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As is often the case, the preface is the last task to be finished during the preparation of a large volume such as you are now holding. The first task, obtaining approval for a symposium on the industrial applications, now seems a long time ago. The idea orginated with John Stevens, probably in 1982, from his observation of papers dealing with industrial applications of the Mossbauer effect appearing in the Mossbauer Effect Reference and Data Journal. His initial suggestion for a symposium entitled "Industrial Applications of the Mossbauer Effect" to be held at a national meeting of the American Chemical Society eventually led to the symposium at the International Chemical Congress of Pacific Basin Societies which met in Honolulu, Hawaii in December 1984. This volume is the result of the symposium at the above mentioned Congress, but is not actually the 'proceedings' of the symposium because this volume does not contain all of the over one hundred Mossbauer effect papers that were pre sented at the symposium. Rather it contains a selection of papers that the or ganizing committee for the symposium deemed most appropriate for a volume devoted to industrial applications of the Mossbauer effect. The final volume also contains six chapters that were not a part of the symposium but which are closely related to the topic. There is another difference from many proceedings.
Mössbauer Spectroscopy of Environmental Materials and their Industrial Utilization provides a description of the properties of materials formed on the earth's surface, their synthetic analogs where applicable, and the products of their modifications in the course of natural processes, such as weathering, or in industrial processing as reflected in their Mössbauer spectra. Particular emphasis is placed on the way in which these processes can be observed and elucidated through the use of Mössbauer spectroscopy. The first chapter covers the basic theory of the Mössbauer effect and Chapters 2 and 3 deal with the nuts and bolts of experimental Mössbauer spectroscopy. The principles of these first three chapters, illustrated with many case studies, are applied to different areas of interest in Chapters 4 through 12. The book is directed to a broad audience ranging from graduate students in environmental sciences or chemical engineering with little or no expertise in Mössbauer spectroscopy to researchers from other disciplines who are familiar with this technique but wish to learn more about possible applications to environmental materials and issues.
This book is for the most part made up of the invited papers presented at the International Conference on Applica tions of the Kdssbauer effect, held at Aye1eth Hashahar, Israel, in August 1972. The purpose of the conference was to review perspec tives in MHssbauer spectroscopy from the point of view of applications in various fields of science - mainly physics, chemistry, and biology. It was hoped that the bringing together of scientists who work in different disciplines but use a common tool would encourage interdisciplinary re search and widen the horizon of the individual researcher. Both these features have been an important and unique characteristic of Kdssbauer research in the past decade. Accordingly, the main papers were presented in the following areas: magnetic properties of solids, applications to in organic chemistry, biochemical studies, amorphous systems, metal alloys, advances in high-resolution studies, and the new techniques for studying recoil-free spectra from isolated atoms in inert materials. A special panel discussion was devoted to the subject of phase transitions. Recent years have witnessed a rapid growth in the use of X-ray photoelec tron spectroscopy for the study of the physics and chemistry of solids. A report on this area of research and its rela tion to Kdssbauer studies has been included.
Disordered nature of structural arrangement in amorphous and nanocrystalline alloys gives rise to advantageous soft magnetic properties in particular from a practical application viewpoint [1]. Especially nanocrystalline alloys attract a lot of scienti?c interest because, contrary to their amorphous counterparts, their magnetic parameters do not substantially deteriorate at elevated temperatures during the process of their practical exploitation. To bene?t from their unique magnetic pr- erties, the mechanism of crystallization should be known. Here, we present the study of structural transformation of NANOPERM-type alloys by the help of Mössbauer spectrometry, conventional X-ray diffraction (XRD), and by an advanced diffraction of synchrotron radiation. 2 Experimental Alloys of the composition Fe Mo Cu B for x = 12, 15, 17, 20 prepared by 91?x 8 1 x 57 rapid quenching on a rotating wheel were analyzed in the as-cast state by Fe transmission Mössbauer spectrometry (TMS) and by conversion electron Mössbauer spectrometry (CEMS). The obtained as-quenched ribbons were about 10 mm wide and 20 ?m thick. The nanocrystalline state was achieved by annealing about 2 cm ? long samples for 1 h at temperatures up to 650 C in a vacuum. Conventional XRD was performed with Cu-K radiation in Bragg-Brentano con?guration with graphite ? monochromator in the diffracted beam. Monochromatic synchrotron radiation of 7keV(? = 0. 178 nm) provided at the KMC-2 beamline at BESSY Berlin was used for in situ examinations of structural transformations during continuous heat treatment.