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For my past sins, Leslie Ettre has given me the privilege of writing a few words to preface his excellent little book. It gives me great pleasure to do so, because of the many years of fruitful collabo ration we have had at Perkin-Elmer, because it is refreshing to see a treatise in gas chromatography in which the theoretical treatment has been bared to its essentials, without a mushrooming of formulae which, by means of an ever increasing number of parameters, account for more and more, and explain less and less, and because the author has recognized that the gas chromatographic column is a nearly passive element in its own right which deserves to have a treatise written nearly exclusively about it, just as electrical circuit theory can be discussed without elaborate references to vacuum tubes and meters. I wish this conscientiously written volume the success it deserves. M. J. E. GOLAY VII Preface Gas chromatography is a separation technique used primarily in analytical chemistry. Therefore, it is evident that special emphasis should be placed on that particular part of the apparatus in which the separation takes place. This part is the column, the heart of the gas chromatograph. The goal of researchers in the field of gas chromatography has been-from the beginning-to understand the separation process so that they might design columns with the best possible performance. Such investigation led M. J. E.
The need for this second edition is dictated by developments that have occurred in this rapidly changing field and by sins of omission and sins of commission in the first edition. Projections available at the time of this writing indicate that gas chromoatography will remain the world's most widely used analytical technique for some time.
Analytical Gas Chromatography is a free-standing introduction to and guide through the rapidly progressing field of analytical gas chromatography. The book is divided into 10 chapters that cover various aspects of analytical gas chromatography, from most advantageous column type to troubleshooting. The opening chapters of the book discuss the advantages of the open tubular column over the packed column. This topic is followed by significant chapters on various variables in the gas chromatographic process, including sample injection, stationary phase, carrier gas, and installation. The effect of changes in these variables on the solution elution order is also considered. A chapter also examines the influence of instrumental design features, such as excessive or unswept volumes in the flow path; suitability of the detection mode; and speed and fidelity of the data-handling equipment. The book also presents selected methods that have been employed to achieve better results for a given gas chromatographic problem. The application areas of gas chromatographic process, including food, flavor, fragrance, petroleum- and chemical-related, environment, biology, and medicine, are also presented. The concluding chapter addresses the basic troubleshooting knowledge and considers other chromatographic problems and methods for their rectification.
New York : Wiley, c1984.
The primary aim of this volume is to make the chemist familiar with the numerous stationary phases and column types, with their advantages and disadvantages, to help in the selection of the most suitable phase for the type of analytes under study. The book also provides detailed information on the chemical structure, physico-chemical behaviour, experimental applicability, physical data of liquid and solid stationary phases and solid supports. Such data were previously scattered throughout the literature. To understand the processes occurring in the separation column and to offer a manual both to the beginner and to the experienced chromatographer, one chapter is devoted to the basic theoretical aspects. Further, as the effectiveness of the stationary phase can only be considered in relation to the column type, a chapter on different column types and the arrangement of the stationary phase within the column is included.The secondary aim of this book is to stimulate the development of new and improved standardized stationary phases and columns, in order to improve the reproducibility of separations, as well as the range of applications.
The method of choice for analysis of organic pollutants in the environ­ ment is gas chromatography, using one of the most common detection systems such as flame ionization, electron capture, and mass spectro­ metric detection. Perhaps the most prevalent difference in practice among the envi­ ronmental analytical chemists involves the type of column used in gas chromatography. The traditional packed-column gas chromatography is rapidly being replaced with wall-coated open tubular (WCOT) columns. However, in using WCOT columns there are difficulties in reporting analytical data and the means of quantitation. This book is intended to present a survey of the salient features of WCOT column gas chromatography that relate to the selection ofWCOT columns, their technology, separation efficiency, and determination of the principal groups of organic micropollutants, such as hydrocarbons, aromatics, polynuclear aromatic hydrocarbons, organochlorine pollu­ tants, chlorinated phenols, dioxins, dibenzofurans, ureas, carbamates, and odor-causing substances in complex environmental matrices. Hence, it is the hope of the authors that the content of this book will be of significance to a wide spectrum of disciplines that include environmental chemistry, industrial hygiene and health, toxicology, genetics, and in­ dustry.
The New Edition of the Well-Regarded Handbook on Gas Chromatography Since the publication of the highly successful first edition of Basic Gas Chromatography, the practice of chromatography has undergone several notable developments. Basic Gas Chromatography, Second Edition covers the latest in the field, giving readers the most up-to-date guide available, while maintaining the first edition's practical, applied approach to the subject and its accessibility to a wide range of readers. The text provides comprehensive coverage of basic topics in the field, such as stationary phases, packed columns and inlets, capillary columns and inlets, detectors, and qualitative and quantitative analysis. At the same time, the coverage also features key additions and updated topics including: Gas chromatography-mass spectrometry (GC-MS) Sampling methods Multidimensional gas chromatography Fast gas chromatography Gas chromatography analysis of nonvolatile compounds Inverse gas chromatography and pyrolysis gas chromatography Along with these new and updated topics, the references, resources, and Web sites in Basic Gas Chromatography have been revised to reflect the state of the field. Concise and fundamental in its coverage, Basic Gas Chromatography, Second Edition remains the standard handbook for everyone from undergraduates studying analytical chemistry to working industrial chemists.
This book provides up-to-date information on a wide range of developments in chromatographic methods and applications. It also presents timely, cutting-edge reviews in the fields of bio-, analytical, organic, polymer, and pharmaceutical chemistry.