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This book is a printed edition of the Special Issue "Electrochemically Engineering of Nanoporous Materials" that was published in Nanomaterials
This book provides in-depth knowledge about the fabrications, structures, properties and applications of three outstanding electrochemically engineered nanoporous materials including porous silicon, nanoporous alumina and nanotubular titania. The book integrates three major themes describing these materials. The first theme is on porous silicon reviewing the methods for preparation by electrochemical etching, properties and methods for surface functionalization relevant for biosensing applications. Biomedical applications of porous silicon are major focus, described in several chapters reviewing recent developments on bioanalysis, emerging capture probes and drug delivery. The second theme on nanoporous alumina starts with describing the concept of self-organized electrochemical process used for synthesis nanopore and nanotube structures of valve metal oxides and reviewing recent development and progress on this field. The following chapters are focused mainly on optical properties and biosensing application of nanoporous alumina providing the reader with the depth of understanding of the structure controlled optical and photonic properties and design of optical biosensing devices using different detection principles such as photoluminescence, surface plasmon resonance, reflective spectrometry, wave guiding, Raman scattering etc. The third theme is focused on nanotubular titania reviewing three key applications including photocatalysis, solar cells and drug delivery. The book represents an important resource for academics, researchers, industry professionals, post-graduate and high-level undergraduate students providing them with both an overview of the current state-of-the-art on these materials and their future developments.
Electrochemical engineering of nanoporous materials is a cost-effective and facile synthesis approach that enables the production of a range of nanoscale materials with controllable dimensions and properties. Recent decades have witnessed extensive research activity into the advanced engineering of nanoporous materials, from fundamental studies to applied science. These nanomaterials offer a set of unique and exclusive advantages for a wealth of applications, including catalysis, energy storage and harvesting, electronics, photonics, sensing, templates, and membranes. This Special Issue is dedicated to recent research advances in electrochemical engineering of nanoporous materials and their application across several disciplines and research fields. The broad and interdisciplinary applicability of these nanomaterials will be of profound and immediate interest for a broad audience, ranging from physicists, chemists, engineers, materials scientists, bioengineers, and nanomedicine experts.
Porous materials are of scientific and technological importance because of the presence of voids of controllable dimensions at the atomic, molecular, and nanometer scales, enabling them to discriminate and interact with molecules and clusters. Interestingly the big deal about this class of materials is about the “nothingness” within — the pore space. International Union of Pure and Applied Chemistry (IUPAC) classifies porous materials into three categories — micropores of less than 2 nm in diameter, mesopores between 2 and 50 nm, and macropores of greater than 50 nm. In this book, nanoporous materials are defined as those porous materials with pore diameters less than 100 nm.Over the last decade, there has been an ever increasing interest and research effort in the synthesis, characterization, functionalization, molecular modeling and design of nanoporous materials. The main challenges in research include the fundamental understanding of structure-property relations and tailor-design of nanostructures for specific properties and applications. Research efforts in this field have been driven by the rapid growing emerging applications such as biosensor, drug delivery, gas separation, energy storage and fuel cell technology, nanocatalysis and photonics. These applications offer exciting new opportunities for scientists to develop new strategies and techniques for the synthesis and applications of these materials.This book provides a series of systematic reviews of the recent developments in nanoporous materials. It covers the following topics: (1) synthesis, processing, characterization and property evaluation; (2) functionalization by physical and/or chemical treatments; (3) experimental and computational studies on fundamental properties, such as catalytic effects, transport and adsorption, molecular sieving and biosorption; (4) applications, including photonic devices, catalysis, environmental pollution control, biological molecules separation and isolation, sensors, membranes, hydrogen and energy storage, etc./a
This book gives detailed information about the fabrication, properties and applications of nanoporous alumina. Nanoporous anodic alumina prepared by low-cost, simple and scalable electrochemical anodization process due to its unique structure and properties have attracted several thousand publications across many disciplines including nanotechnology, materials science, engineering, optics, electronics and medicine. The book incorporates several themes starting from the understanding fundamental principles of the formation nanopores and theoretical models of the pore growth. The book then focuses on describing soft and hard modification techniques for surface and structural modification of pore structures to tailor specific sensing, transport and optical properties of nano porous alumina required for diverse applications. These broad applications including optical biosensing, electrochemical DNA biosensing, molecular separation, optofluidics and drug delivery are reviewed in separated book chapters. The book appeals to researchers, industry professionals and high-level students.
