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Among the topics of interest to organic chemists today are the versatility and uniqueness of electrolysis procedures in organic synthesis, as well as the latest advances in methodology, including basic concepts for the design of electrolysis conditions and apparatus. The International Symposium on Electroorganic Synthesis met in Kurashiki, Japan, in September 1997 for lectures on all aspects of current research in the field. This volume comprising the papers from the symposium consists of two parts. Part I, Electrooxidation, includes papers on alcohols and phenols, olefins and aromatics, halogenation, polymers, and electrodes, among others. Included in Part II, Electroreduction, are papers on carbonyl compounds, halogen-containing compounds, reaction with EG bases, and metal complexes. The novel trends presented here will be of special interest to researchers and graduate students in electroorganic chemistry and are a valuable resource for all organic chemists.
This monograph will clearly depict much of the current, leading research into the reactions and properties of organic and bioorganic materials in which electron transfer plays an important role. Organic electrochemistry is increasingly expanding to various interdisciplinary fields and is of major interest to a growing number of researchers and engineers. The contents of this book emphasize the scope of the reaction field at the electrode interface, specifically, electrogenerated active species, new mediatory reactions, and new trends in organic electrochemistry. Many of the results demonstrated in these reports may have broad applications to the development of science and new technologies. The twenty contributing authors are all active researchers in organic electrochemistry, bioelectrochemistry, electrocoordination chemistry, or electroanalytical chemistry.
Modern Synthesis Processes and Reactivity of Fluorinated Compounds focuses on the exceptional character of fluorine and fluorinated compounds. This comprehensive work explores examples taken from all classes of fluorine chemistry and illustrates the extreme reactivity of fluorinating media and the peculiar synthesis routes to fluorinated materials. The book provides advanced and updated information on the latest synthesis routes to fluorocompounds and the involved reaction mechanisms. Special attention is given to the unique reactivity of fluorine and fluorinated media, along with the correlation of those properties to valuable applications of fluorinated compounds. Contains quality content edited, and contributed, by leading scholars in the field Presents applied guidance on the preparation of original fluorinated compounds, potentially transferable from the lab scale to industrial applications Provides practical synthesis information for a wide audience interested in fluorine compounds in many branches of chemistry, materials science, and physics
Practical Aspects of Electroorganic Synthesis presents educational insights into the practical aspects of electrosynthesis methods, providing a variety of examples and techniques. The book covers concepts referred to as "green chemistry" and "sustainable technology." Sections cover direct electrolysis, anodic oxidation, cathodic reduction, mechanistic studies (cyclic voltammetry), and how to set-up electrochemical experiments. Indirect electrolysis is also covered, including an exploration of catalysts and additives to take on modern electrochemical methods. Finally, the book explores the burgeoning new field of paired electrolysis, in which the ultimate green-synthesis applications are possible, with no wasted electrons and very few by-products. This book offers researchers a modern and authoritative resource that brings complete and up-to-date practical concepts of electrosynthesis methods and guides the audience on how to carry out a large number of experimental techniques. Discusses complete and up-to-date practical concepts of electrosynthesis methods Provides sound insights into the experimental approaches of electrosynthesis, covering new and novel synthesis techniques Breaks down the fundamentals aspects of electrolysis into three digestible and logical sections
A presentation of developments in the electrochemistry of C60 and related compounds, electroenzymatic synthesis, conducting polymers, and electrochemical partial fluorination. It contains accounts of carbonyl compounds, anodic oxidation of oxygen-containing compounds, electrosynthesis of bioactive materials, electrolyte reductive coupling, and more.