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Data Quality Objectives (DQOs) for gas and liquid sampling from the sealed canisters in K West Basin have been developed and are presented in this document. This sampling campaign supports the selection of canisters to provide fuel for hot cell examinations and provides an assessment of gas/liquid chemistry for comparison to the results of fuel element hot cell examinations. It also provides information applicable to water cleanup and air permits for the fuel handling associated with moving fuel to dry storage.
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The Data Quality Objectives (DQOs) were established for the examinations of the first group of fuel samples shipped from the K West Basin to the Hanford 327 Building hot cells for examinations to support the Path Forward recommended to solve the safety and environmental concerns associated with the deteriorating fuel in the K Basins. A separate DQO will be prepared for each future shipment of samples to the hot cells. The material stored in the K West Basin must ultimately be removed from the basin and placed in a stable storage configuration until it can be disposed of in a repository. The condition of the fuel in the closed canisters is a major uncertainty for any of the proposed actions. The major question to answer is what are the conditions of the materials in the closed canisters? The data to be gathered during the canister opening, handling, transport, associated hot cell handling, and examinations will also support decisions related to the Path Forward primarily in areas of transportation and the Multi-Canister Overpack (MCO) design.
The Data Quality Objectives (DQOS) were established for the examinations of the second group of K West fuel samples. The examinations will expand the initial understanding obtained for fuel stored in closed canisters with emphasis on whole element drying and conditioning testing and Thermo-Gravimetric Analysis (TGA) for oxidation behavior, drying, and hydrogen release. The laboratory examinations addressed in this DQO take into account the extent and diversity of the fuel damage as indicated by previous in-basin examinations. A total of fifteen fuel elements are identified for laboratory examinations. Three of these elements are designated for surface coating examinations and two elements are designated for examination of subsurface sludge accumulations and for sectioning of small samples for TGA measurement.
The Data Quality Objectives (DQOs) were established for the reaction kinetics studies of the first group of fuel samples shipped from the K West Basin to the Hanford 327 Building hot cells for examinations. A Thermo-Gravimetric Analysis (TGA) system was selected for these measurements and associated hydrogen release and ignition temperature testing. These examinations are an extension of the conditioning testing of sibling samples described in WHC-SD-SNF-DQO-004, Data Quality Objectives for the Initial Fuel Conditioning Examinations.