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While existing books related to DOE are focused either on process or mixture factors or analyze specific tools from DOE science, this text is structured both horizontally and vertically, covering the three most common objectives of any experimental research: * screening designs * mathematical modeling, and * optimization. Written in a simple and lively manner and backed by current chemical product studies from all around the world, the book elucidates basic concepts of statistical methods, experiment design and optimization techniques as applied to chemistry and chemical engineering. Throughout, the focus is on unifying the theory and methodology of optimization with well-known statistical and experimental methods. The author draws on his own experience in research and development, resulting in a work that will assist students, scientists and engineers in using the concepts covered here in seeking optimum conditions for a chemical system or process. With 441 tables, 250 diagrams, as well as 200 examples drawn from current chemical product studies, this is an invaluable and convenient source of information for all those involved in process optimization.
Provides a simple and methodical description of fundamental principles and concepts while simplifying the technical difficulties faced while performing experiments. The topics have been discussed in sufficient detail to provide knowledge of experimental chemistry. The primary objective is to simplify lab procedures and practices for students.
This book is primarily intended for the first year B.Tech students of all branches for their course on engineering chemistry. The main objective of this book is to provide a broad understanding of the chemical concepts, theories and principles of Engineering Chemistry in a clear and concise manner, so that even an average student can grasp the intricacies of the subject. It includes the general concepts of structure and bonding, phase rule, solid state, reaction kinetics and catalysis, electrochemistry, chemical thermodynamics and free energy. Besides, the book introduces topics of applied chemistry like water technology, polymer chemistry and nanotechnology. Each theoretical concept is well supported by illustrative examples. The book also provides a large number of solved problems and illustrations to reinforce the theoretical understanding of concepts. KEY FEATURES (i) Each chapter of the book provides a clear and easy understanding of the definitions, theories and principles. (ii) A large number of well-labelled diagrams help to understand the concepts easily and clearly. (iii) Chapter-wise glossary and important mathematical relations are given for quick revision. (iv) Provides multiple choice questions with answers, short questions and long questions for practice.a
Experimental Methods and Instrumentation for Chemical Engineers, Second Edition, touches many aspects of engineering practice, research, and statistics. The principles of unit operations, transport phenomena, and plant design constitute the focus of chemical engineering in the latter years of the curricula. Experimental methods and instrumentation is the precursor to these subjects. This resource integrates these concepts with statistics and uncertainty analysis to define what is necessary to measure and to control, how precisely and how often.The completely updated second edition is divided into several themes related to data: metrology, notions of statistics, and design of experiments. The book then covers basic principles of sensing devices, with a brand new chapter covering force and mass, followed by pressure, temperature, flow rate, and physico-chemical properties. It continues with chapters that describe how to measure gas and liquid concentrations, how to characterize solids, and finally a new chapter on spectroscopic techniques such as UV/Vis, IR, XRD, XPS, NMR, and XAS. Throughout the book, the author integrates the concepts of uncertainty, along with a historical context and practical examples.A problem solutions manual is available from the author upon request. Includes the basics for 1st and 2nd year chemical engineers, providing a foundation for unit operations and transport phenomena Features many practical examples Offers exercises for students at the end of each chapter Includes up-to-date detailed drawings and photos of equipment
Gives directions for many simple chemistry experiments, including descriptions of necessary equipment, principles, techniques, and safety precautions.
Instrumental methods of analysis have become very popular in industrial and research laboratories due to their rapidity,accuracy,precision,convenience and amenability for automation and computerisation.Although engineers are not expected to carry out hemical analysis by themselves,it is absolutely essential for them to have appreciation regarding the principles,applications,merits and limitations of the modern techniques of instrumental chemical analysis.