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This text explores the optimization of catalytic materials through traditional and novel methods of catalyst preparation, characterization, and monitoring for oxides, supported metals, zeolites, and heteropolyacids. It focuses on the synthesis of bulk materials and of heterogeneous materials, particularly at the nanoscale. The final chapters examine pretreatment, drying, finishing effects, and future applications involving catalyst preparation and the technological advances necessary for continued progress. Topics also include heat and mass transfer limitations, computation methods for predicting properties, and catalyst monitoring on laboratory and industrial scales.
This text explores the optimization of catalytic materials through traditional and novel methods of catalyst preparation, characterization, and monitoring for oxides, supported metals, zeolites, and heteropolyacids. It focuses on the synthesis of bulk materials and of heterogeneous materials, particularly at the nanoscale. The final chapters examin
This book serves as an introduction to the subject, giving readers the tools to solve real-world chemical reaction engineering problems. It features a section of fully solved examples as well as end of chapter problems. It includes coverage of catalyst characterization and its impact on kinetics and reactor modeling. Each chapter presents simple ideas and concepts which build towards more complex and realistic cases and situations. Introduces an in-depth kinetics analysis Features well developed sections on the major topics of catalysts, kinetics, reactor design, and modeling Includes a chapter that showcases a fully worked out example detailing a typical problem that is faced when performing laboratory work Offers end of chapter problems and a solutions manual for adopting professors Aimed at advanced chemical engineering undergraduates and graduate students taking chemical reaction engineering courses as well as chemical engineering professionals, this textbook provides the knowledge to tackle real problems within the industry.
Written by a team of internationally recognized experts, this book addresses the most important types of catalytic reactions and catalysts as used in industrial practice. Both applied aspects and the essential scientific principles are described. The main topics can be summarized as follows: heterogeneous, homogeneous and biocatalysis, catalyst preparation and characterization, catalytic reaction engineering and kinetics, catalyst deactivation and industrial perspective.
Solid catalysts play a fundamental role in all areas between basic research and industrial applications. This book offers a large amount of information about the preparation of solid catalysts. All types of solid catalysts and all important aspects of their preparation are discussed. The highly topical contributions are written by leading experts in disciplines ranging from solid state, interface and solution chemistry to industrial engineering. The straightforward presentation of the material and the comprehensive coverage make this book an essential and indispensible tool for every scientist and engineer working with solid catalysts.
This practical book combines recent progress with a discussion of the general aspects of catalyst preparation. The first part deals with the basic principles of solid catalyst preparation, explaining the main aspects of sol-gel chemistry and interfacial chemistry, followed by such techniques as co-precipitation and immobilization. New tools for catalyst preparation research, including microspectroscopy and high-throughput experimentation, are also taken into account. The second part heightens the practical relevance by providing six case studies on such topics as the preparation of zeolites, hydrotreating catalysts, methanol catalysts and gold catalysts
The proceedings of the VIIth International Symposium on the Scientific Bases for the Preparation of Heterogeneous Catalysts, are in line with the general scope of this series of events. Emphasis in all Symposia has been on the scientific aspects of the preparation of new and industrial catalysts, or on new methods of preparation, rather than on the catalytic reactions in which such solids are ultimately used. In the present context, the catalytic event itself has only been considered as another, though often decisive, method of catalyst characterization.
Explaining methods for carrying out chemical syntheses without the use of catalysts, this book shows how avoiding catalysts during synthesis can mean less use of toxic chemicals, environmentally damaging chemicals, or endangered elements, and lower costs.
The phenomenon of catalysis is found in many homogeneous and heterogeneous systems undergoing chemical change, where it effects the rates of approach to the equilibrium state in processes as diverse as those found in the stars, the earth's mantle, living organisms, and the various chemistries utilized by industry. The economies and the living standards of both developed and developing countries depend to varying degrees upon the efficacy of their chemical industries. Con sequently, this century has seen a wide exploration and expansion of catalytic chemistry together with an intensive investigation of specific, essential processes like those contributing to life-supporting agricultures. Prime among the latter must surely be the "fixation" of atmospheric nitrogen by catalytic hydrogenation to anhydrous ammonia, still the preferred synthetic precursor of the nitrogenous components of fertilizers. In each decade contemporary concepts and techniques have been used to further the understanding, as yet incomplete, of the catalyst, the adsorbates, the surface reactions, and the technology of large-scale operation. The contributors to the present volume review the state of the art, the science, and the technology; they reveal existing lacunae, and suggest ways forward. Around the turn of the century, Sabatier's school was extending the descriptive catalytic chemistry of hydrogenation by metals to include almost all types of multiple bond. The triple bond of dinitrogen, which continued to be more resistant than the somewhat similar bonds in carbon monoxide and ethyne, defied their efforts.