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Research on ferroelectricity and ferroelectric materials started in 1920 with the discovery by Valasek that the variation of spontaneous polarization in Rochelle salt with sign and magnitude of an applied electric field traced a complete and reproducible hysteresis loop. Activity in the field was sporadic until 1935, when Busch and co-workers announced the observation of similar behavior in potassium dihydrogen phosphate and related compounds. Progress thereafter continued at a modest level with the undertaking of some theoretical as well as further experimental studies. In 1944, von Hippel and co-workers discovered ferroelectricity in barium titanate. The technological importance of ceramic barium titanate and other perovskites led to an upsurge of interest, with many new ferroelectrics being identified in the following decade. By 1967, about 2000 papers on various aspects of ferroelectricity had been published. The bulk of this widely dispersed literature was concerned with the experimental measurement of dielectric, crystallographic, thermal, electromechanical, elastic, optical, and magnetic properties. A critical and excellently organized cpmpilation based on these data appeared in 1969 with the publica tion of Landolt-Bornstein, Volume 111/3. This superb tabulation gave instant access to the results in the literature on nearly 450 pure substances and solid solutions of ferroelectric and antiferroelectric materials. Continuing interest in ferroelectrics, spurred by the growing importance of electrooptic crystals, resulted in the publication of almost as many additional papers by the end of 1969 as had been surveyed in Landolt-Bornstein.
This volume is a joint effort of the Research Materials Information Center (RMIC) of the Solid State Division at Oak Ridge National Laboratory and the Libraries and Information Systems Center at Bell Telephone Laboratories (BTL) Murray Hill, N. J. The Research Materials Information Center has, since 1963, been answering inquiries on the avail ability, preparation, and properties of inorganic solid-state research materials. The preparation of bibliographies has been essential to this function, and the interest in ferroelectrics led to the compila tion of the journal and report literature on that subject. The 1962 book Ferroelectric Crystals, by Jona and Shirane, was taken as a cutoff point, and all papers through mid-1969 received by the Center have been included. The Libraries and Information Systems Center of BTL has, over a period of years, developed a proprie tary package of computer programs called BELDEX, which formats and generates indexes to biblio graphic material. This group therefore undertook to process RMIC's ferroelectric references by BELDEX so that both laboratories could have the benefit of an indexed basic bibliography in this important research area.
This thesis explores the fascinating properties of domain walls in ferroelectric materials. Domain walls can be used as model systems to study fundamental aspects of interface physics, such as crackling noise, with implications extending to a broad variety of systems, from material fracture and earthquakes to solar flares and collective decision making. Ferroelectric domain walls also show functional properties absent from the domains themselves, such as enhanced conduction leading to the tantalizing possibility of reconfigurable nanoelectronic circuitry where domain walls are active components. This work discusses the crackling physics of domain walls in thin films of Pb(Zr0.2Ti0.8)O3, as well as links between the local conductivity of domain walls and nanoscale geometrical distortions due to defects, and discusses unusual polarization textures with rotational components at crossings of ferroelastic twin domains. The results presented in this thesis have important implications for the experimental study of crackling systems.
The ferroelectric material barium titanate exhibits exceptional electro-optic and dielectric properties, making it desirable for electro-optic applications, especially in thin film form. The effective nonlinear optical and dielectric properties of BaTiO3 films are determined by the ferroelectric domain structure. The ferroelectric domain structures of epitaxial BaTiO3 films on MgO (100) substrates were investigated using x-ray diffraction (XRD), scanning probe microscopy (SPM), and second harmonic generation (SHG) techniques.