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Small-angle scattering (SAS) is the premier technique for the characterization of disordered nanoscale particle ensembles. SAS is produced by the particle as a whole and does not depend in any way on the internal crystal structure of the particle. Since the first applications of X-ray scattering in the 1930s, SAS has developed into a standard metho
Particle characterization is an important component in product research and development, manufacture, and quality control of particulate materials and an important tool in the frontier of sciences, such as in biotechnology and nanotechnology. This book systematically describes one major branch of modern particle characterization technology - the light scattering methods. This is the first monograph in particle science and technology covering the principles, instrumentation, data interpretation, applications, and latest experimental development in laser diffraction, optical particle counting, photon correlation spectroscopy, and electrophoretic light scattering. In addition, a summary of all major particle sizing and other characterization methods, basic statistics and sample preparation techniques used in particle characterization, as well as almost 500 latest references are provided. The book is a must for industrial users of light scattering techniques characterizing a variety of particulate systems and for undergraduate or graduate students who want to learn how to use light scattering to study particular materials, in chemical engineering, material sciences, physical chemistry and other related fields.
Engineering of nanophase materials and devices is of vital interest in electronics, semiconductors and optics, catalysis, ceramics and magnetism. Research associated with nanoparticles has widely spread and diffused into every field of scientific research, forming a trend of nanocrystal engineered materials. The unique properties of nanophase materials are entirely determined by their atomic scale structures, particularly the structures of interfaces and surfaces. Development of nanotechnology involves several steps, of which characterization of nanoparticles is indespensable to understand the behavior and properties of nanoparticles, aiming at implementing nanotechnolgy, controlling their behavior and designing new nanomaterials systems with super performance. The book will focus on structural and property characterization of nanocrystals and their assemblies, with an emphasis on basic physical approach, detailed techniques, data interpretation and applications. Intended readers of this comprehensive reference work are advanced graduate students and researchers in the field, who are specialized in materials chemistry, materials physics and materials science.
This book explores generalized Lorenz–Mie theories when the illuminating beam is an electromagnetic arbitrary shaped beam relying on the method of separation of variables. The new edition includes an additional chapter covering the latest advances in both research and applications, which are highly relevant for readers. Although it particularly focuses on the homogeneous sphere, the book also considers other regular particles. It discusses in detail the methods available for evaluating beam shape coefficients describing the illuminating beam. In addition it features applications used in many fields such as optical particle sizing and, more generally, optical particle characterization, morphology-dependent resonances and the mechanical effects of light for optical trapping, optical tweezers and optical stretchers. Furthermore, it provides various computer programs relevant to the content.
This reference details particle characterization, dynamics, manufacturing, handling, and processing for the employment of multiphase reactors, as well as procedures in reactor scale-up and design for applications in the chemical, mineral, petroleum, power, cement and pharmaceuticals industries. The authors discuss flow through fixed beds, elutriation and entrainment, gas distributor and plenum design in fluidized beds, effect of internal tubes and baffles, general approaches to reactor design, applications for gasifiers and combustors, dilute phase pneumatic conveying, and applications for chemical production and processing. This is a valuable guide for chemists and engineers to use in their day-to-day work.
Increasing possibilities of computer-aided data processing have caused a new revival of optical techniques in many areas of mechanical and chemical engi neering. Optical methods have a long tradition in heat and mass transfer and in fluid dynamics. Global experimental information is not sufficient for de veloping constitution equations to describe complicated phenomena in fluid dynamics or in transfer processes by a computer program. Furthermore, a detailed insight with high local and temporal resolution into the thermo and fluiddynamic situations is necessary. Sets of equations for computer program in thermo dynamics and fluid dynamics usually consist of two types of formulations: a first one derived from the conservation laws for mass, energy and momentum, and a second one mathematically modelling transport processes like laminar or turbulent diffusion. For reliably predicting the heat transfer, for example, the velocity and temperature field in the boundary layer must be known, or a physically realistic and widely valid correlation describing the turbulence must be avail able. For a better understanding of combustion processes it is necessary to know the local concentration and temperature just ahead of the flame and in the ignition zone.
The Lorenz-Mie theory, describing the interaction between a homogeneous sphere and an electromagnetic plane wave, is likely to be one of the most famous theories in light scattering. But, with the advent of lasers and their increasing development in various fields, it has become too old-fashioned to meet most of the modern requisites. The book deals with generalized Lorenz-Mie theories when the illuminating beam is an electromagnetic arbitrary shaped beam, relying on the method of separation of variables. A particular emphasis is stressed on the case of the homogeneous sphere but other regular particles are considered too. An extensive discussion of the methods available to the evaluation of beam shape coefficients describing the illuminating beam is provided, and several methods are discussed. Applications concern many fields such as optical particle sizing and, more generally, optical particle characterization, morphology-dependent resonances, or mechanical effects of light for optical trapping, optical tweezers and optical stretchers. Various computer programs relevant to the contents of the book are furthermore provided.
The 2013 Materials Science eBook Sampler includes select material from seven Materials Science titles. Titles are from a number of Wiley imprints including Wiley, Wiley-VCH, Wiley-American Ceramic Society, Wiley-Scrivener and Wiley-The Minerals, Metals and Materials Society. The material that is included for each selection is the book’s full Table of Contents as well as a sample chapter. If you would like to read more from these books, you can purchase the full book or e-book at your favorite online retailer.
In fluid mechanics, non-intrusive measurements are fundamental in order to improve knowledge of the behavior and main physical phenomena of flows in order to further validate codes. The principles and characteristics of the different techniques available in laser metrology are described in detail in this book. Velocity, temperature and concentration measurements by spectroscopic techniques based on light scattered by molecules are achieved by different techniques: laser-induced fluorescence, coherent anti-Stokes Raman scattering using lasers and parametric sources, and absorption spectroscopy by tunable laser diodes, which are generally better suited for high velocity flows. The size determination of particles by optical means, a technique mainly applied in two-phase flows, is the subject of another chapter, along with a description of the principles of light scattering. For each technique the basic principles are given, as well as optical devices and data processing. A final chapter reminds the reader of the main safety precautions to be taken when using powerful lasers.
This book describes and illustrates metal spray and spray deposition from the process engineering, metallurgical, and application viewpoints. The authors include step-by-step fundamental information for the metal spray process and detail current engineering developments and applications. They offer industry insight on non-equilibrium solidification processes for yielding stable metal structures and properties.