept Of The Crystallographic Methods And Principles Before Proceeding To Learn The Physics Of Solids. The Present Authors Have Earlier Written The Book Entitled Crystallography For The Solid State Physics (Wiley 1982). The Book Proved Very Popular With The Students And Reviewers Also Highly Commended The Book, (E.G. One Of The Reviewers Termed It As A Treasure Chest Of Knowledge In Crystallography). However, It Has Been Felt That Solid State Physics Component In The Earlier Book Was Rather Too Little In Content. The Present Book Is An Attempt To Enlarge This Content So As To Provide Solid State Portion Its Due Share. To Accomplish This Already Existing Chapters On Solid State Have Been Enlarged And Some New Chapters Have Been Added. The Book S Intended To Serve As An Introductory Text For All Graduate And Undergraduate Students Whose Eventual Aim Is To Specialise In Solid State Physics.
Systematic Materials Analysis focuses on the broad range of instrumental methods that brings new approaches to materials analysts to yield the desired information about a given material. This book explores the specific instruments that briefly outline the theories of operation. Organized into ten chapters, this volume starts with an overview of the analytical methods on the bases of specimen limitations and information desired, and then examines the use of flow charts encompassing the various instruments. This text then discusses the use of the charts, which present a complete listing of analytical instrumentation arranged so as to enable the selection of the best method for a given analytical task. Other chapters outline the theories of operation and describe the capability of the methods for quantitative and qualitative measurements of chemical composition, texture, and structure as applicable. This book is a valuable resource for materials analysts, engineers, biological scientists, laboratory administrators, and researchers.
The first edition of this book has been out of print for seven years. The ques tion as to whether a new edition should be produced was answered affirmatively on many counts. I think that the considerations which led me to write this book in 1949 are still valid (see Preface to the First Edition). Moreover, a description of those areas of interest which together comprise the field of Mineralogy seems to be more necessary than ever, because of the rapid advances which have been made. Due to the rapid extension of our knowledge, I did not dare again to treat the whole field by myself. Accordingly, Professor ZEMANN kindly agreed to revise the first part of the book dealing with Crystallography. He made many important corrections. In Part II the basic question arose as to whether the physical-chemical approach to rock forming processes, becoming more and more important, required inclusive treatment of the fundamentals of physical chemistry in the book. I see certain dangers in trying to produce a petrology text which is physical chemically self-sufficient. Thus, I retain the same opinion which prevailed when I wrote the previous edition; namely that the necessary basic knowledge should be acquired in lectures and laboratory classes in physics, chemistry, and physical chemistry, and with the help of standard literature dealing with these subjects. This back ground is, therefore, presumed and fundamentals are only referred to occasionally.
This highly readable, popular textbook for upper undergraduates and graduates comprehensively covers the fundamentals of crystallography and symmetry, applying these concepts to a large range of materials. New to this edition are more streamlined coverage of crystallography, additional coverage of magnetic point group symmetry and updated material on extraterrestrial minerals and rocks. New exercises at the end of chapters, plus over 500 additional exercises available online, allow students to check their understanding of key concepts and put into practice what they have learnt. Over 400 illustrations within the text help students visualise crystal structures and more abstract mathematical objects, supporting more difficult topics like point group symmetries. Historical and biographical sections add colour and interest by giving an insight into those who have contributed significantly to the field. Supplementary online material includes password-protected solutions, over 100 crystal structure data files, and Powerpoints of figures from the book.