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Ein Praxisleitfaden der Polymeranalyse für alle, die sich in Polymerlabors mit Analytik, Qualitätskontrolle oder Produktentwicklung beschäftigen. Der Autor erläutert, aus seinem umfangreichen Erfahrungsschatz, welche Probleme in welchen Situationen auftreten können. Viele Fallstudien helfen bei der Anwendung der Erkenntnisse im Laboralltag. Mit einer umfangreichen Datensammlung zu physikalischen Eigenschaften von Polymeren! (07/00)
Technical and technological development demands the creation of new materials that are stronger, more reliable, and more durable-materials with new properties. This new book covers a broad range of polymeric materials and technology and provides researchers in polymer science and technology with new research on the functional materials production c
Covering a broad range of polymer science topics, Handbook of Polymer Synthesis, Characterization, and Processing provides polymer industry professionals and researchers in polymer science and technology with a single, comprehensive handbook summarizing all aspects involved in the polymer production chain. The handbook focuses on industrially important polymers, analytical techniques, and formulation methods, with chapters covering step-growth, radical, and co-polymerization, crosslinking and grafting, reaction engineering, advanced technology applications, including conjugated, dendritic, and nanomaterial polymers and emulsions, and characterization methods, including spectroscopy, light scattering, and microscopy.
This volume provides an overview of polymer characterization test methods. The methods and instrumentation described represent modern analytical techniques useful to researchers, product development specialists, and quality control experts in polymer synthesis and manufacturing. Engineers, polymer scientists and technicians will find this volume useful in selecting approaches and techniques applicable to characterizing molecular, compositional, rheological, and thermodynamic properties of elastomers and plastics.
Presents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background. Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation. Written by experts in the various areas of thermal analysis Relevant and detailed experiments and examples follow each chapter.
Based on Wiley's renowned Encyclopedia of Polymer Science and Technology, this book provides coverage of key methods of characterization of the physical and chemical properties of polymers, including atomic force microscopy, chromatographic methods, laser light scattering, nuclear magnetic resonance, and thermal analysis, among others. Written by prominent scholars from around the world, this reference presents over twenty-five self -contained articles on the most used analytical techniques currently practiced in polymer science.
Written by expert contributors from the academic and industrial sectors, this book presents traditional and modern approaches to polymer characterization and analysis. The emphasis is on pragmatics, problem solving and property determination; real-world applications provide a context for key concepts. The characterizations focus on organic polymer and polymer product microstructure and composition. Approaches molecular characterization and analysis of polymers from the viewpoint of problem-solving and polymer property characterization, rather than from a technique championing approach Focuses on providing a means to ascertaining the optimum approach or technique(s) to solve a problem/measure a property, and thereby develop an analytical competence in the molecular characterization and analysis of real-world polymer products Provides background on polymer chemistry and microstructure, discussions of polymer chain, morphology, degradation, and product failure and additive analysis, and considers the supporting roles of modeling and high-throughput analysis
This book introduces the techniques used for the analysis of polymers. It covers the main aspects of polymer science and technology; identification, polymerization, molecular weight, structure, surface properties, degradation and mechanical properties. * Clear explanations of each analytical technique * Describes the application of techniques to the study of polymers * Encourages learning through numerous self-assessment questions and answers * Structured for flexible learning
Many of the compositional analysis applications involving thermogravimetry have focused on the determination of concentrations of one or two additives to a polymeric matrix. Paramount to the utility of such a thermogravimetric approach for filled polymers is that the matrix pyrolyzes repeatably, if not completely. Equally important is the understanding of the components constituting the high temperature residue (ash) and how they are derived. Two examples will be addressed in which controlling or understanding the chemistry of the experiment highlights the significance of the above-mentioned factors in achieving useful compositional analyses. In the first example, an ammoniated atmosphere is employed to achieve repeatable pyrolysis of silicone rubber to measure the carbon black filler content. The second example emphasizes the understanding of decomposition chemistry to distinguish two inorganic fillers retained as ash. In this example the evolution of CO2 from CaCO3 is used to identify the calcium oxide portion of the ash in a polystyrene + carbon black + silicone oil + calcium carbonate + titanium dioxide system.