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In this book on quantitative analysis and reagent preparation, the authors adopt a novel approach-all the preparations have been given in the form of organic reactions in alphabetical order, with their respective reaction mechanisms. The procedures of some preparations are also discussed. Estimation of various compounds and functional groups is also included. A complete is deveoted to chromatography, with exercises.
This manual for practical qualitative analysis covers the use of spectroscopic methods for identification of various functional groups, Comprehensive tables giving methods for the systematic identification of pure specimens, separation of mixtures and compounds, and procedures for preparation of derivatives are some of the salient features of the book.
In revising the text opportunity has been taken to introduce SI units throughout. An Appendix has been included which contains tables of SI units and a table of conversion factors for use when consulting data in non-SI units. Chapter 19 now includes experiments demon strating the use of ion-exchange and solid-liquid chromatography_ Exercises involving colorimetry have been included in Chapter 17. These techniques are introduced as part of a complementary exercise where their relevance is seen as part of a complete piece of work. Minor improvements have been made to some of the experimental procedures and we are grateful to those who have made helpful suggestions in this respect. G. PASS H. SUTCLIFFE iii Preface to the First Edition The student of inorganic chemistry is fortunate in having a wide choice of textbooks covering the descriptive and theoretical aspects of the sUbject. There is no comparable choice of textbooks covering practical inorganic chemistry. Moreover, there is a tendency for many students to draw an unfortunate distinction between chemistry taught in the lecture room, and laboratory work. Consideration of these points prompted the preparation of this book, in which we have attempted to emphasize the relationship between theory and practice.
For BSc. and MSc. as per UGC syllabuses. Develops manipulative practical skill. Starting from simple preparations goes on to compounds involving two, three or more steps based on several types of reactions. Help understand intricacies, theoretical aspects and practical limitations of a known reaction leading to mastery of the art of organic synthesis.
There has been significant expansion in the application of atomic spectrographic techniques in recent years, which has brought with it the need to provide more flexible methods to a wider range of samples, particularly non-aqueous samples. This book compares the traditional and improved methods in the analysis of non-aqueous samples for elemental analyses by atomic emission spectroscopic methods whilst describing procedures that will attempt to improve sample preparation methods.
A Clear And Reliable Guide To Students Of Practical Organic Chemistry At The Undergraduate And Postgraduate Levels. This Edition S Special Emphasis Is On Semi Micro Methods And Modern Techniques And Reactions.