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This is the first textbook to present a comprehensive and instructive view of the theory and applications of this growing technique.
The isotope dilution mass spectrometry (IDMS) technique is well known and widely reported in the literature. However, its application can present considerable difficulties with regard to obtaining reliable results. Produced jointly by the Royal Society of Chemistry's Analytical Methods Committee and the Valid Analytical Measurement (VAM) programme, the aim of this book is to provide a simplified yet robust methodology, together with adequate guidance, to enable laboratories wishing to use the technique to obtain reliable data. The methodologies, for inorganic and organic mass spectrometry, which use exact and approximate matching, are illustrated with worked examples and clear diagrammatic representations. A comprehensive glossary of terms, references to key publications and an extensive IDMS bibliography are also provided. Clear and comprehensive in coverage, Guidelines for Achieving High Accuracy in Isotope Dilution Mass Spectrometry (IDMS) will provide valuable assistance to a wide variety of analytical chemists interested in applying the IDMS technique to their own measurement applications.
Isotope Dilution Mass Spectrometry (IDMS) has become an essential tool in research laboratories and is increasingly used in routine analysis labs (including environmental, food safety and clinical applications). This is the first textbook to present a comprehensive and instructive view of the theory and applications of this growing technique. The main objective of this book is to cover the theory and applications of Isotope Dilution in Analytical Chemistry. The scope is comprehensive to include elemental analysis, speciation analysis, organic analysis and biochemical and clinical analysis together with applications in metabolism studies and traceability of goods. Until now there have been no books published with the same general scope (only book chapters on particular applications). This is a textbook focused at post-graduate level covering the basic knowledge required for doctoral studies in this field. Isotope Dilution Mass Spectrometry will also outline practical applications of interest for routine testing laboratories where isotope dilution procedures are implemented or can be implemented in the future. This unique book covers all the theoretical and practical aspects of Isotope Dilution Mass Spectrometry (IDMS). Due to the increasing application of IDMS in many research laboratories and the increasing implementation of IDMS methodologies in routine testing laboratories, scientists in industry and working in or affiliated to this area will this an invaluable source of information. Concerning the theoretical aspects, the authors present a uniform theoretical background which grows from previous developments in Organic, Speciation and Elemental analysis both in their own laboratory and in other laboratories around the world. This general approach will be simpler and will also include new emerging fields such as quantitative proteomics and metabolism studies.
Offers a complete overview of the principles, theories and key applications of modern mass spectrometry in this introductory textbook. Following on from the highly successful first edition, this edition is extensively updated including new techniques and applications. All instrumental aspects of mass spectrometry are clearly and concisely described; sources, analysers and detectors. * Revised and updated * Numerous examples and illustrations are combined with a series of exercises to help encourage student understanding * Includes biological applications, which have been significantly expanded and updated * Also includes coverage of ESI and MALDI
Determination of Toxic Organic Chemicals in Natural Waters, Sediments and Soils: Determination and Analysis reviews the latest techniques for the determination and assessment of both current and emerging organic compounds in a range of important environmental contexts. A wide range of organic compounds in non-saline waters are discussed in the opening chapters, including hydrocarbons, surface active agents and volatile organic compounds. This is followed by multiorganics, pesticides and organometallic compounds in non-saline waters. Organic compounds in aqueous precipitation are then explored before the book goes on to discuss compounds in soils, including extraction techniques, insecticides, herbicides and fungicides, and organometallic compounds. Finally, the concluding chapters focus on compounds in sediments, providing readers with the latest information in the field and supporting them as they address the important issue surrounding organic material throughout ecosystems. - Highlights the latest methods for analyzing a wide range of organic compounds - Supports researchers by providing detailed information across a range of ecosystems - Includes detailed guidance for assessing complex mixtures of organic compounds in the environment
This work provides detailed coverage of the applications of proven spectometric techniques in soil science. It presents analytical approaches important in the study of pool sizes and the dynamics of macro- and micronutrients, the structure and function of soil organic matter, and the co-evolution of soils, plant communities and climate. Interdisciplinary perspectives from soil science, ecology, geology, chemistry, biogeochemistry, agronomy and physics, are offered.
Written by an internationally recognized group of editors and contributors, Handbook of Elemental Speciation, Volume 2 provides a comprehensive, cross-disciplinary presentation of the analytical techniques involved in speciation. Comprehensive coverage of key elements and compounds in situ Addresses the analysis and impact of these elements and compounds, e.g. arsenic, lead, copper, iron, halogens, etc., in food, the environment, clinical and occupational health Detailed methodology and data are reported, as well as regulatory limits Includes general introduction on the impact in these key areas