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About Book Analytical methods that are portable, reasonably priced, and use simple instruments have been made possible by electrochemistry. Investigations and monitoring of biological samples, industrial products, and the environment also frequently employ electroanalytical procedures with a high degree of accuracy, precision, sensitivity, and selectivity. This book describes the detailed electrochemical terms and concepts engaged in the electrochemical reactions at the electrodes in electrochemical cells. Various types of electrode processes to display the electrochemical main features are concentrated. The basic electroanalytical cell systems and their practical electroanalysis are discussed simply. The book provides readers with a thorough grounding in the fundamentals of electrode reactions and the principles of electrochemical methods. The application of electroanalytical methods to chemical systems is the main prominence while the basic principles of electrochemistry are also discussed. Moreover, I am pretty sure that this book will improve the confidence of young researchers and students to think and remember electroanalytical concepts. I highly believe that this book will go a long way to satisfy the long-felt need of young researchers/students for a friendly guide on electrochemical analysis and sensors. Thank you, Dr. Govindhan Maduraiveeran
The critically acclaimed guide to the principles, techniques, and instruments of electroanalytical chemistry-now expanded and revised Joseph Wang, internationally renowned authority on electroanalytical techniques, thoroughly revises his acclaimed book to reflect the rapid growth the field has experienced in recent years. He substantially expands the theoretical discussion while providing comprehensive coverage of the latest advances through late 1999, introducing such exciting new topics as self-assembled monolayers, DNA biosensors, lab-on-a-chip, detection for capillary electrophoresis, single molecule detection, and sol-gel surface modification. Along with numerous references from the current literature and new worked-out examples, Analytical Electrochemistry, Second Edition offers clear, reader-friendly explanations of the fundamental principles of electrochemical processes as well as important insight into the potential of electroanalysis for problem solving in a wide range of fields, from clinical diagnostics to environmental science. Key topics include: The basics of electrode reactions and the structure of the interfacial region Tools for elucidating electrode reactions and high-resolution surface characterization An overview of finite-current controlled potential techniques Electrochemical instrumentation and electrode materials Principles of potentiometric measurements and ion-selective electrodes Chemical sensors, including biosensors, gas sensors, solid-state devices, and sensor arrays
Electrochemistry plays a key role in a broad range of research and applied areas including the exploration of new inorganic and organic compounds, biochemical and biological systems, corrosion, energy applications involving fuel cells and solar cells, and nanoscale investigations. The Handbook of Electrochemistry serves as a source of electrochemical information, providing details of experimental considerations, representative calculations, and illustrations of the possibilities available in electrochemical experimentation. The book is divided into five parts: Fundamentals, Laboratory Practical, Techniques, Applications, and Data. The first section covers the fundamentals of electrochemistry which are essential for everyone working in the field, presenting an overview of electrochemical conventions, terminology, fundamental equations, and electrochemical cells, experiments, literature, textbooks, and specialized books. Part 2 focuses on the different laboratory aspects of electrochemistry which is followed by a review of the various electrochemical techniques ranging from classical experiments to scanning electrochemical microscopy, electrogenerated chemiluminesence and spectroelectrochemistry. Applications of electrochemistry include electrode kinetic determinations, unique aspects of metal deposition, and electrochemistry in small places and at novel interfaces and these are detailed in Part 4. The remaining three chapters provide useful electrochemical data and information involving electrode potentials, diffusion coefficients, and methods used in measuring liquid junction potentials. * serves as a source of electrochemical information * includes useful electrochemical data and information involving electrode potentials, diffusion coefficients, and methods used in measuring liquid junction potentials * reviews electrochemical techniques (incl. scanning electrochemical microscopy, electrogenerated chemiluminesence and spectroelectrochemistry)
Electrochemistry for Bioanalysis provides a comprehensive understanding of the benefits and challenges of the application of electrochemical and electroanalytical techniques for measurement in biological samples. The book presents detailed information on measurement in a host of various biological samples from single cells, tissues and in vivo. Sections cover real insights surrounding key experimental design and measurement within multiple complex biological environments. Finally, users will find discussions on emerging topics such as electrogenerated chemiluminescence and the use of additive manufacturing for biosensor fabrication. Continuous learning reinforcement throughout the book, including problems for self-assessment, make this an ideal resource. Balances the fundamentals of electrochemical and neurochemical methods with current advances in the field of bioanalysis Includes self-assessment scenarios on experimental design and validation to teach readers key factors and considerations in measurement Highlights applications (such as sensors and biosensors) and key points within each chapter
Das führende Werk auf seinem Gebiet - jetzt durchgängig auf den neuesten Stand gebracht! Die theoretischen Grundlagen der Elektrochemie, erweitert um die aktuellsten Erkenntnisse in der Theorie des Elektronentransfers, werden hier ebenso besprochen wie alle wichtigen Anwendungen, darunter modernste Verfahren (Ultramikroelektroden, modifizierte Elektroden, LCEC, Impedanzspektrometrie, neue Varianten der Pulsvoltammetrie und andere). In erster Linie als Lehrbuch gedacht, läßt sich das Werk aber auch hervorragend zum Selbststudium und zur Auffrischung des Wissensstandes verwenden. Lediglich elementare Grundkenntnisse der physikalischen Chemie werden vorausgesetzt.
