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“A primer on soil analysis using visible and near-infrared (vis-NIR) and mid-infrared (MIR) spectroscopy” is the first training material on the topic of soil spectroscopy for beginner levels, by the Global Soil Laboratory Network Initiative on Soil Spectroscopy (GLOSOLAN-Spec) of the Global Soil Partnership, FAO. This document provides an introduction to the use of soil spectroscopy for soil analysis and covers the basic and fundamental procedures for using this technology for soil analysis. The series “Soil spectroscopy training material” is part of the Global Soil Laboratory Network (GLOSOLAN) to strengthen the capacity of laboratories in soil analysis. It provides a series of training materials covering wide range of topics in soil vis-NIR and MIR spectroscopy. The overall objective is to develop national and regional soil spectral libraries with an estimation service, and to provide advisory services on appropriate instrumentation.
Site-specific management of crop production systems holds promise for maintaining high yields while preserving soil quality. This management requires detailed spatial data on soil physical and chemical characteristics but traditional testing can be slow and expensive. Recently, sensor-based approaches including reflectance spectroscopy have been proposed as alternatives for quicker, easier soil analysis. The objectives of this study were to investigate the soil property estimation capabilities of reflectance sensing with a spectrometer and with a mobile two-band sensor. In the spectrometer evaluation using profile (to 1 m) samples collected from 32 plots with varying soil characteristics, several important soil quality properties were successfully estimated. Highest accuracy was for dried and ground soil samples which had an R2 of 0.97 and 0.91 for total carbon and nitrogen, respectively. Results with field-moist soil were nearly as accurate, showing that this may be a viable, and more efficient, option. The mobile two-band sensor was evaluated in two central Missouri production fields. It showed good accuracy (R2 = 0.75) for estimating soil organic carbon (SOC) with 20 in-field calibration points. However, this accuracy was not maintained when calibration equations were applied in full-field mapping. Laboratory data collection showed that a sensor with different wavelength bands might provide more accurate results, but this would need to be verified with a wider range of soils.
This book reports on developments in Proximal Soil Sensing (PSS) and high resolution digital soil mapping. PSS has become a multidisciplinary area of study that aims to develop field-based techniques for collecting information on the soil from close by, or within, the soil. Amongst others, PSS involves the use of optical, geophysical, electrochemical, mathematical and statistical methods. This volume, suitable for undergraduate course material and postgraduate research, brings together ideas and examples from those developing and using proximal sensors and high resolution digital soil maps for applications such as precision agriculture, soil contamination, archaeology, peri-urban design and high land-value applications, where there is a particular need for high spatial resolution information. The book in particular covers soil sensor sampling, proximal soil sensor development and use, sensor calibrations, prediction methods for large data sets, applications of proximal soil sensing, and high-resolution digital soil mapping. Key themes: soil sensor sampling – soil sensor calibrations – spatial prediction methods – reflectance spectroscopy – electromagnetic induction and electrical resistivity – radar and gamma radiometrics – multi-sensor platforms – high resolution digital soil mapping - applications Raphael A. Viscarra Rossel is a scientist at the Commonwealth Scientific and Industrial Research Organisation (CSIRO) of Australia. Alex McBratney is Pro-Dean and Professor of Soil Science in the Faculty of Agriculture Food & Natural Resources at the University of Sydney in Australia. Budiman Minasny is a Senior Research Fellow in the Faculty of Agriculture Food & Natural Resources at the University of Sydney in Australia.
At a time when computerized laboratory automation is producing a da ta explosion, chemists are turning to applied mathematics and statistics for the tools to extract useful chemical information from data. This rush to find applicable methods has lead to a somewhat confusing body of literature that represents a barrier to chemists wishing to learn more about chemometrics. The confusion results partly from the mixing of chemical notation and nomenclature with those of statistics, applied mathematics and engineering. Additionally, in the absence of collaboration with mathematicians, chemists have, at times, misused data analysis methodology and even reinvented methods that have seen years of service in other fields. The Chemometrics Society has worked hard to solve this problem since it was founded in 1974 with the goal of improving communications between the chemical sciences and applied mathe matics and statistics. The NATO Advanced Study Institute on Chemometrics is evidence of this fact as it was initiated in response to a call from its membership for advanced training in several areas of chemometrics. This Institute focused on current theory and application in the new field of Chemometrics: Use of mathematical and statistical methods, Ca) to design or select optimal measurement procedures and experiments; and Cb) to provide maximum chemical information by analyzing chemical data. The Institute had two formal themes and two informal themes.
This book presents the basic concepts of quantitative soil science and, within this framework, it seeks to construct a new body of knowledge. There is a growing need for quantitative approach in soil science, which arises from a general demand for improved economic production and environmental management. Pedometrics can be defined as the development and application of statistical and mathematical methods applicable to data analysis problems in soil science. This book shows how pedometrics can address key soil-related questions from a quantitative point of view. It addresses four main areas which are akin to the problems of conventional pedology: (i) Understanding the pattern of soil distribution in character space – soil classification, (ii) Understanding soil spatial and temporal variation, (iii) Evaluating the utility and quality of soil and ultimately, (iv) Understanding the genesis of soil. This is the first book that address these problems in a coherent quantitate approach.
The best single reference for both the theory and practice of soil physical measurements, Methods, Part 4 adopts a more hierarchical approach to allow readers to easily find their specific topic or measurement of interest. As such it is divided into eight main chapters on soil sampling and statistics, the solid, solution, and gas phases, soil heat, solute transport, multi-fluid flow, and erosion. More than 100 world experts contribute detailed sections.
Over the past few decades, exciting developments have taken place in the field of near-infrared spectroscopy (NIRS). This has been enabled by the advent of robust Fourier transform interferometers and diode array solutions, coupled with complex chemometric methods that can easily be executed using modern microprocessors. The present edited volume intends to cover recent developments in NIRS and provide a broad perspective of some of the challenges that characterize the field. The volume comprises six chapters overall and covers several sectors. The target audience for this book includes engineers, practitioners, and researchers involved in NIRS system design and utilization in different applications. We believe that they will greatly benefit from the timely and accurate information provided in this work.