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A completely thorough and up-to-date guide to modern distillation methods and their applications Distillation has been used for separating liquid mixtures for more than two thousand years, and it continues to be the most widely used separation technique in key industries throughout the industrialized world. Although the basic principles have remained the same since the days of the ancient Egyptians, new distillation and distillation control methods continue to be developed to satisfy a variety of highly specialized requirements. Encyclopedic in scope, this book provides distillation technicians with a uniquely comprehensive, up-to-date account of distillation methods currently employed in the oil, petrochemical, chemical, and pharmaceutical industries. The authors begin by acquainting readers with the principles of vapor-liquid equilibrium and the essential calculations for determining phase equilibria and equilibrium curves. Subsequent chapters are devoted to practical discussions of virtually all modern distillation methods, including batch, single stage, multistage continuous, multistage batch, and others. A wide array of industrial applications are described, including everything from crude oil distillation and argon recovery from air to water purification and ammonia recovery from wastewater. Special sections deal with the separation of azeotropic mixtures and the energy demand of distillation processes. Concluding chapters are devoted to detailed, extremely well illustrated descriptions of practical equipment design and modern distillation control methods. Distillation: Principles and Practice is an indispensable working resource for distillation technicians working in the oil, petrochemical, chemical, and pharmaceutical industries.
Distillation Principles and Practice Second Edition covers all the main aspects of distillation including the thermodynamics of vapor/liquid equilibrium, the principles of distillation, the synthesis of distillation processes, the design of the equipment, and the control of process operation. Most textbooks deal in detail with the principles and laws of distilling binary mixtures. When it comes to multi-component mixtures, they refer to computer software nowadays available. One of the special features of the second edition is a clear and easy understandable presentation of the principles and laws of ternary distillation. The right understanding of ternary distillation is the link to a better understanding of multi-component distillation. Ternary distillation is the basis for a conceptual process design, for separating azeotropic mixtures by using an entrainer, and for reactive distillation, which is a rapidly developing field of distillation. Another special feature of the book is the design of distillation equipment, i.e. tray columns and packed columns. In practice, empirical know-how is preferably used in many companies, often in form of empirical equations, which are not even dimensionally correct. The objective of the proposed book is the derivation of the relevant equations for column design based on first principles. The field of column design is permanently developing with respect to the type of equipment used and the know-how of two-phase flow and interfacial mass transfer.
Batch Distillation: Science and Practice is a must have for distillers of all experience levels. Inside you'll find discussions on the history of distillation, distillation chemistry, considerations for purchasing a still and much more. Strickland uses an easy-to-read conversational tone to detail difficult to parse topics such as making distillation cuts, different distillation techniques, how to operate simple and hybrid batch stills and even how to approach the distillation of botanicals for spirits such as gin or absinthe. Throughout the text you'll find anecdotes and real-world wisdom on these and many other topics to help you on your path to making high-calibre spirits.
Distillation: Fundamentals and Principles — winner of the 2015 PROSE Award in Chemistry & Physics — is a single source of authoritative information on all aspects of the theory and practice of modern distillation, suitable for advanced students and professionals working in a laboratory, industrial plants, or a managerial capacity. It addresses the most important and current research on industrial distillation, including all steps in process design (feasibility study, modeling, and experimental validation), together with operation and control aspects. This volume features an extra focus on the conceptual design of distillation. - Winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers - Practical information on the newest development written by recognized experts - Coverage of a huge range of laboratory and industrial distillation approaches - Extensive references for each chapter facilitates further study
Distillation: Equipment and Processes—winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers—is a single source of authoritative information on all aspects of the theory and practice of modern distillation, suitable for advanced students and professionals working in a laboratory, industrial plants, or a managerial capacity. It addresses the most important and current research on industrial distillation, including all steps in process design (feasibility study, modeling, and experimental validation), together with operation and control aspects. This volume features an extra focus on distillation equipment and processes. - Winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers - Practical information on the newest development written by recognized experts - Coverage of a huge range of laboratory and industrial distillation approaches - Extensive references for each chapter facilitates further study
Written specifically for use in the educational program of the production division of Seagram Distillers Corporation, this volume provides a fundamental explanation of the physical and chemical processes involved in the operation of a grain alcohol distillery.
A timely treatment of distillationcombining steady-state designand dynamic controllability As the world continues to seek new sources of energy, the distillation process remains one of the most important separation methods in the chemical, petroleum, and energy industries. And as new renewable sources of energy and chemical feedstocks become more universally utilized, the issues of distillation design and control will remain vital to a future sustainable lifestyle. Distillation Design and Control Using Aspen Simulation introduces the current status and future implications of this vital technology from the dual perspectives of steady-state design and dynamics. Where traditional design texts have focused mainly on the steady-state economic aspects of distillation design, William Luyben also addresses such issues as dynamic performance in the face of disturbances. Utilizing the commercial simulators Aspen Plus and Aspen Dynamics, the text guides future and practicing chemical engineers first in the development of optimal steady-state designs of distillation systems, and then in the development of effective control structures. Unique features of the text include: * In-depth coverage of the dynamics of column design to help develop effective control structures for distillation columns * Development of rigorous simulations of single distillation columns and sequences of columns * Coverage of design and control of petroleum fractionators Encompassing nearly four decades of research and practical developments in this dynamic field, the text represents an important reference for both students and experienced engineers faced with distillation problems.
Distillation: Operation and Applications—winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers—is a single source of authoritative information on all aspects of the theory and practice of modern distillation, suitable for advanced students and professionals working in a laboratory, industrial plants, or a managerial capacity. It addresses the most important and current research on industrial distillation, including all steps in process design (feasibility study, modeling, and experimental validation), together with operation and control aspects. This volume features an extra focus on distillation applications. - Winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers - Practical information on the newest development written by recognized experts - Coverage of a huge range of laboratory and industrial distillation approaches - Extensive references for each chapter facilitates further study
After an overview of the fundamentals, limitations, and scope of reactive distillation, this book uses rigorous models for steady-state design and dynamic analysis of different types of reactive distillation columns and quantitatively compares the economics of reactive distillation columns with conventional multi-unit processes. It goes beyond traditional steady-state design that primarily considers the capital investment and energy costs when analyzing the control structure and the dynamic robustness of disturbances, and discusses how to maximize the economic and environmental benefits of reactive distillation technology.
This book essentially summarises the water shortage crisis in the world and its possible solution by using solar energy through solar stills. The world is facing an urgent problem. By 2015, 40 per cent of the world's population will be living in regions without adequate fresh water supply. Presently, almost all sea water desalination plans are electricity based and highly power intensive. With more than half the world likely to become dependent on sea water desalination such an energy-expensive scenario is clearly not sustainable.The aim of the book is to provide the most recent information on various practices, developments and improvements in water distillation, heat and mass transfer in solar distillation, thermal modelling and embedded energy of solar stills, and the applications of solar distillation in today's world. The concluding chapter also deals with economic analysis of solar distillation. To simplify the subject, figures, tables, solved examples and problems with hints are given at the end of each chapter, and there are appendices and a glossary of meaningful terms to assist the reader. The authors have written an outstanding academic work which carries weight and resonance beyond university courses and libraries, and which impacts on the global population.