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High purity uranium compounds were needed for precision calorimetric investigations being conducted by the Chemical Engineering Division of the Argonne National Laboratory. Because these compounds could not be commercially obtained in the necessary purity and stoichiometry, they must be specially prepared and analyzed; this program was initiated for that purpose. The purity and stoichiometry were to be established by chemical analysis and X-ray diffraction. The objectives of the project were to explore methods of preparation, and to prepare 500-gram samples of compounds from the following: UAl3, UAl4, UBe13, UB2, UB4, UB12, UC, U2C3, UC2, UN, UN2, US, US2, USi, USi2, USi3, USe2, and UTe. Actually, fourteen of these were prepared, plus UAl2. Small samples of USe and USe2 were prepared, and numerous attempts were made to prepare USi.
This publication presents additional refractory-ceramic property data to supplement those published in the first edition of the Materials Selection Handbook, Is sued in October, 1963, as RTD-TDR-63-4102. The materials covered are nonmetallic inorganic crystalline materials with melting points above 273 deg F (150 deg C), including intermetallic compounds and excluding glass, carbon, and graphite. The data are from literature published in 1961 and 1962. This technical documentary report has been reviewed and is approved.