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Praise for the Fourth Edition"Outstanding praise for previous editions.the single best general reference for the organic chemist."-Journal of the Electrochemical Society"The cast of editors and authors is excellent, the text is, in general, easily readable and understandable, well documented, and well indexed those who purchase the book will be sa
This book provides the first practical, hands-on approach to electroorganic synthesis. It includes many details of the experimental design of cells, electrodes, electrolytes, and so on, as well as methods and reaction conditions for a large range of chemical transformations. By demonstrating the practicalities and versatility of electroorganic synthesis, this book encourages synthetic chemists to learn electrochemical methods for use in their daily activities.
The editors, Lund (emeritus, organic chemistry, Aarhus U., Denmark) and Hammerich (chemistry, U. of Copenhagen), have substantially revised and expanded this basic reference work (originally edited by Bazier). There are two new chapters--on the electrochemistry of C60 compounds and electroenzymatic synthesis--and one-third of the chapters have been rewritten by new authors, these are: carbonyl compounds; anodic oxidation of oxygen-containing compounds; anodic oxidation of sulfur- and selenium-containing compounds; electrosynthesis of bioactive materials (this replaces natural products and pharmaceuticals); organoelemental compounds; reductive coupling; electrochemical partial fluorination; electrogenerated bases; industrial electroorganic chemistry; and conducting polymers. The international group of contributors are all academics in various disciplines in chemistry. Annotation copyrighted by Book News, Inc., Portland, OR
This textbook is an accessible overview of the broad field of organic electrochemistry, covering the fundamentals and applications of contemporary organic electrochemistry. The book begins with an introduction to the fundamental aspects of electrode electron transfer and methods for the electrochemical measurement of organic molecules. It then goes on to discuss organic electrosynthesis of molecules and macromolecules, including detailed experimental information for the electrochemical synthesis of organic compounds and conducting polymers. Later chapters highlight new methodology for organic electrochemical synthesis, for example electrolysis in ionic liquids, the application to organic electronic devices such as solar cells and LEDs, and examples of commercialized organic electrode processes. Appendices present useful supplementary information including experimental examples of organic electrosynthesis, and tables of physical data (redox potentials of various organic solvents and organic compounds and physical properties of various organic solvents).
Practical Aspects of Electroorganic Synthesis presents educational insights into the practical aspects of electrosynthesis methods, providing a variety of examples and techniques. The book covers concepts referred to as "green chemistry" and "sustainable technology." Sections cover direct electrolysis, anodic oxidation, cathodic reduction, mechanistic studies (cyclic voltammetry), and how to set-up electrochemical experiments. Indirect electrolysis is also covered, including an exploration of catalysts and additives to take on modern electrochemical methods. Finally, the book explores the burgeoning new field of paired electrolysis, in which the ultimate green-synthesis applications are possible, with no wasted electrons and very few by-products. This book offers researchers a modern and authoritative resource that brings complete and up-to-date practical concepts of electrosynthesis methods and guides the audience on how to carry out a large number of experimental techniques. - Discusses complete and up-to-date practical concepts of electrosynthesis methods - Provides sound insights into the experimental approaches of electrosynthesis, covering new and novel synthesis techniques - Breaks down the fundamentals aspects of electrolysis into three digestible and logical sections
Baizer (1914-1988) was the foremost internationally recognized authority on organic electrosynthesis. In this festschrift , derived from a memorial symposium held in Montreal, May 1990, as part of the 177th meeting of the Electrochemical Society, and also marking the 25th anniversary of electroorgan
Designed for undergraduate and beginning graduate courses in organic synthesis.