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Direct Synthesis of Metal Complexes provides in-depth coverage of the direct synthesis of coordination and organometallic compounds. The work is primarily organized by methods, but also covers highly relevant complexes, such as metal-polymer coordination compounds. This updated reference discusses recent developments in cryosynthesis, electrosynthesis, and tribosynthesis (popular as it doesn’t require organic solvents), with special attention paid to ‘greener’ methodologies and approaches. Additionally, the book describes physical methods of zero-valent metal interaction with organic matter, including sputtering, ultrasonic treatment and synthesis in ionic liquids. The book presents completely new content as a follow-up to the 1999 Elsevier Science publication Direct Synthesis of Coordination and Organometallic Compounds that was edited by Dr. Garnovskii and Dr. Kharisov. Covers current methods and techniques of metal interactions with organic media leading to metal chelates, adducts, di- and polymetallic complexes, metal-containing macrocycles, supported coordination compounds (i.e., metal complexes on carbon nanotubes), and more Describes reactivities of distinct forms of elemental metals (powders, sheets, nanoparticles (including a host of less-common metal nanostructures) with organic phase (liquid, solid and gaseous) and water Includes experimental procedures, with examples of direct synthesis, at the end of each chapter
International Series of Monographs in Analytical Chemistry, Volume 47: Analytical Chemistry of Molybdenum and Tungsten describes the chemical and instrumental methods of analysis of molybdenum and tungsten. This book is composed of 15 chapters that particularly consider detailed methods for determining these metals in typical samples and their alloys by both classical and modern techniques. The opening chapters discuss the history, occurrence, physico-chemical properties, and applications of molybdenum and tungsten. The succeeding chapters deal with the metals’ sampling, decomposition, separation, and qualitative detection. Considerable chapters are devoted to various chemical and instrumental methods for their analysis, including gravimetry, titrimetry, colorimetry, polarography, amperometry, coulometry, emission and atomic absorption spectroscopy, X-ray spectrophotometry, mass spectrometry, and radiochemical methods. The concluding chapter examines the determination of impurities and alloying elements. This book will prove useful to analytical and inorganic chemists, as well as analytical and inorganic chemistry students.
Kurti and Czako have produced an indispensable tool for specialists and non-specialists in organic chemistry. This innovative reference work includes 250 organic reactions and their strategic use in the synthesis of complex natural and unnatural products. Reactions are thoroughly discussed in a convenient, two-page layout--using full color. Its comprehensive coverage, superb organization, quality of presentation, and wealth of references, make this a necessity for every organic chemist. * The first reference work on named reactions to present colored schemes for easier understanding* 250 frequently used named reactions are presented in a convenient two-page layout with numerous examples* An opening list of abbreviations includes both structures and chemical names * Contains more than 10,000 references grouped by seminal papers, reviews, modifications, and theoretical works * Appendices list reactions in order of discovery, group by contemporary usage, and provide additional study tools* Extensive index quickly locates information using words found in text and drawings