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This report presents a cost analysis of Caprolactam production from benzene The process examined involves the following steps: benzene is hydrogenated to cyclohexane; cyclohexane is oxidized to a mixture of cyclohexanol and cyclohexanone; cyclohexanol is dehydrogenated to cyclohexanone; cyclohexanone undergoes an oximation reaction with hydroxilamine; and the oxime produced is rearranged to Caprolactam. Ammonium sulfate is also generated as by-product. This report was developed based essentially on the following reference(s): (1) "Caprolactam", Ullmann's Encyclopedia of Industrial Chemistry, 7th edition (2) "Cyclohexane", Ullmann's Encyclopedia of Industrial Chemistry, 7th edition Keywords: Cyclohexanone, Cyclohexanol, Lactam Synthesis, Lactam Purification, Ammonium Sulfate Crystallization
This report presents a cost analysis of Caprolactam production from benzene. The process examined involves the following steps: benzene is hydrogenated to cyclohexane; cyclohexane is oxidized to a mixture of cyclohexanol and cyclohexanone; cyclohexanol is dehydrogenated to cyclohexanone; cyclohexanone undergoes an oximation reaction with hydroxilamine; and the oxime produced is rearranged to Caprolactam. Ammonium sulfate is also generated as by-product. This report was developed based essentially on the following reference(s): (1) "Caprolactam", Ullmann's Encyclopedia of Industrial Chemistry, 7th edition (2) "Cyclohexane", Ullmann's Encyclopedia of Industrial Chemistry, 7th edition Keywords: Cyclohexanone, Cyclohexanol, Lactam Synthesis, Lactam Purification, Ammonium Sulfate Crystallization
This report presents a cost analysis of Methyl Chloride production from methanol and hydrogen chloride The process examined is a typical catalytic vapor phase process. In this process, methanol and anhydrous HCl are combined in vapor phase and passed through a catalyst bed. Reactor vapor outlet is quenched, dried by sulfuric acid scrubbing and then purified to generate high-purity Methyl Chloride. This report was developed based essentially on the following reference(s): (1) "Chloromethanes", Ullmann's Encyclopedia of Industrial Chemistry, 2012; (2) Handbook of Industrial Chemistry and Biotechnology, 2012 Keywords: Chloromethane, R-40, HCC-40, chlorosilanes production
This report presents a cost analysis of Benzene production from pyrolysis gasoline (pygas). The process examined is a typical extractive distillation process. First pygas is fractionated into 3 hydrocarbon cuts, a C5s stream and a heavies stream are generated as by-products. The remaining C6s fraction is then fed to an extractive distillation system to recover benzene. This report was developed based essentially on the following reference(s): "Benzene", Ullmann's Encyclopedia of Industrial Chemistry, 7th edition Keywords: BTX, Aromatics, Hydrotreatment, Diprolene, Distapex, Lurgi, ED
This report presents a cost analysis of Nitrobenzene production from benzene and nitric acid. The process examined is similar to NORAM's adiabatic benzene nitration process. In this process, benzene, nitric acid, and sulfuric acid are sent to a plug-flow nitrator containing jet-impingement elements. The product from nitration is washed and purified, producing technical-grade Nitrobenzene. This report was developed based essentially on the following reference(s): (1) US Patent 20110245547, issued to NORAM International Limited in 2011 (2) "Nitrobenzene and Nitrotoluene", McKetta, J. J. and Cunningham, W. A.. Encyclopedia of Chemical Processing and Design, Vol. 31 Keywords: NORAM, Benzene Nitration
This report presents a cost analysis of Ethylbenzene (EB) production from benzene and polymer grade (PG) ethylene. The process examined is a typical liquid-phase alkylation process using zeolite catalyst. This report was developed based essentially on the following reference(s): Keywords: Ethylbenzene, Ethylene, Benzene, Alkylation, CB&I Lummus/UOP EB One, ExxonMobil/Badger EB Max, Polimeri Europa, Zeolite
This report presents a cost analysis of Cyclohexane from benzene and hydrogen. The process examined is a liquid phase hydrogenation process. In this process, benzene is hydrogenated in a liquid-phase reactor in the presence of a nickel-based catalyst. The reactor's overhead is sent to a second reactor to convert the non-reacted benzene. This report was developed based essentially on the following reference(s): US Patent 5,668,293, issued to Institut Francais du Petrole in 1997 Keywords: Benzene Hexahydride, Cycloalkane, Liquid-Phase Reaction, Hydrogenation Reaction, IFP
This report presents a cost analysis of Benzene production from pyrolysis gasoline (pygas) The process examined is a typical extractive distillation process. First pygas is fractionated into 3 hydrocarbon cuts, a C5s stream and a heavies stream are generated as by-products. The remaining C6s fraction is then fed to an extractive distillation system to recover benzene. This report was developed based essentially on the following reference(s): "Benzene", Ullmann's Encyclopedia of Industrial Chemistry, 7th edition Keywords: BTX, Aromatics, Hydrotreatment, Diprolene, Distapex, Lurgi, ED
This report presents a cost analysis of Linear Alkylbenzene (LAB) production from C10-C13 n-paraffins cut and benzene. The process examined is a typical dehydrogenation/alkylation process. In the process examined, the C10-C13 n-paraffins are dehydrogenated to their respectives olefins, which are further alkylated with benzene to produce the Linear Alkylbenzene (LAB) product. This report was developed based essentially on the following reference(s): Keywords: LAB, Linear Alkyl Benzene, Linear Paraffins, UOP, Pacol Process, DeFine Process, PEP Process
This report presents a cost analysis of Aniline production from nitrobenzene and hydrogen. The process examined is similar to BASF's vapor phase nitrobenzene hydrogenation process. This report was developed based essentially on the following reference(s): Keywords: Bayer, Borsodchem, Sinopec