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Packed bed columns are largely employed for absorption, desorption, rectification and direct heat transfer processes in chemical and food industry, environmental protection and also processes in thermal power stations like water purification, flue gas heat utilization and SO2 removal. These Separation processes, are estimated to account for 40%-70% of capital and operating costs in process industry. Packed bed columns are widely employed in this area. Their usage also for direct heat transfer between gas and liquid, enlarge their importance. They are the best apparatuses, from thermodynamical point of view, for mass and heat transfer processes between gas and liquid phase. Their wide spreading is due to low capital investments and operating costs. Since 1995 there has not been published a specialised book in this area, and this is a period of quick development of packed columns. Packed Bed Columns reflects the state of this field including the author's experience on creating and investigating of new packings, column internals and industrial columns. - Considers the theories of mass transfer processes and shows how they help the construction of highly effective packings - Complete information about the performance characteristics of different modern types of highly effective packings - Considers the models for calculation and areas of their application
This broad-based book covers the three major areas of Chemical Engineering. Most of the books in the market involve one of the individual areas, namely, Fluid Mechanics, Heat Transfer or Mass Transfer, rather than all the three. This book presents this material in a single source. This avoids the user having to refer to a number of books to obtain information. Most published books covering all the three areas in a single source emphasize theory rather than practical issues. This book is written with emphasis on practice with brief theoretical concepts in the form of questions and answers, not adopting stereo-typed question-answer approach practiced in certain books in the market, bridging the two areas of theory and practice with respect to the core areas of chemical engineering. Most parts of the book are easily understandable by those who are not experts in the field. Fluid Mechanics chapters include basics on non-Newtonian systems which, for instance find importance in polymer and food processing, flow through piping, flow measurement, pumps, mixing technology and fluidization and two phase flow. For example it covers types of pumps and valves, membranes and areas of their use, different equipment commonly used in chemical industry and their merits and drawbacks. Heat Transfer chapters cover the basics involved in conduction, convection and radiation, with emphasis on insulation, heat exchangers, evaporators, condensers, reboilers and fired heaters. Design methods, performance, operational issues and maintenance problems are highlighted. Topics such as heat pipes, heat pumps, heat tracing, steam traps, refrigeration, cooling of electronic devices, NOx control find place in the book. Mass transfer chapters cover basics such as diffusion, theories, analogies, mass transfer coefficients and mass transfer with chemical reaction, equipment such as tray and packed columns, column internals including structural packings, design, operational and installation issues, drums and separators are discussed in good detail. Absorption, distillation, extraction and leaching with applications and design methods, including emerging practices involving Divided Wall and Petluk column arrangements, multicomponent separations, supercritical solvent extraction find place in the book.
Annular Two-Phase Flow presents the wide range of industrial applications of annular two-phase flow regimes. This book discusses the fluid dynamics and heat transfer aspects of the flow pattern. Organized into 12 chapters, this book begins with an overview of the classification of the various types of interface distribution observed in practice. This text then examines the various regimes of two-phase flow with emphasis on the regions of occurrence of the annular flow regime. Other chapters consider the single momentum and energy balances, which illustrate the differences and analogies between single- and two-phase flows. This book discusses as well the simple modes for annular flow with consideration to the calculation of the profile of shear stress in the liquid film. The final chapter deals with the techniques that are developed for the measurement of flow pattern, entrainment, and film thickness. This book is a valuable resource for chemical engineers.
Provides a holistic approach to multiphase catalytic reactors from their modeling and design to their applications in industrial manufacturing of chemicals Covers theoretical aspects and examples of fixed-bed, fluidized-bed, trickle-bed, slurry, monolith and microchannel reactors Includes chapters covering experimental techniques and practical guidelines for lab-scale testing of multiphase reactors Includes mathematical content focused on design equations and empirical relationships characterizing different multiphase reactor types together with an assortment of computational tools Involves detailed coverage of multiphase reactor applications such as Fischer-Tropsch synthesis, fuel processing for fuel cells, hydrotreating of oil fractions and biofuels processing
Miniaturization has cost and time-saving advantages for numerous applications in chemistry, pharmacy, medicine and biotechnology. Additionally, microreaction technology offers new solutions for the automobile industry and environmental technology, e.g. fuel cells, or mobile sensor systems for on-the-spot analysis. Therefore, the 3rd International Conference on Microreaction Technology - IMRET 3 is an important forum for creating awareness of the wide variety of the new trends in this up-and-coming discipline.
Mixed or multiphase flows of solid/liquid or solid/gas are commonly found in many industrial fields, and their behavior is complex and difficult to predict in many cases. The use of computational fluid dynamics (CFD) has emerged as a powerful tool for the understanding of fluid mechanics in multiphase reactors, which are widely used in the chemical, petroleum, mining, food, beverage and pharmaceutical industries. Computational Techniques for Multiphase Flows enables scientists and engineers to the undertand the basis and application of CFD in muliphase flow, explains how to use the technique, when to use it and how to interpret the results and apply them to improving aplications in process enginering and other multiphase application areas including the pumping, automotive and energy sectors. - Understandable guide to a complex subject - Important in many industries - Ideal for potential users of CFD
The widespread adoption of microreactors has been hindered by a lack of knowledge regarding rules and parameters needed for their design. This dissertation deals with the investigation of interfacial area and liquid mass transport in microreactors for gas/liquid reactions. Observations of a reduction in conversion occurring when changing from a glass laboratory device to a stainless steel process device motivated investigations into the effect of material and surface properties on the gas/liquid flow and reaction. This work takes a look inside the machined microstructures produced at the Institute for Micro Process Engineering of the Karlsruhe Institute of Technology and investigates the nature of the solid surfaces resulting from the machining process—the surface roughness and the contact angle of the resulting surface. The effect of wettability on gas/liquid flow in microreactors has been investigated in capillaries of various materials. The absorption of carbon dioxide into aqueous solutions of sodium hydroxide has been used to investigate gas/liquid flow and reaction in capillaries and in a microstructured falling film reactor. Under certain limiting assumptions depending upon the exact rates of reaction and transport, values of the interfacial area and liquid mass transport coefficient can be derived from measurements of reaction. This dissertation contributes a small step towards a better understanding of how measurements of the interfacial area and mass transfer coefficient can be performed, demonstrates why the effect of material wettability cannot be ignored, and provides a stronger basis for further work in the development of general correlations describing microstructured gas/liquid reactors.
The phenomenon of "mass transfer with chemical reaction" takes place whenever one phase is brought into contact with one or more other phases not in chemical equilibrium with it. This phenomenon has industrial, biological and physiological importance. In chemical process engineering, it is encountered in both separ ation processes and reaction engineering. In some cases, a chemical reaction may deliberately be employed for speeding up the rate of mass transfer and/or for increasing the capacity of the solvent; in other cases the multiphase reaction system is a part of the process with the specific aim of product formation. Finally, in some cases, for instance "distillation with chemical reaction", both objectives are involved. Although the subject is clearly a chemical engineering undertakin~, it requires often a good understanding of other subjects, such as chemistry and fluid mechanics etc., leading to publications in diversified areas. On the other har.d, the subject has always been a major field and one of the most fruitful for chemical engineers.