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Packed bed columns are largely employed for absorption, desorption, rectification and direct heat transfer processes in chemical and food industry, environmental protection and also processes in thermal power stations like water purification, flue gas heat utilization and SO2 removal. These Separation processes, are estimated to account for 40%-70% of capital and operating costs in process industry. Packed bed columns are widely employed in this area. Their usage also for direct heat transfer between gas and liquid, enlarge their importance. They are the best apparatuses, from thermodynamical point of view, for mass and heat transfer processes between gas and liquid phase. Their wide spreading is due to low capital investments and operating costs. Since 1995 there has not been published a specialised book in this area, and this is a period of quick development of packed columns. Packed Bed Columns reflects the state of this field including the author's experience on creating and investigating of new packings, column internals and industrial columns. - Considers the theories of mass transfer processes and shows how they help the construction of highly effective packings - Complete information about the performance characteristics of different modern types of highly effective packings - Considers the models for calculation and areas of their application
The?rstGermanedition of thebook“Fluiddynamicsofpackedcolumns with modern random and structured packings for gas/liquid systems” was published in 1991. It sold out within a few years. Added to this were numerous enquiries, in particular within the industry, prompting me to publish a second, extended edition. A packed column remains the core element of any diffusional separation process. This underlines the need for basic design principles for packed columns, which enhance the design process by making it more accurate and reliable. The SBD (suspended bed of droplets) model introduced in the ?rst German edition of the book was well received by the experts and is now used by a large number of com- nies in the industry, as it offers improved reliability in the ?uid dynamic design of packed columns. For the purpose of facilitating the design process, the SBD model was in- grated into the simulation programme ChemCAD. The software programme FDPAK, which is available for Windows, has certainly contributed to the widespread use of the SBD model. The programme is very user-friendly and the calculation results are p- sented in tabular as well as graphic form, showing ?ood load, pressure drop and hold-up diagrams in the entire operating range.
The phenomenon of "mass transfer with chemical reaction" takes place whenever one phase is brought into contact with one or more other phases not in chemical equilibrium with it. This phenomenon has industrial, biological and physiological importance. In chemical process engineering, it is encountered in both separ ation processes and reaction engineering. In some cases, a chemical reaction may deliberately be employed for speeding up the rate of mass transfer and/or for increasing the capacity of the solvent; in other cases the multiphase reaction system is a part of the process with the specific aim of product formation. Finally, in some cases, for instance "distillation with chemical reaction", both objectives are involved. Although the subject is clearly a chemical engineering undertakin~, it requires often a good understanding of other subjects, such as chemistry and fluid mechanics etc., leading to publications in diversified areas. On the other har.d, the subject has always been a major field and one of the most fruitful for chemical engineers.
The widespread adoption of microreactors has been hindered by a lack of knowledge regarding rules and parameters needed for their design. This dissertation deals with the investigation of interfacial area and liquid mass transport in microreactors for gas/liquid reactions. Observations of a reduction in conversion occurring when changing from a glass laboratory device to a stainless steel process device motivated investigations into the effect of material and surface properties on the gas/liquid flow and reaction. This work takes a look inside the machined microstructures produced at the Institute for Micro Process Engineering of the Karlsruhe Institute of Technology and investigates the nature of the solid surfaces resulting from the machining process—the surface roughness and the contact angle of the resulting surface. The effect of wettability on gas/liquid flow in microreactors has been investigated in capillaries of various materials. The absorption of carbon dioxide into aqueous solutions of sodium hydroxide has been used to investigate gas/liquid flow and reaction in capillaries and in a microstructured falling film reactor. Under certain limiting assumptions depending upon the exact rates of reaction and transport, values of the interfacial area and liquid mass transport coefficient can be derived from measurements of reaction. This dissertation contributes a small step towards a better understanding of how measurements of the interfacial area and mass transfer coefficient can be performed, demonstrates why the effect of material wettability cannot be ignored, and provides a stronger basis for further work in the development of general correlations describing microstructured gas/liquid reactors.
Micro process engineering is approaching both academia and industry. With the provision of micro devices, systems and whole plants by commercial suppliers, one main barrier for using these units has been eliminated. This book focuses on processes and their plants rather than on devices: what is 'before', 'behind' and 'around' micro device fabrication - and gives a comprehensive and detailed overview on the micro-reactor plants and three topic-class applications which are mixing, fuel processing, and catalyst screening. Thus, the book reflects the current level of development from 'micro-reactor design' to 'micro-reactor process design'.
Reviews and compares the major types of bioreactors, defines their pros and cons, and identifies research needs and figures of merit that have yet to be addressed Describes common modes of operation in bioreactors Covers the three common bioreactor types, including stirred-tank bioreactors, bubble column bioreactors, and airlift bioreactors Details less common bioreactors types, including fixed bed bioreactors and novel bioreactor designs Discusses advantages and disadvantages of each bioreactor and provides a procedure for optimal bioreactor selection based on current process needs Reviews the problems of bioreactor selection globally while considering all bioreactor options rather than concentrating on one specific bioreactor type
This complete reference book covers topics in heat and mass transfer, containing extensive information in the form of interesting and realistic examples, problems, charts, tables, illustrations, and more. Heat and Mass Transfer emphasizes practical processes and provides the resources necessary for performing accurate and efficient calculations.This excellent reference comes with a complete set of fully integrated software available for download at crcpress.com, consisting of 21 computer programs that facilitate calculations, using procedures developed in the text. Easy-to-follow instructions for software implementation make this a valuable tool for effective problem-solving.
This book gives a practical account of the modern theory of calculation of absorbers for binary and multicomponent physical absorption and absorption with simultaneous chemical reaction. The book consists of two parts: the theory of absorption and the calculation of absorbers. Part I covers basic knowledge on diffusion and the theory of mass transfer in binary and multicomponent systems. Significant stress is laid on diffusion theory because this forms the basis for the absorption process. In the next chapters the fundamentals of simultaneous mass transfer and chemical reaction, the theory of the desorption of gases from liquids and the formulation of differential mass balances are discussed. Part II is devoted to the calculation of absorbers and the classification of absorbers. The chapters present calculation methods for the basic types of absorber with a detailed analysis of the calculation methods for packed, plate and bubble columns. The authors illustrate the presented material with a large number of examples, starting with simple ones for binary systems and ending with column calculation for multicomponent systems.
The phenomenon of "mass transfer with chemical reaction" takes place whenever one phase is brought into contact with one or more other phases not in chemical equilibrium with it. This phenomenon has industrial, biological and physiological importance. In chemical process engineering, it is encountered in both separ ation processes and reaction engineering. In some cases, a chemical reaction may deliberately be employed for speeding up the rate of mass transfer and/or for increasing the capacity of the solvent; in other cases the multiphase reaction system is a part of the process with the specific aim of product formation. Finally, in some cases, for instance "distillation with chemical reaction," both objectives are involved. Although the subject is clearly a chemical engineering undertakin, it requires often a good understanding of other subjects, such as chemistry and fluid mechanics etc., leading to publications in diversified areas. On the other har.d, the subject has always been a major field and one of the most fruitful for chemical engineers."