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This report presents a cost analysis of Polyethylene Furanoate (PEF) production starting from raw sugar and monoethylene glycol (MEG). The process examined is similar to the Avantium YXY process, followed by a process that copolymerizes FDCA and MEG. In this process, a raw sugar (sucrose) is inverted to glucose and fructose. The glucose is isomerized to fructose. Then, fructose is converted to methoxy methyl furan (MMF) intermediate, which is oxidized to FDCA. This process generates methyl acetate and methyl levulinate as by-products. The FDCA generated and MEG are polymerized to PEF in two polymerization steps in order to obtain Bottle-Grade PEF. This report was developed based essentially on the following reference(s): (1) US Patent 8519167, issued to Furanix Technologies B.V. in 2013 (2) US Patent 20160024039, issued to Furanix Technologies B.V. in 2016 (3) WO Patent 2015137807, issued to Furanix Technologies in 2015 Keywords: Polyethylene Furanoate, PEF, Green FDCA, Hydroxyl Methyl Furfural, HMF, Purified Terephthalic Acid, Polyethylene 2,5-Furandicarboxylate, MEG
This report presents a cost analysis of Polyethylene Furanoate (PEF) production starting from glucose and monoethylene glycol (MEG). The process examined is similar to the Avantium YXY process, followed by a process that copolymerizes FDCA and MEG. In this process, a 70 wt% glucose-water syrup feed is isomerized to fructose. Then, fructose is converted to methoxy methyl furan (MMF) intermediate, which is oxidized to FDCA. This process generates methyl acetate and methyl levulinate as by-products. The FDCA generated and MEG are polymerized to PEF in two polymerization steps in order to obtain Bottle-Grade PEF. This report was developed based essentially on the following reference(s): (1) US Patent 8519167, issued to Furanix Technologies B.V. in 2013 (2) US Patent 20160024039, issued to Furanix Technologies B.V. in 2016 (3) WO Patent 2015137807, issued to Furanix Technologies in 2015 Keywords: Polyethylene Furanoate, PEF, Green FDCA, Hydroxyl Methyl Furfural, HMF, Purified Terephthalic Acid, Polyethylene 2,5-Furandicarboxylate, MEG
This report presents a cost analysis of Polyethylene Furanoate (PEF) production from monoethylene glycol (MEG) and 2,5-furandicarboxylic acid (FDCA). In this process, FDCA and MEG are polymerized to PEF in two polymerization steps in order to obtain Bottle-Grade PEF: melt-phase polymerization and solid-state polymerization. This report was developed based essentially on the following reference(s): (1) WO Patent 2015137807, issued to Furanix Technologies in 2015 (2) US Patent 6749821 issued to UOP in 2004 Keywords: Polyethylene Furanoate, Polyethylene 2,5-Furandicarboxylate, PEF, Green PEF, FDCA, MEG
This report presents a cost analysis of Polytrimethylene Terephthalate (PTT) production starting from raw sugar and terephthalic acid. The process examined combines a process similar to DuPont process for generating propanediol and a process similar to Degussa (now Evonik) process for producing PTT. In this process, raw sugar (sucrose) is diluted and sucrose is hydrolyzed into glucose and fructose (invert sugars). The invert sugars are then fermented to produce Propanediol. This report was developed based essentially on the following reference(s): Keywords: 1,3-Polypropylene Terephthalate, TPA, Dimethyl Terephthalate, DMT, Bio-PDO, Trimethylene Glycol, PTT, Aerobic Fermentation
This report presents a cost analysis of 2,5-Furandicarboxylic Acid (FDCA) production from raw sugar (sucrose). The process examined is a non-commercial route based concepts presented on recently published patents and articles. In this process, sucrose is hydrolyzed into glucose and fructose and the glucose obtained is isomerized into fructose. The resulting fructose is dehydrated to hydroxymethylfurfural (HMF) in ionic liquid medium, which is then oxidized to FDCA. This report was developed based essentially on the following reference(s): (1) DE Patent 102008009933, issued to Friedrich-Schiller-Universitat Jena, in 2009 (2) US Patent 20140256964 issued to Eastman in 2014 Keywords: Green FDCA, Hydroxyl Methyl Furan, HMF, ionic liquid
This report presents a cost analysis of Invert Sugar Syrup production from raw sugar (sucrose) using a sucrose inversion process. The process examined is similar to European Sugar Holdings S.A.R.L. process. In this process, raw sugar (sucrose) is diluted and sucrose is hydrolyzed into glucose and fructose (invert sugar). This inversion reaction occurs in an ion-exchange resin bed. This report was developed based essentially on the following reference(s): US Patent 8404109, issued to European Sugar Holdings in 2013 Keywords: Liquid Sugar, Liquid Invert, Dextrose, Cation-Exchange, IX
This report presents a cost analysis of Polyethylene Terephthalate (PET) production from ethylene glycol and purified terephthalic acid (PTA). The process examined is similar to Invista NG3 process. In this process, PET oligomers are first polymerized in a melt-phase step, and then passed through a solid-state polymerization step. This report was developed based essentially on the following reference(s): US Patents 5786443 and 5730913, both issued to DuPont in 1998 (both assigned to Invista in 2004) Keywords: Thermoplastic Polymer, Polyester, High Intrinsic Viscosity, Melt-Phase Polycondensation