Nanoporous Materials IV contains the invited lectures and peer-reviewed oral and poster contributions to be presented at the 4th International Symposium on Nanoporous Materials, which will be hosted in Niagara Falls, Ontario, Canada, June 7-10, 2005. This volume covers complementary approaches to and recent advances in the field of nanostructured materials with pore sizes larger than 1nm, such as periodic mesoporous molecular sieves (e.g., MCM-41 and SBA-15) and related materials including clays, ordered mesoporous carbons, colloidal crystal templated materials, porous polymers and sol gels. The broad range of topics covered in relation to the synthesis and characterization of ordered mesoporous materials are of great importance for advanced adsorption, catalytic, separation and environmental processes as well as for the development of nanotechnology. This volume contains over 120 contributions related to the synthesis of ordered mesoporous silicas, organosilicas, nonsiliceous inorganic materials, carbons, polymers and related materials, their characterization and applications in adsorption, catalysis and environmental clean up.* Unique contributions brings readers up-to-date on new research and application developments* Figures and tables supplement comprehensive topics * Extensive author and subject index
This series of books, which is published at the rate of about one per year, addresses fundamental problems in materials science. The contents cover a broad range of topics from small clusters of atoms to engineering materials and involve chemistry, physics, and engineering, with length scales ranging from Ångstromsup to millimeters. The emphasis is on basic science rather than on applications. Each book focuses on a single area ofcurrent interest and brings together leading experts to give an up-to-date discussion of their work and the work ofothers. Each article contains enough references that the interested reader can accesstherelevant literature. Thanks aregiven to the Center forFundamental Materials Research atMichigan State University forsupportingthis series. M.F. Thorpe, Series Editor E-mail: [email protected] EastLansing,Michigan, September, 1995 PREFACE This book records selected papers given at an interdisciplinary Symposium on Access in Nanoporous Materials held in Lansing, Michigan, on June 7-9, 1995. Broad interest in the synthesis of ordered materials with pore sizes in the 1.0-10 nm range was clearly manifested in the 64 invited and contributed papers presented by workers in the formal fields of chemistry, physics, and engineering. The intent of the symposium was to bring together a small number ofleading researchers within complementary disciplines to share in the diversity of approaches to nanoporous materials synthesis and characterization.
High-surface-area materials have recently attracted significant interest due to potential applications in various fields such as electrochemistry and catalysis, gas-phase catalysis, optics, sensors and actuators, energy harvesting and storage. In contrast to classical materials the properties of high-surface-area materials are no longer determined by their bulk, but by their nanoscale architecture. Nanoporous gold (np-Au) represents the fascinating class of mesoporous metals that have been intensively investigated in recent years. The current interest and the increasing number of scientific publications show that np-Au by itself is an outstanding nano-material that justifies a book devoted to all aspects of its properties and applications. The resulting publication is a discussion of this unique nano-material and is an accessible and comprehensive introduction to the field. The book provides a broad, multi-disciplinary platform to learn more about the properties of nanoporous gold from an inter-disciplinary perspective. It starts with an introduction and overview of state-of-the-art applications and techniques characterizing this material and its applications. It then covers the progress in research within the last years. The chapters are in-depth overviews written by the world's leading scientists in the particular field. Each chapter covers one technique or application so that the reader can easily target their favoured topic and will get the latest and state-of-the-art information in the field.
Handbook of Emerging Materials for Sustainable Energy provides a comprehensive accounting on the fundamentals, current developments, challenges and future prospects of emerging materials for the development of sustainable energy. Each chapter addresses a distinct and important area within the energy field and includes comprehensive data to support the materials being presented. Sections cover Batteries, Capacitors and Supercapacitors, Fuel cells, Thermoelectrics, Novel illumination sources and techniques, Photovoltaics & Solar cells, Alternative energy sources, hydrogen as an energy source, including hydrogen production and fuel generation, the use of Biofuels and Carbon dioxide. The book concludes with three chapters related to advanced materials under development for energy conservation and environmental protection, including theories, methodologies and simulations established for advanced materials. - Covers a broad scope of advanced materials that have been developed for energy and environmental sustainability - Provides detailed and updated information about the structural and functional features of various emerging materials and their multifaceted applications - Includes supplementary data alongside each chapter
Nanohybrid and Nanoporous Materials for Aqueous Environmental Pollution Control gives a comprehensive treatment of fabrication methods and their application in environmental remediation, including adsorption, catalysis and signal transfer in pollutant detection. The design, fabrication and application of nanohybrid and nanoporous materials for environmental pollution control are described in detail, along with discussions on their synthesis, characterization, and applications in different aspects of pollutant treatment. Chapters introduce the design and synthesis of magnetic nanohybrid materials, advanced oxide process-photocatalytic degradation of environmental pollutants based on nanomaterials, and nanohybrids of iron based materials for reduction and oxidation of aqueous recalcitrant pollutant. Finally, challenges and suggestions in the application of nanomaterials for environmental pollution control are discussed, as is an analysis of the future perspective of nanomaterials for environmental application. - Presents the most up-to-date developments in this rapidly progressing field - Provides suggestions to address challenges and solve current problems related to the application of nanoporous materials - Discusses future trends and perspectives in the area of nanohybrid and nanoporous materials