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Handbook of Preparative Inorganic Chemistry, Volume 2, Second Edition focuses on the methods, mechanisms, and chemical reactions involved in conducting experiments on inorganic chemistry. Composed of contributions of various authors, the second part of the manual focuses on elements and compounds. Included in the discussions are copper, silver, and gold. Numerical calculations and diagrams are presented to show the properties, compositions, and chemical reactions of these materials when exposed to varying laboratory conditions. The manual also looks at other elements such as scandium, yttrium, titanium, zirconium, hafnium, and thorium. Lengthy discussions on the characteristics and nature of these elements are presented. The third part of the guidebook discusses special compounds. The manual also provides formula and subject index, including an index for procedures, materials, and devices. Considering the value of information presented, the manual can best serve the interest of readers and scientists wanting to institute a system in the conduct of experiments in laboratories.
Handbook of Preparative Inorganic Chemistry, Volume 1, Second Edition focuses on the methods and mechanisms involved in conducting experiments on inorganic chemistry. Composed of contributions of various authors, the first part of the handbook focuses on special methods and devices for inorganic preparations. The materials mentioned include metals, plastics, pure solvents, and mercury. The text also looks at the importance of temperature and electrical discharges at the laboratory. The second part focuses on elements and compounds, hydrogen peroxide, and fluorine. Schematic diagrams and numerical representations are presented. The chemical reactions of these compounds when exposed to different laboratory conditions are analyzed through numerical representations and schematic diagrams. The handbook also presents lengthy discussions on the properties, compositions, and chemical responses of elements, compound, alkali metals, and earth metals. The formulas, reactions, and methodologies used in the experiments are presented. Considering the value of experiments contained, this manual is a valuable reference for readers interested in studying inorganic chemistry.
Preparative methods. Elements and compounds. Hydrogen, deuterium, water. Hydrogen peroxide. Fluorine, hydrogen fluoride. Fluorine compounds. Chlorine, bromine, iodine. Oxygen, ozone. Sulfur, selenium, tellurium. Nitrogen. Phosphorus. Arsenic, antimony, bismuth. Carbon. Silicon and germanium. Tin and lead. Boron. Aluminum. Gallium, indium, thallium. Alkaline earth metals. Alkali metals. Copper, silver, gold. Zinc, cadmium, mercury. Scandium, yttrium, rare earths. Titanium, zirconium, hafnium, thorium. Vanadium, niobium, tantalum. Chromium, molybdenum, tungsten, uranium. Manganese. Rhenium. Iron. Cobalt, nickel. The platinum metals. Adsorbents and catalysts. Hydroxo salts. Iso - and heteropoly acids and their salts. Carbonyl and nitrosyl compounds. Alloys and intermetallic compounds.
Preparative methods. Elements and compounds. Hydrogen, deuterium, water. Hydrogen peroxide. Fluorine, hydrogen fluoride. Fluorine compounds. Chlorine, bromine, iodine. Oxygen, ozone. Sulfur, selenium, tellurium. Nitrogen. Phosphorus. Arsenic, antimony, bismuth. Carbon. Silicon and germanium. Tin and lead. Boron. Aluminum. Gallium, indium, thallium. Alkaline earth metals. Alkali metals. Copper, silver, gold. Zinc, cadmium, mercury. Scandium, yttrium, rare earths. Titanium, zirconium, hafnium, thorium. Vanadium, niobium, tantalum. Chromium, molybdenum, tungsten, uranium. Manganese. Rhenium. Iron. Cobalt, nickel. The platinum metals. Adsorbents and catalysts. Hydroxo salts. Iso - and heteropoly acids and their salts. Carbonyl and nitrosyl compounds. Alloys and intermetallic compounds.
A best seller since 1966, Purification of Laboratory Chemicals keeps engineers, scientists, chemists, biochemists and students up to date with the purification of the chemical reagents with which they work, the processes for their purification, and guides readerd on critical safety and hazards for the safe handling of chemicals and processes.The Sixth Edition is updated and provides expanded coverage of the latest chemical products and processing techniques, safety and hazards. The book has been reorganised and is now fully indexed by CAS Registry Numbers. Compounds are now grouped to make navigation easier and literature references for all substances and techniques have been added, and ambiguous alternate names and cross references have been removed. - The only comprehensive chemical purification reference, a market leader since 1966, Amarego delivers essential information for research and industrial chemists, pharmacists and engineers: '... (it) will be the most commonly used reference book in any chemical or biochemical laboratory' (MDPI Journal) - An essential lab practice and proceedures manual. Improves efficiency, results and safety by providing critical information for day-to-day lab and processing work. Improved, clear organization and new indexing delivers accurate, reliable information on processes and techniques of purification along with detailed physical properties. - The Sixth Edition has been reorganised and is fully indexed by CAS Registry Numbers; compounds are now grouped to make navigation easier; literature references for all substances and techniques have been added; ambiguous alternate names and cross references removed; new chemical products and processing techniques are covered; hazards and safety remain central to the book.
The contributors to this book discuss inorganic synthesis reactions, dealing with inorganic synthesis and preparative chemistry under specific conditions. They go on to describe the synthesis, preparation and assembly of six important categories of compounds with wide coverage of distinct synthetic chemistry systems
Basic Techniques of Preparative Organic Chemistry covers a detailed guide for carrying out the procedures commonly needed in preparative organic chemistry. The book discusses the nature of organic reactions; the basic principles of preparative organic chemistry; unit operations; and good laboratory practice. The text then provides a review of apparatus and equipment and describes the potential hazards involved in a chemical operation, such as toxicity, bodily injuries, smoking, fire, explosion, and implosion. Techniques and unit operations for carrying out a reaction and for isolating and purifying a reaction product; and the criteria for and methods of assessing purity are also considered. The book further tackles packing and storing products and samples and making reports and communications. Students taking organic chemistry courses will find the text useful.
In revising the text opportunity has been taken to introduce SI units throughout. An Appendix has been included which contains tables of SI units and a table of conversion factors for use when consulting data in non-SI units. Chapter 19 now includes experiments demon strating the use of ion-exchange and solid-liquid chromatography_ Exercises involving colorimetry have been included in Chapter 17. These techniques are introduced as part of a complementary exercise where their relevance is seen as part of a complete piece of work. Minor improvements have been made to some of the experimental procedures and we are grateful to those who have made helpful suggestions in this respect. G. PASS H. SUTCLIFFE iii Preface to the First Edition The student of inorganic chemistry is fortunate in having a wide choice of textbooks covering the descriptive and theoretical aspects of the sUbject. There is no comparable choice of textbooks covering practical inorganic chemistry. Moreover, there is a tendency for many students to draw an unfortunate distinction between chemistry taught in the lecture room, and laboratory work. Consideration of these points prompted the preparation of this book, in which we have attempted to emphasize the relationship between theory and practice.