The new edition of the cornerstone text on electrochemistry Spans all the areas of electrochemistry, from the basicsof thermodynamics and electrode kinetics to transport phenomena inelectrolytes, metals, and semiconductors. Newly updated andexpanded, the Third Edition covers important new treatments, ideas,and technologies while also increasing the book's accessibility forreaders in related fields. Rigorous and complete presentation of the fundamentalconcepts In-depth examples applying the concepts to real-life designproblems Homework problems ranging from the reinforcing to the highlythought-provoking Extensive bibliography giving both the historical developmentof the field and references for the practicing electrochemist.
Electrogenerated chemiluminescence (ECL) is a powerful and versatile analytical technique, which is widely applied for biosensing and successfully commercialized in the healthcare diagnostic market. After introducing the fundamental concepts, this book will highlight the recent analytical applications with a special focus on immunoassays, genotoxicity, imaging, DNA and enzymatic assays. The topic is clearly at the frontier between several scientific domains involving analytical chemistry, electrochemistry, photochemistry, materials science, nanoscience and biology. This book is ideal for graduate students, academics and researchers in industry looking for a comprehensive guide to the different aspects of electrogenerated chemiluminescence.
Provides an overview of research in Diamond Electrochemistry, as well as practical applications of diamond electrodes. With chapters written by experts in their respective fields, this book serves as a useful source of information for electrochemists working in physical or analytical chemistry.
Third Edition covers the latest advances in methodologies, sensors, detectors, and mIcrochips The greatly expanded Third Edition of this internationally respected text continues to provide readers with a complete panorama of electroanalytical techniques and devices, offering a balancebetween voltammetric and potentiometric techniques. Emphasizing electroanalysis rather than physical electrochemistry, readers gain a deep understanding of the fundamentals of electrodereactions and electrochemical methods. Moreover, readers learn to apply their newfoundknowledge and skills to solve real-world analytical problems. The text consists of six expertly crafted chapters: * Chapter 1 introduces fundamental aspects of electrode reactions and the structure of the interfacial region * Chapter 2 studies electrode reactions and high-resolution surface characterization, using techniques ranging from cyclic voltammetry to scanning probe microscopies * Chapter 3 features an overview of modern finite-current controlled potential techniques * Chapter 4 presents electrochemical instrumentation and electrode materials, including modified electrodes and ultramicroelectrodes * Chapter 5 details the principles of potentiometric measurements and various classes of ion selective electrodes * Chapter 6 explores the growing field of chemical sensors, including biosensors, gas sensors, microchip devices, and sensor arrays Among the new topics covered, readers discover DNA biosensors, impedance spectroscopy, detection of capillary electrophoresis, diamond electrodes, carbon-nanotube and nanoparticle-based arrays and devices, large-amplitude AC voltammetry, solid-state ion-selective electrodes, ion selective electrodes for trace analysis, and lab-on-a-chip devices. New figures, worked examples, and end-of-chapter questions have also been added to this edition. Given the rapid pace of discovery and growth of new applications in the field, this text is essential for an up-to-date presentation of the latest advances in methodologies, sensors, detectors, and microchips. It is recommended for graduate-level courses in electroanalytical chemistry and as a supplement for upper-level undergraduate courses in instrumental analysis. The text also meets the reference needs for any industry, government, or academic laboratory engaged in electroanalysis and biosensors.
For the first time, the authors provide a comprehensive and consistent presentation of all techniques available in this field. They rigorously analyze the behavior of different electrochemical single and multipotential step techniques for electrodes of different geometries and sizes under transient and stationary conditions. The effects of these electrode features in studies of various electrochemical systems (solution systems, electroactive monolayers, and liquid-liquid interfaces) are discussed. Explicit analytical expressions for the current-potential responses are given for all available cases. Applications of each technique are outlined for the elucidation of reaction mechanisms. Coverage is comprehensive: normal pulse voltammetry, double differential pulse voltammetry, reverse pulse voltammetry and other triple and multipulse techniques, such as staircase voltammetry, differential staircase voltammetry, differential staircase voltcoulommetry, cyclic voltammetry, square wave voltammetry and square wave voltcoulommetry.