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Preparation and Characterization of Materials brings together the proceedings of the Indo-U.S. Workshop on the Preparation and Characterization of Materials, held on February 19-23, 1981, at the Indian Institute of Science in Bangalore, India. The papers focus on advances and developments in the preparation and characterization of materials such as ferroics, layered materials, metal oxides and other electronic materials, amorphous materials including glasses, and high-temperature ceramics. This book is comprised of 25 chapters and begins with a discussion on crystal growth and other preparation techniques, touching on topics such as solid state synthesis of complex oxides and preparation of soft ferrites. The application of neutron scattering techniques and analytical electron microscopy to materials research and materials science is then considered, along with the dielectric and electro-optic applications of ferroics and the preparation and characterization of synthetic layered inorganic ion exchangers. Subsequent chapters deal with metal oxides and other electronic materials; glasses and other amorphous materials; and high-temperature ceramics such as silicon nitride. This monograph will be of interest to materials scientists and engineers as well as students and researchers in materials science.
The field of molecular materials research looks at the preparation and characterization of potentially useful materials with enhanced physical, chemical, and biomedical properties. Molecular Materials: Preparation, Characterization, and Applications discusses the cutting-edge interdisciplinary research in the area of advanced molecular-based materials. This book explores multiple aspects of molecular materials, including their synthesis and characterization, and gives information on their application in various fields.
This book focuses on the widely used experimental techniques available for the structural, morphological, and spectroscopic characterization of materials. Recent developments in a wide range of experimental techniques and their application to the quantification of materials properties are an essential side of this book. Moreover, it provides concise but thorough coverage of the practical and theoretical aspects of the analytical techniques used to characterize a wide variety of functional nanomaterials. The book provides an overview of widely used characterization techniques for a broad audience: from beginners and graduate students, to advanced specialists in both academia and industry.
Comprising two volumes, Thermoelectrics and Its Energy Harvesting reviews the dramatic improvements in technology and application of thermoelectric energy with a specific intention to reduce and reuse waste heat and improve novel techniques for the efficient acquisition and use of energy. This volume, Modules, Systems and Applications in Thermoelectrics, discusses the practical, novel, and truly groundbreaking applications of thermoelectrics in a range of markets. The book details the U.S. interest in alternative energy and energy harvesting, specifically, the current efforts to use thermoelectric generators (TGs) to reduce emissions. Internationally, it expounds on the strong interest in Japan, Korea and Europe to incorporate TGs in cars to reduce fuel consumption and meet EU carbon dioxide emission targets; the European plans to build an isotopic powered thermoelectric generator; and India’s use of TG s in converting hot water from steel mills into electricity.
"A thoroughly updated and expanded new edition, this work features a logical, detailed, and self-contained coverage of the latest materials characterization techniques. Reflecting the enormous progress in the field since the last edition, this book details a variety of new powerful and accessible tools, improvements in methods arising from new instrumentation and approaches to sample preparation, and characterization techniques for new types of materials, such as nanomaterials. Researchers in materials science and related fields will be able to identify and apply the most appropriate method in their work"--
Chemical Analysis and Material Characterization by Spectrophotometry integrates and presents the latest known information and examples from the most up-to-date literature on the use of this method for chemical analysis or materials characterization. Accessible to various levels of expertise, everyone from students, to practicing analytical and industrial chemists, the book covers both the fundamentals of spectrophotometry and instrumental procedures for quantitative analysis with spectrophotometric techniques. It contains a wealth of examples and focuses on the latest research, such as the investigation of optical properties of nanomaterials and thin solid films. - Covers the basic analytical theory that is essential for understanding spectrophotometry - Emphasizes minor/trace chemical component analysis - Includes the spectrophotometric analysis of nanomaterials and thin solid films - Thoroughly describes methods and uses easy-to-follow, practical examples and experiments
This book covers state-of-the-art techniques commonly used in modern materials characterization. Two important aspects of characterization, materials structures and chemical analysis, are included. Widely used techniques, such as metallography (light microscopy), X-ray diffraction, transmission and scanning electron microscopy, are described. In addition, the book introduces advanced techniques, including scanning probe microscopy. The second half of the book accordingly presents techniques such as X-ray energy dispersive spectroscopy (commonly equipped in the scanning electron microscope), fluorescence X-ray spectroscopy, and popular surface analysis techniques (XPS and SIMS). Finally, vibrational spectroscopy (FTIR and Raman) and thermal analysis are also covered.
Microstructural characterization is usually achieved by allowing some form of probe to interact with a carefully prepared specimen. The most commonly used probes are visible light, X-ray radiation, a high-energy electron beam, or a sharp, flexible needle. These four types of probe form the basis for optical microscopy, X-ray diffraction, electron microscopy, and scanning probe microscopy. Microstructural Characterization of Materials, 2nd Edition is an introduction to the expertise involved in assessing the microstructure of engineering materials and to the experimental methods used for this purpose. Similar to the first edition, this 2nd edition explores the methodology of materials characterization under the three headings of crystal structure, microstructural morphology, and microanalysis. The principal methods of characterization, including diffraction analysis, optical microscopy, electron microscopy, and chemical microanalytical techniques are treated both qualitatively and quantitatively. An additional chapter has been added to the new edition to cover surface probe microscopy, and there are new sections on digital image recording and analysis, orientation imaging microscopy, focused ion-beam instruments, atom-probe microscopy, and 3-D image reconstruction. As well as being fully updated, this second edition also includes revised and expanded examples and exercises, with a solutions manual available at http://develop.wiley.co.uk/microstructural2e/ Microstructural Characterization of Materials, 2nd Edition will appeal to senior undergraduate and graduate students of material science, materials engineering, and materials chemistry, as well as to qualified engineers and more advanced researchers, who will find the book a useful and comprehensive general reference source.
These papers by leading experts look at current methods for synthesizing new materials. The methods presented include chemical vapor deposition synthesis, solution synthesis, pyrolysis and combustion synthesis, and polymer synthesis. Featuring in-depth coverage of ceramic materials, the volume also discusses group III nitrides, fullerenes, and ferroelectrics.
In this concise handbook leading experts give a broad overview of the latest developments in this emerging and fascinating field of nano-sized materials. Coverage includes new techniques for the synthesis of nanoparticles as well as an in-depth treatment of their characterization and chemical and physical properties. The future applications of these advanced materials are also discussed. The wealth of information included makes this an invaluable guide for graduate students as well as scientists in materials science, chemistry or physics - looking for a comprehensive treatment of the topic.