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Introductory Titrimetric and Gravimetric Analysis discusses the different types of titration and the weighing of different solutions in solid form. Coverage is made on acid- base titration, argentometric titrations, and oxidation- reduction titrations. Iodometric titrations and complexometric titrations are also explained. Extensive discussion on each of the titration method, along with some examples and laboratory experiments, is given. The process of weight measurement of damp powder is one example of the experiments. The book is a manual that guides a student to the correct ways of conducting an experiment made on such solutions as sodium hydroxide using hydrochloric acid and oxalic acid. Outcome of such experiments in terms of composition, weight of solutions, and measurement of pressure in certain environment is tabulated and briefly explained. Logarithms and antilogarithms are included at the end of the book. The text will serve as a good laboratory manual for students preparing for science examination as well as for chemists and chemical engineers.
Surpassing its bestselling predecessors, this thoroughly updated third edition is designed to be a powerful training tool for entry-level chemistry technicians. Analytical Chemistry for Technicians, Third Edition explains analytical chemistry and instrumental analysis principles and how to apply them in the real world. A unique feature of this edition is that it brings the workplace of the chemical technician into the classroom. With over 50 workplace scene sidebars, it offers stories and photographs of technicians and chemists working with the equipment or performing the techniques discussed in the text. It includes a supplemental CD that enhances training activities. The author incorporates knowledge gained from a number of American Chemical Society and PITTCON short courses and from personal visits to several laboratories at major chemical plants, where he determined firsthand what is important in the modern analytical laboratory. The book includes more than sixty experiments specifically relevant to the laboratory technician, along with a Questions and Problems section in each chapter. Analytical Chemistry for Technicians, Third Edition continues to offer the nuts and bolts of analytical chemistry while focusing on the practical aspects of training.
Pergamon Series in Analytical Chemistry, Volume 2: Basic Analytical Chemistry brings together numerous studies of the vast expansion in the use of classical and instrumental methods of analysis. This book is composed of six chapters. After providing a theoretical background of analytical chemistry, this book goes on dealing with the fundamental principles of chemical equilibria in solution. The subsequent chapters consider the advances in qualitative and quantitative chemical analyses. These chapters present a unified view of these analyses based on the Bronsted-Lowry theory and the donor-acceptor principle. These topics are followed by discussions on instrumental analysis using various methods, including electrochemical, optical, spectroscopic, and thermal methods, as well as radioactive isotopes. The finals chapters examine the separation methods and the essential features of organic chemical analysis that are different from methods for inorganic compounds. This book is of value to analytical chemists and researchers.
Written as a training manual for chemistry-based laboratory technicians, this thoroughly updated fourth edition of the bestselling Analytical Chemistry for Technicians emphasizes the applied aspects rather than the theoretical ones. The book begins with classical quantitative analysis and follows with a practical approach to the complex world of sophisticated electronic instrumentation commonly used in real-world laboratories. Providing a foundation for the two key qualities—the analytical mindset and a basic understanding of the analytical instrumentation—this book helps prepare individuals for success on the job. Chapters cover sample preparation; gravimetric analysis; titrimetric analysis; instrumental analysis; spectrochemical methods, such as atomic spectroscopy and UV-Vis and IR molecular spectrometry; chromatographic techniques, including gas chromatography and high-performance liquid chromatography; electroanalytical methods; and more. Incorporating an additional ten years of teaching experience since the publication of the third edition, the author has made significant updates and enhancements to the fourth edition. More than 150 new photographs and either new or reworked drawings spanning every chapter to assist the visual learner A new chapter on mass spectrometry, covering GC-MS, LC-MS, LC-MS-MS, and ICP-MS Thirteen new laboratory experiments An introductory section before chapter 1 to give students a preview of general laboratory considerations, safety, laboratory notebooks, and instrumental analysis Additional end-of-chapter problems, expanded "report"-type questions, and inclusion of relevant section headings in the Questions and Problems sections Application Notes in each chapter An appendix providing a glossary of quality assurance and good laboratory practice (GLP) terms
The second edition of Analytical Chemistry for Technicians provides the "nuts and bolts" of analytical chemistry and focuses on the practical aspects for training a technician-level laboratory worker. This edition presents new and expanded chapters, innumerable questions and problems, and modified experiments that present a fresh and challenging approach. Some of the topics that have been expanded include chemical equilibrium, chromatography, Kjeldahl method, and molarity and moles where EDTA and water hardness calculations are concerned. New discussions of the Ag/AgCl and combination pH electrodes have been added, while the discussion of ion-selective electrodes has been expanded. The chapter introducing instrumental analysis and computers now includes discussions of "y = mx + b" and the method of least squares. The book also includes discussions of FTIR, topics of NMR, and mass spectrometry, which are found in the new infrared spectrometry chapter.
Contents: Introduction, Introduction to Laboratory Work, Measurement by Weight, Measurement by Volume, General Remarks on Volumetric Analysis, Evaluation of Analytical Data, pH and Buffers, Solvent Extraction, General Remarks on Gravimetric Methods of Analysis, Radox Titrations, Precipitation Titrations, Complexometric Titrations, Chromatography, Electroanalytical Techniques.