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Many years have passed since the last edition of the present book was published. The discovery during this period of many new reagents has resulted in a vast accumulation of data on their application and made this completely revised edition necessary.Numerous new tests and various new chapters have been added. Chapters 3,4 and 5 of the fifth edition have been combined into one chapter, which is divided into sections devoted to the elements. These sections are arranged in alphabetical order to make for easier location of information on a given element. To further improve the usefulness of the volume, a reference list has been provided for each sub-section followed by a biography of the appropriate quantitative methods.
Covering all theoretical and practical aspects of the applications of spot tests to organic analysis, this book includes information on more than 900 tests. It continues to be an indispensable reference to organic and analytical chemists in academia and in industry.
First written in 1935, Shriner remains a classic text in the field. Coauthor Christine Hermann has introduced modern methods and topics and completely updated the illustration and photo program. The book is ideal for the Advanced Organic Lab and for Spectroscopy courses.
The American edition of our monograph is not a mere translation of the Czech edition, which appeared some five years ago. We have had to respect the fact that even such a short period has sufficed for progress in this field, and that the field of application of methods of organic analysis has widened. We have therefore revised a number of chapters in Part 1, the general part of the monograph-mainly those devoted to chromatographic methods, which have been extended and complemented by methods of thin-layer chromatography and electrophoresis. The chapters on the theory of color reactions and on analytical literature have also been extended; the chapter on spectral methods has been extended by including the use of proton magnetic resonance in organic analysis, and the list of references has been enlarged by adding books of importance for organic analysis. In Part 2, the part dealing specifically with various elements and chemical groups, we have extended the chapters on solubility and on acids and bases. The methods for the detection and identification of given classes of compounds have also been supplemented by references to recent papers.
Quantitative Organic Microanalysis, Second Edition presents the recommendations of the American Chemical Society group for specification and methods of organic microanalysis. This book is organized into 23 chapters, and starts with discussions on test samples, blank tests, second type of efficient vibration-absorbing balance table, and microchemical balances. Other general topics covered include the Kjeldahl procedures to determine nitrogen compounds; oxygen flask combustions; determination of fluorine; and microhydrogenation. The final chapters present the modification of the procedure for the determination of oxygen using gravimetry. This book will be of great value to microanalysts, researchers, and college students who wants to expand their understanding in organic microanalysis.
The Systematic Identification of Organic Compounds A comprehensive introduction to the identification of unknown organic compounds Identifying unknown compounds is one of the most important parts of the study of chemistry. From basic characteristics such as melting and/or boiling point to more complex data generated through cutting-edge techniques, the range of possible methods for identifying unknown organic compounds is substantial. The utility of a research reference which compiles known techniques and characteristics of possible compounds is clear. The Systematic Identification of Organic Compounds provides such a reference, designed to teach a hands-on approach in the chemistry lab. It takes readers step-by-step through the process of identifying an unknown compound and elucidating its structure from infrared, nuclear magnetic resonance, and mass spectra in addition to solubility characteristics, melting point, boiling point, and classification tests. The result is an essential overview for advanced chemistry students looking to understand this exciting area of laboratory work. Readers of the ninth edition of The Systematic Identification of Organic Compounds will also find: A detailed chapter on safety, personal protection equipment, chemical storage, safety data sheets, and other safety concerns New NMR, IR, and mass spectra with detailed explanations on interpretation Questions at the end of each chapter designed to facilitate and reinforce progression, keyed to a companion website for instructors Tables of known compounds including data relevant for identification Companion website with structural problems from experimental data for students to practice how to reason and solve The Systematic Identification of Organic Compounds is a useful reference for advanced undergraduates and graduate students studying organic chemistry, organic spectroscopy, and related subjects.
Techniques of organic analysis; Procedures for tentative identification of an unknown; Procedures for final characterization of an unknown; Tables of organic compounds with their constants and derivatives.