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This revised and updated Second Edition of Polymer Synthesis II continues in the tradition of Volume I in presenting detailed laboratory instructions for the preparation of various polymers. Each chapter is organized by functional groups, and each chapter not only presents preparative methods, but also includes a brief introductory summary, reviews of the very latest journal articles and patents, and safety hazards and precautions. Procedures have been chosen on the basis of safety considerations and ease of being carried out with standard laboratory equipment. This comprehensive treatment of each polymer group makes Polymer Synthesis II an indispensable guide for industrial and academic chemists as well as for students in the field. Covers each polymer class, heavily referencing these with patent literature to illustrate commercial applications Provides new and updated information for each functional group Contains many new preparations, including
This volume, which completes the Second Edition of this widely respected three-volume set, continues the tradition of providing detailed and concise laboratory instructions for the preparation of organic and inorganic polymers. Updates are provided on the preparation of various types of polymers including olefin-sulfur dioxide copolymers, polythioesters, sulfide polymers, polyisocyanates, polyoxyalkylhydroxy compounds, polyvinyl carbazole, polyvinyl acetate, polyallyl esters, and polyvinyl flouride. The procedures were chosen on the basis of safety and to be representative of preparation methods for a general class of polymers. Fundamental and practical information on polymer synthesis is combined with extensive references and reviews of the patent literature. Completes the Second Edition of three-volume set Brings together useful preparative methods for polymers and resins Organized by functional group Includes new polymerization methods
The first English edition of this book was pubUshed in 1971 with the late Prof. Dr. Werner Kern as coauthor. In 1997, for the preparation of the third edition, Prof. Dr. Helmut Ritter joined the team of authors and in 2001 Prof. Dr. Brigitte Voit and Prof. Dr. Matthias Rehahn complemented this team. The change in authors has not altered the basic concept of this 4th edition: again we were not aimed at compiling a comprehensive collection of recipes. In stead, we attempted to reach a broader description of the general methods and techniques for the synthesis, modification, and characterization of macromo- cules, supplemented by 105 selected and detailed experiments and by sufficient theoretical treatment so that no additional textbook be needed in order to under stand the experiments. In addition to the preparative aspects we have also tried to give the reader an impression of the relation of chemical structure and mor phology of polymers to their properties, as well as of areas of their application.
This laboratory manual covers important techniques for polymer synthesis and characterization, and provides newcomers with a comprehensive introduction to the basic principles of highlighted techniques. The reader will benefit from the clear writing style and straightforward approach to fairly complex ideas. The book also provides references that the more advanced reader can use to obtain in-depth explanations of techniques. Polymer Synthesis and Characterization will serve as a useful resource for industrial technicians and researchers in polymer chemistry and physics, material science, and analytical chemistry. Combines the extensive industrial and teaching experience of the authors Introduces the user to the concept of "Good Manufacturing Practice" Presents experiments that are representative of a wide variety of polymerization and characterization methods Includes numerous references for more advanced students, technicians, and researcher
Polymer Syntheses, Volume I presents detailed laboratory instructions for the preparation of polymers by different functional group classes. This book provides the laboratory procedures for the preparation of polymers containing phosphorus in various oxidation states. Organized into 15 chapters, this volume begins with an overview of some selected preparative methods for carrying out the major methods of polymerization in the laboratory. This text then examines the synthesis of phosphonitrilic polymers. Other chapters consider the synthesis of peroxide and hydroperoxide free radical initiators. This book discusses as well the principles involved in the preparation of emulsion polymers, which are applicable to the preparation of polymers of a wide variety of vinyl monomers and many copolymerizations. The final chapter deals with the chemistry of organometallic and organometalloid peroxides. This book is a valuable resource for chemists involved in the designing of phosphorus polymers to meet fire retardant requirements of various products.
Covering a broad range of polymer science topics, Handbook of Polymer Synthesis, Characterization, and Processing provides polymer industry professionals and researchers in polymer science and technology with a single, comprehensive handbook summarizing all aspects involved in the polymer production chain. The handbook focuses on industrially important polymers, analytical techniques, and formulation methods, with chapters covering step-growth, radical, and co-polymerization, crosslinking and grafting, reaction engineering, advanced technology applications, including conjugated, dendritic, and nanomaterial polymers and emulsions, and characterization methods, including spectroscopy, light scattering, and microscopy.
How can a scientist or engineer synthesize and utilize polymers to solve our daily problems? This introductory text, aimed at the advanced undergraduate or graduate student, provides future scientists and engineers with the fundamental knowledge of polymer design and synthesis to achieve specific properties required in everyday applications. In the first five chapters, this book discusses the properties and characterization of polymers, since designing a polymer initially requires us to understand the effects of chemical structure on physical and chemical characteristics. Six further chapters discuss the principles of polymerization reactions including step, radical chain, ionic chain, chain copolymerization, coordination and ring opening. Finally, material is also included on how commonly known polymers are synthesized in a laboratory and a factory. This book is suitable for a one semester course in polymer chemistry and does not demand prior knowledge of polymer science.
Photoinitiating systems for polymerization reactions are largely encountered in a variety of traditional and high-tech sectors, such as radiation curing, (laser) imaging, (micro)electronics, optics, and medicine. This book extensively covers radical and nonradical photoinitiating systems and is divided into four parts: * Basic principles in photopolymerization reactions * Radical photoinitiating systems * Nonradical photoinitiating systems * Reactivity of the photoinitiating system The four parts present the basic concepts of photopolymerization reactions, review all of the available photoinitiating systems and deliver a thorough description of the encountered mechanisms. A large amount of experimental and theoretical data has been collected herein. This book allows the reader to gain a clear understanding by providing a general discussion of the photochemistry and chemistry involved. The most recent and exciting developments, as well as the promising prospects for new applications, are outlined.
Polymer Syntheses, Volume III provides useful polymer synthesis information. The book discusses the olefin-sulfur dioxide copolymers; the polythioesters; and sulphide polymers. The text also describes polymerizations reactions of mono and diisocyanates; polyoxyalkylation of hydroxyl compounds; and polymerization reactions of N-vinyl carbazole and related monomers. The polymerization of vinyl acetate and other vinyl esters; the polymerization of allyl esters; and the polymerization of vinyl fluoride are also considered. The book further tackles miscellaneous polymer preparations.
A relatively compact, but nonetheless comprehensive, review of the most important preparative methods for the synthesis and chemical modification of polymers. The contents are subdivided according to chemical structure of the polymer backbone. Complementary emphasis is on special properties and appl